Facile and manifest spectrophotometric methods for the determination of six quinolone antibiotics in pharmaceutical formulations using iron salts

Medicinal Chemistry Research

Volumn 19, Issue 9, 2010, Pages 1259-1272

  Siddiqui, Farhan Ahmed ^a   Arayne, M Saeed ^a   Sultana, Najma ^a   Mirza, Agha Zeeshan ^a   Qureshi, Faiza ^a   Zuberi, M Hashim ^a  

^a UNIVERSITY OF KARACHI   (Pakistan)

Author keywords

Ciprofloxacin; Gatifloxacin; Levofloxacin; Norfloxacin; Ofloxacin; Pefloxacin

Indexed keywords

CIPROFLOXACIN; FERRIC AMMONIUM CITRATE; FERRIC CHLORIDE; GATIFLOXACIN; IRON; IRON SALT; LEVOFLOXACIN; NORFLOXACIN; OFLOXACIN; PEFLOXACIN;

ARTICLE; CHEMICAL REACTION; COMPLEX FORMATION; CONCENTRATION (PARAMETERS); DRUG DETERMINATION; SPECTROPHOTOMETRY;

EID: 78650171579     PISSN: 10542523     EISSN: None     Source Type: Journal    
DOI: 10.1007/s00044-009-9268-7     Document Type: Article

References (23)

