Simultaneous spectrophotometric determination of losartan potassium, amlodipine besilate and hydrochlorothiazide in pharmaceuticals by chemometric methods

Acta Pharmaceutica

Volumn 60, Issue 2, 2010, Pages 141-152

  Nagavalli, D ^a   Vaidhyalingam, V ^b   Santha, A ^c   Sankar, A ^a   Divya, O ^d  

^a Adhiparasakthi College of Pharmacy   (India)

^b MADRAS MEDICAL COLLEGE   (India)

^c C L BAID METHA COLLEGE OF PHARMACY   (India)

^d INDIAN INSTITUTE OF TECHNOLOGY MADRAS   (India)

Author keywords

amlodipin besilat; amlodipine besilate; chemometry; hidroklorotiazid; hydrochlorothiazide; kemometrija; losartan; losartan potassium; spectrophotometry; spektrofotometrija

Indexed keywords

AMLODIPINE BESYLATE; HYDROCHLOROTHIAZIDE; LOSARTAN POTASSIUM;

ARTICLE; CALIBRATION; CHEMOMETRIC ANALYSIS; HUMAN; MULTIPLE LINEAR REGRESSION ANALYSIS; NONHUMAN; PARTIAL LEAST SQUARES REGRESSION; PRINCIPAL COMPONENT ANALYSIS; REGRESSION ANALYSIS; SPECTROPHOTOMETRY; TABLET FORMULATION;

EID: 78650102573     PISSN: 13300075     EISSN: 18469558     Source Type: Journal    
DOI: 10.2478/v10007-010-0017-8     Document Type: Article

References (23)

1. th ed., Merck and Co. Inc., White House Station 2003.
2. N. Erk, Analysis of binary mixtures of losartan potassium and hydrochlorothiazide by using high performance liquid chromatography, ratio derivative spectrophotometric and compensation technique, J. Pharm. Biomed. Anal. 24 (2001) 603-611.
3. D. L. Hertzog, J. F. McCafferty, X. Fang, R. J. Tyrrell, R. A. Reed, Development and validation of a stability-indicating HPLC method for the simultaneous determination of losartan potassium, hydrochlorothiazide, and their degradation products, J. Pharm. Biomed. Anal. 30 (2002) 747-760.
4. M. Polinko, K. Riffel, S. Hengchang and L. O. Man-Wai, Simultaneous determination of losartan and EXP3174 in human plasma and urine utilizing liquid chromatography/tandem mass spec-trometry, J. Pharm. Biomed. Anal. 33 (2003) 73-84; DOI:10.1016/S0731-7085(03)00348-0. (Pubitemid 37297519)
5. R. K. Barman, M. A. Islam, M. Ahmed, M. I. Ibnewahed, R. Islam, A. Khan, M. B. Hossain and B. M. Rahman, Simultaneous high-performance liquid chromatographic determination of atenolol and amlodipine in pharmaceutical- dosage form, Pak. J. Pharm. Sci. 20 (2007) 274-279.
6. M. D. Malesuik, S. G. Cardoso, L. Bajerski and F. A. Lanzanova, Determination of amlodipine in pharmaceutical dosage forms by liquid chromatography and ultraviolet spectrophotometry, J. AOAC Int. 89 (2006) 359-364.
7. F. Belal, I. A. Al-Zaagi, E. A. Gadkariem and M. A. Abounassif, A stability-indicating LC method for the simultaneous determination of ramipril and hydrochlorothiazide in dosage forms, J. Pharm. Biomed. Anal. 24 (2001) 335-342.
8. O. C. Lastra, I. G. Lemus, H. J. Sánchez and R. F. Pérez, Development and validation of a UV derivative spectrophotometric determination of losartan potassium in tablets, J. Pharm. Biomed. Anal. 33 (2003) 175-180.
9. M. C. Ferro, P. M. Castellano and T. S. Kaufman, Simultaneous determination of amiloride hy-drochloride and hydrochlorothiazide in synthetic samples and pharmaceutical formulations by multivariate analysis of spectrophotometric data, J. Pharm. Biomed. Anal. 30 (2002) 1121-1131.
10. M. A. Obando, J. M. Estela and V. Cerda, Simultaneous determination of hydrochlorothiazide and losartan potassium in tablets by high-performance low-pressure chromatography using a multi-syringe burette coupled to a monolithic column, Anal. Bioanal. Chem. 391 (2008) 2349-2356.
11. S. A. Shah, I. S. Rathod, B. N. Suhagia, S. S. Savale and J. B. Patel, Simultaneous determination of losartan and hydrochlorothiazide in combined dosage forms by first-derivative spectroscopy and high-performance thin-layer chromatography, J. AOAC Int. 84 (2001) 1715-1723.
12. R. B. Kakde, V. H. Kotak and D. L. Kale, High performance thin layer chromatographic method for simultaneous estimation of amlodipine besilate and bisoprolol fumarate in pharmaceutical preparations, Pharma Rev. Dec-2008, 168-170.
13. Y. Ma, F. Qin, X. Sun, X. Lu and F. Li, Determination and pharmacokinetic study of amlodipine in human plasma by ultra performance liquid chromatography-electrospray ionization mass spectrometry, J. Pharm. Biomed. Anal. 43 (2007) 1540-1545. (Pubitemid 46282391)
14. R. Kramer, Chemometric Techniques in Quantitative Analysis, Marcel Dekker, New York 1998.
15. H. Martens and T. Naes, Multivariate Calibration, Wiley, New York 1989.
16. E. Dinç and A. Ozdemir, Linear regression analysis and its application to multivariate chroma-tographic calibration for the quantitative analysis of two-component mixtures, Farmaco 60 (2005) 591-597.
17. R. Brereton, Chemometrics. Data Analysis for the Laboratory and Chemical Plant, Wiley, Chichester 2003.
18. R. Bro, Håndbog i Multivariabel Kalibrering, Jordbrugsforlaget, Copenhagen, 1996.
19. E. Dinç and D. Baleanu, Spectrophotometric quantitative determination of cilazapril and hydro-chlorothiazide in tablets by chemometric methods, J. Pharm. Biomed. Anal. 30 (2002) 715-723.
20. Nagaraj, K. Vipul and M. Rajshree, Simultaneous quantitative resolution of atorvastatin calcium and fenofibrate in pharmaceutical preparation by using derivative ratio spectrophotometry and chemometric calibrations, Anal. Sci. 23 (2007) 445-451; DOI: 10.2116/analsci.23.445.
21. I. M. Palabiyik, E. Dinç and F. Onur, Simultaneous spectrophotometric determination of pse-udoephedrine hydrochloride and ibuprofen in a pharmaceutical preparation using ratio spectra derivative spectrophotometry and multivariate calibration techniques, J. Pharm. Biomed. Anal. 34 (2004) 473-483.
22. R. G. Brereton, Multilevel multifactor designs for multivariate calibration, Analyst 122 (1997) 1521-1529.
23. G. R. Flåten and A. D. Walmsley, Using design of experiments to select optimum calibration model parameters, Analyst 128 (2003) 935-943; DOI: 10.1039/b301555f. (Pubitemid 36897886)