Simultaneous quantitative measurement of gaseous species composition and solids volume fraction in a gas/solid flow

AIChE Journal

Volumn 56, Issue 11, 2010, Pages 2850-2859

  Laviolette, Jean Philippe ^a   Patience, Gregory S ^a   Chaouki, Jamal ^a  

^a ÉCOLE POLYTECHNIQUE DE MONTRÉAL   (Canada)

Author keywords

Bubble; Emulsion; Fiber optics; Fluidization; FT IR; Gaseous species composition; Infrared spectroscopy; Solids volume fraction

Indexed keywords

ABSORBANCE SPECTRUM; ABSORBANCES; BEAM INTENSITY; BUBBLE; BUBBLE PHASIS; FIBEROPTIC PROBES; FT-IR; FUEL MOLE FRACTIONS; GAS TRACERS; GAS/SOLID FLOW; GASEOUS SPECIES; IN-SITU MEASUREMENT; MOLAR FRACTIONS; NOVEL APPLICATIONS; PROOF OF CONCEPT; QUANTITATIVE MEASUREMENT; RELATIVE ERRORS; SOLIDS VOLUME FRACTION; SPECTROSCOPIC METHOD; TIME-AVERAGED; TRACER GAS;

EMULSIFICATION; FIBER OPTICS; FIBERS; FLUID DYNAMICS; FLUIDIZATION; FLUIDIZED BEDS; INFRARED SPECTROSCOPY; PROBES; SPECTROSCOPIC ANALYSIS; TITRATION;

VOLUME FRACTION;

INSECTIVORA;

EID: 78650343675     PISSN: 00011541     EISSN: 15475905     Source Type: Journal    
DOI: 10.1002/aic.12210     Document Type: Article

References (41)