1. Arayne MS, Sultana N, Siddiqui FA, Mirza AZ, Zuberi MH (2008) Spectrophotometric techniques to determine tranexamic acid; kinetic studies using ninhydrin and direct measuring using ferric chloride. J Mol Struct. doi: 10.1016/j.molstruc.2008.04.026
2. Arayne MS, Sultana N, Rizvi SBS, Haroon U (2009) In vitro drug interaction studies of atorvastatin with ciprofloxacin, gatifloxacin, and ofloxacin. Med Chem Res. doi: 10.1007/s00044-009-9225-5
3. F Belal AA Al-Majed AM Al-Obaid 1999 Methods analysis 4-quinolone antibacterials Talanta 50 765 786 1:CAS:528:DyaK1MXmvFCis74%3D 10.1016/S0039-9140(99)00139-3 18967768
4. HA Benesi JH Hildebrand 1949 A spectrophotometric investigation of the interaction of iodine with aromatic hydrocarbons J Am Chem Soc 71 8 2703 2707 1:CAS:528:DyaH1MXktlCisA%3D%3D 10.1021/ja01176a030
5. SK Bhowal TK Das 1991 Spectrophotometric determination of same recently introduced antibacterial drugs using ferric chloride Anal Lett 24 25 37 1:CAS:528:DyaK3MXhvFaksbs%3D
6. British Pharmacopoeia (1999) British Pharmacopoeia, vol 1. Her Majesty's Stationary Office, London, pp 69-370, 1034-1035
7. G Carlucci 1998 Analysis of fluoroquinolones in biological fluids by high-performance liquid chromatography J Chromatogr A 812 343 367 1:CAS:528:DyaK1cXktFGksLw%3D 10.1016/S0021-9673(98)00274-X 9691331 (Pubitemid 28300447)
8. DK Chen A McGeer JCD Azavedo DE Low 1999 Decreased susceptibility of Streptococcus pneumoniae to fluoroquinolones in Canada N Engl J Med 341 233 239 1:CAS:528:DyaK1MXltVOjurY%3D 10.1056/NEJM199907223410403 10413735 (Pubitemid 29334521)
9. D Currie L Lynas DG Kennedy WJ McCaughey 1998 Evaluation of modified EC four-plate method to detect antimicrobial drugs Food Addit Contam 15 651 660 1:CAS:528:DyaK1cXlvVSlur8%3D 10209575
10. CL Flurer 1997 Analysis of antibiotics by capillary electrophoresis Electrophoresis 18 2427 2437 1:CAS:528:DyaK1cXis1Wlug%3D%3D 10.1002/elps. 1150181233 9456057 (Pubitemid 28020603)
11. MI Franch JA Ayllón J Peral X Domènech 2004 Fe(III)-photocatalysed degradation of low chain carboxylic acids. Implication of the iron salt Appl Catal B Environ 50 89 99 1:CAS:528:DC%2BD2cXjs1Wlu7k%3D 10.1016/j.apcatb.2003.12.024 (Pubitemid 38572564)
12. L Fratini EES Schapoval 1996 Ciprofloxacin determination by visible light spectrophotometry using iron(III) nitrate Int J Pharm 127 279 282 1:CAS:528:DyaK28Xhslegtb8%3D 10.1016/0378-5173(95)04290-3 (Pubitemid 26092140)
13. M Gopalakrishnan J Thanusu V Kanagarajan 2007 Synthesis and biological evaluation of 5,7-diaryl-4,4-dimethyl-4,5,6,7-tetrahydropyridino[3,4-d]-1,2,3- thiadiazoles Med Chem Res 16 392 401 1:CAS:528:DC%2BD1cXks12qsrw%3D 10.1007/s00044-007-9051-6
14. PJ Ihrke MG Papich TC Demanuelle 1999 The use of fluoroquinolones in veterinary dermatology Vet Dermatol 10 193 204 10.1046/j.1365-3164.1999.00179.x
15. Jayashree BS, Thomas S, Nayak Y (2009) Design and synthesis of 2-quinolones as antioxidants and antimicrobials: a rational approach. Med Chem Res. doi: 10.1007/s00044-009-9184-x
16. S Joshi 2002 HPLC separation of antibiotics present in formulated and unformulated samples J Pharm Biomed Anal 28 795 809 1:CAS:528: DC%2BD38XktVaqtrY%3D 10.1016/S0731-7085(01)00706-3 12039621 (Pubitemid 34564523)
17. Martin AN, Swarbrick J, Cammarata A (1969) Physical pharmacy, 3rd edn. Lee & Febiger, Philadelphia, p 344
18. VF Samanidou CE Demetriou IN Papadoyannis 2003 Direct determination of four fluoroquinolones, enoxacin, norfloxacin, ofloxacin, and ciprofloxacin, in pharmaceuticals and blood serum by HPLC Anal Bioanal Chem 375 623 629 1:CAS:528:DC%2BD3sXitVagsbg%3D 12638045
19. D Sanzgiri SR Knaub CM Riley 1994 Quantitative determination of gatifloxacin, levofloxacin, lomefloxacin and pefloxacin fluoroquinolonic antibiotics in pharmaceutical preparations by high-performance liquid chromatography Anal Profiles Drug Subst Excipients 23 325 369
20. M Shaharyar MA Ali MM Abdullah 2007 Synthesis and antiproliferative activity of 1-[(sub)]-6-fluoro-3-[(sub)]-1,3,4-oxadiazol-2-yl-7-piperazino-1,4- dihydro-4-quinolinone derivatives Med Chem Res 16 292 299 1:CAS:528: DC%2BD1cXjslCjur0%3D 10.1007/s00044-007-9031-x
21. SW Sun LY Chen 1997 Optimization of capillary electrophoretic separation of quinolone antibacterials using the overlapping resolution mapping scheme J Chromatogr A 766 215 224 1:CAS:528:DyaK2sXisF2isLk%3D 10.1016/S0021-9673(96) 00992-2 (Pubitemid 27166350)
22. K Venugopal RN Saha 2005 New, simple, and validated UV-spectrophotometric methods for the estimation of gatifloxacin in bulk and formulations Il Farmaco 60 906 912 1:CAS:528:DC%2BD2MXhtFyktrjL 10.1016/j.farmac.2005.08.010 16226753 (Pubitemid 41586265)
23. Wolfson JS, Hooper DC (1989) Introduction. In: Wolfson JS, Hooper DC (eds) Quinolone antimicrobial agents. American Society for Microbiology, Washington, DC, pp 1-4