A simple and rapid dispersive liquid-liquid microextraction method followed by GC-FID for determination of N-methylpyrrolidine in cefepime

Journal of Separation Science

Volumn 33, Issue 23-24, 2010, Pages 3767-3773

  Farajzadeh, Mir Ali ^a   Goushjuii, Leila ^a   Bashour, Yousef ^b  

^a UNIVERSITY OF TABRIZ   (Iran)

^b Daana Pharmaceutical Company   (Iran)

Author keywords

Cefepime; Dispersive liquid liquid microextraction; Gas chromatography; N methylpyrrolidine

Indexed keywords

CALIBRATION GRAPHS; CEFEPIME; CORRELATION COEFFICIENT; DISPERSIVE LIQUID-LIQUID MICROEXTRACTION; EXPERIMENTAL FACTORS; EXTRACTION SOLVENTS; EXTRACTION TIME; GAS CHROMATOGRAPHY-FLAME IONIZATION DETECTIONS; METHYLPYRROLIDINE; OPTIMIZED CONDITIONS; PREPARATION PROCEDURES; REAL SAMPLES; SALT EFFECT; SALTING-OUT AGENTS; SAMPLE PREPARATION TECHNIQUES; SAMPLE SIZES;

GAS CHROMATOGRAPHY; IONIZATION OF GASES; IONIZATION OF LIQUIDS; LIQUID CHROMATOGRAPHY; LIQUIDS; OPTIMIZATION; ORGANIC SOLVENTS; PH EFFECTS; SAMPLING; SODIUM CHLORIDE;

SOLVENT EXTRACTION;

BICARBONATE; CARBONIC ACID; CEFEPIME; CHLOROFORM; METHANOL; METHYLPYRROLIDINE; PYRROLIDINE DERIVATIVE; SODIUM CHLORIDE; UNCLASSIFIED DRUG; WATER;

ARTICLE; DRUG STRUCTURE; GAS CHROMATOGRAPHY; HYDROLYSIS; LIQUID LIQUID EXTRACTION; LIQUID PHASE MICROEXTRACTION; PRIORITY JOURNAL; SOLVENT EXTRACTION;

ANTI-BACTERIAL AGENTS; BUFFERS; CEPHALOSPORINS; CHROMATOGRAPHY, GAS; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; OSMOLAR CONCENTRATION; PYRROLIDINES; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SOLVENTS;

EID: 78650102442     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201000510     Document Type: Article

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