1. Werther J, Molerus O. The local structure of gas fluidized beds-I. A statistically based measuring system. Int J Multiphase Flow. 1973; 1: 103-122.
2. Yates JG, Simons SRJ. Experimental methods in fluidization research. Int J Multiphase Flow. 1994; 20: 297-330.
3. Hage B, Werther J. The guarded capacitance probe-a tool for the measurement of solids flow patterns in a laboratory and industrial fluidized bed. Powder Technol. 1997; 93: 235-245.
4. Begovich J, Watson JS. An electroconductivity technique for the measurement of axial variation of hold-ups in three-phase fluidized beds. AIChE J. 1978; 24: 351-354.
5. Uribe-Salas A, Gomez CO, Finch JA. A conductivity technique for gas and solids holdup determination in three-phase reactors. Chem Eng Sci. 1994; 49: 1-10.
6. Liu M, Wang T, Yu W, Wang J. An electrical conductivity probe method for measuring the local solid holdup in a slurry system. Chem Eng J. 2007; 132: 37-46.
7. Huizenga P, Meijer R, Kuipers JAM, van Swaaij WPM. Fluoroptic solids holdup measurements in slurry systems. AIChE J. 1998; 44: 982-988.
8. Cutolo A, Rendina I, Arena U, Marzocchella A, Massimilla L. Optoelectronic technique for the characterization of high concentration gas-solid suspension. Appl Opt. 1990; 29: 1317-1322.
9. Ishida M, Tanaka H. Optical probe to detect both bubbles and suspended particles in a three-phase fluidized bed. J Chem Eng Japan. 1982; 15: 389-391.
10. Hu T, Yu B, Wang Y. Holdups and models of three phase fluidized beds. In: Ostergaard K, Sorensen A, editors. Fluidization V. New York: Engineering Foundation, 1986: 353.
11. Esmaeili B, Chaouki J, Dubois C. An evaluation of the solid hold-up distribution in a fluidized bed of nanoparticles using radioactive densitometry and fibre optics. Can J Chem Eng. 2008; 86: 543-552.
12. Gandhi B, Prakash A, Bergougnou MA. Hydrodynamic behaviour of slurry column at high solids concentrations. Powder Technol. 1999; 103: 80-94.
13. Chaouki J, Larachi F, Duduković MP. Noninvasive tomographic and velocimetric monitoring of multiphase flows. Ind Eng Chem Res. 1997; 36: 4476-4503.
14. Pugsley T, Tanfara H, Malcus S, Cui H, Chaouki J, Winters C. Verification of fluidized bed electrical capacitance tomography measurements with a fibre optic probe. Chem Eng Sci. 2003; 58: 3923-3934.
15. Marashdeh Q, Fan LS, Du B, Warsito W. Electrical capacitance tomography-a perspective. Ind Eng Chem Res. 2008; 47: 3708-3719.
16. Razzak SA, Barghi S, Zhu JX, Mi Y. Phase holdup measurements in a gas-liquid-solid circulating fluidized bed (GLSCFB) riser using electrical resistance tomography and optical fibre probe. Chem Eng J. 2009; 147: 210-218.
17. Uchida S, Okamura S, Katsumata T. Measurement of longitudinal distribution of solids holdup in a three-phase fluidized bed by ultrasonic technique. Can J Chem Eng. 1989; 67: 166-169.
18. Luypaert J, Massart DL, Vander Heyden Y. Near-infrared spectroscopy applications in pharmaceutical analysis. Talanta. 2007; 72: 865-883.
19. Swarbrick B. Process analytical technology: a strategy for keeping manufacturing viable in Australia. Vib Spectrosc. 2007; 44: 171-178.
20. Armaroli T, Bécue T, Gautier S. Diffuse reflection infrared spectroscopy (drifts): application to the in situ analysis of catalysts. Oil Gas Sci Technol. 2004; 59: 215-237.
21. Kondo JN, Yang S, Zhu Q, Inagaki S, Domen K. In situ infrared study of n-heptane isomerization over Pt/H-beta zeolites. J Catal. 2007; 248: 53-59.
22. 2 vapor concentration during vapour hydrogen peroxide (VHP) sterilisation. Pharm Res. 1997; 14: 294-298.
23. Rantanen J, Räsänen E, Tenhunen J, Känsäkoski M, Mannermaa J-P, Yliruusi J. In-line moisture measurement during granulation with a four-wavelength near infrared sensor: an evaluation of particle size and binder effects. Eur J Pharm Biopharm. 2000a; 50: 271-276.
24. Rantanen J, Antikainen O, Mannermaa J-P, Yliruusi J. Use of the near-infrared reflectance method for measurement of moisture content during granulation. Pharm Dev Technol. 2000; 5: 209-217.
25. Cogdill RP, Anderson CA, Delgado M, Chisholm R, Bolton R, Herkert T, Afnan AM, Drennen JK III. Process analytical technology case study part I: feasibility studies for quantitative near-infrared method development. AAPS PharmSciTech. 2005; 6: E273-E283.
26. Triadaphillou S, Martin E, Montague G, Norden A, Jeffkins P, Stimpson S. Fermentation process tracking through enhanced spectral calibration modeling. Biotechnol Bioeng. 2007; 97: 554-567.
27. Andersson M, Josefson M, Langkilde FW, Wahlund K-G. Monitoring of a film coating process for tablets using near infrared reflectance spectrometry. J Pharm Biomed Anal. 1999; 20: 27-37.
28. Kirsch JD, Drennen JK. Determination of film-coated tablet parameters by near-infrared spectroscopy. J Pharm Biomed Anal. 1995; 13: 1273-1281.
29. Kirsch JD, Drennen JK. Near-infrared spectroscopic monitoring of the film coating process. Pharm Res. 1996; 13: 234-237.
30. Abrahamsson C, Johansson J, Andersson-Engels S, Svanberg S, Folestad S. Time-resolved NIR spectroscopy for quantitative analysis of intact pharmaceutical tablets. Anal Chem. 2005; 77: 1055-1059.
31. Hailey PA, Doherty P, Tapsell P, Oliver T, Aldridge PK. Automated system for the on-line monitoring or powder blending processes using near-infrared spectroscopy. Part I. system development and control. J Pharm Biomed Anal. 1996; 14: 551-559.
32. Sonja Sekulic S, Wakeman J, Doherty P, Hailey PA. Automated system for the on-line monitoring of powder blending processes using near-infrared spectroscopy: Part II. Qualitative approaches to blend evaluation. J Pharm Biomed Anal. 1998; 17: 1285-1309.
33. Sonja Sekulic S, Ward HW, Brannegan DR, Stanley ED, Evans CL, Sciavolino ST, Hailey PA, Aldridge PK. On-line monitoring of powder blend homogeneity by near-infrared spectroscopy. Anal Chem. 1996; 68: 509-513.
34. Frake P, Greenhalgh D, Grierson SM, Hempenstall JM, Rudd DR. Process control and end-point determination of a fluid bed granulation by application of near infra-red spectroscopy. Int J Pharm. 1997; 151: 75-80.
35. Bellamy LJ, Nordon A, Littlejohn D. Real-time monitoring of powder mixing in a convective blender using non-invasive reflectance NIR spectrometry. The Analyst. 2008; 133: 58-64.
36. Cui H, Mostoufi N, Chaouki J. Comparison of measurement techniques of local particle concentration for gas-solid fluidization. In: Kwauk M, Li J, Yang W-C, editors. Fluidization X. New York: Engineering Foundation, 2001: 779-786.
37. De Paepe ATG, Dyke JM, Hendra PJ, Langkilde FW. Rotating samples in FT-RAMAN spectrometers. Spec Acta Part A. 1997; 53: 2261-2266.
38. Berntsson O, Danielsson L-G, Folestad S. Characterization of diffuse reflectance fiber probe sampling on moving solids using a Fourier transform near-infrared spectrometer. Anal Chim Acta. 2001; 431: 125-131.
39. Andersson M, Svensson O, Folestad S, Josefson M, Wahlund K-G. NIR spectroscopy on moving solids using a scanning grating spectrometer-impact on multivariate process analysis. Chemometr Intell Lab Sys. 2005; 75: 1-11.
40. Skoog DA, Holler FJ, Crouch SR. Principles of Instrumental Analysis, 6th Ed. Independence, KY: Brooks Cole, 2006.
41. Cui H, Sauriol P, Chaouki J. High temperature fluidized bed reactor: measurements, hydrodynamics and simulation. Chem Eng Sci. 2003; 58: 1071-1077.