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Volumn 52, Issue 1, 2011, Pages 117-121

Asymmetric Michael addition catalysed by sugar-based prolinamides in solvent-free conditions

Author keywords

[No Author keywords available]

Indexed keywords

AMIDE; BENZOIC ACID; CYCLOHEXANONE; GLUCOSAMINE; KETONE; PROLINAMIDE; PROLINE; UNCLASSIFIED DRUG;

EID: 78649895764     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2010.10.148     Document Type: Article
Times cited : (38)

References (38)
  • 31
    • 78649842570 scopus 로고    scopus 로고
    • 1H NMR analysis to determine the diastereomeric ratio of syn and anti adducts. The reaction mixture was subjected to silica gel column chromatography using ethyl acetate and hexane (10:90-20:80) as eluent to afford pure product. The HPLC analysis of the Michael product was performed on a chiral stationary phase using hexane-isopropanol as eluting solvent
    • 1H NMR analysis to determine the diastereomeric ratio of syn and anti adducts. The reaction mixture was subjected to silica gel column chromatography using ethyl acetate and hexane (10:90-20:80) as eluent to afford pure product. The HPLC analysis of the Michael product was performed on a chiral stationary phase using hexane-isopropanol as eluting solvent.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.