A new oxomolybdate component extracted from the "virtual dynamic library" yielding the macrocyclic anion [(MoVI 8O 28)4(MoV 2O2S 2)4]24-

Inorganic Chemistry

Volumn 49, Issue 21, 2010, Pages 9740-9742

  Korenev, Vladimir S ^a,b   Boulay, Antoine G ^a   Dolbecq, Anne ^a   Sokolov, Maxim N ^b   Hijazi, Akram ^a   Floquet, Sébastien ^a   Fedin, Vladimir P ^b   Cadot, Emmanuel ^a  

^a UNIVERSITÉ DE VERSAILLES SAINT QUENTIN EN YVELINES   (France)

^b NIKOLAEV INSTITUTE OF INORGANIC CHEMISTRY   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 78049299188     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic101545w     Document Type: Article

References (34)

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16. VI).
17. -3. The countercation (ammonium and potassium) and crystallization water appear severely disordered within the structure and thereby could not be distinguished from the observed electron densities; therefore, all of these positions were refined as O atoms and considered as crystallization water. The data set was corrected with the program SQUEEZE (PLATON package of crystallographic software) used to remove the disordered solvent or counterion contribution to the overall intensity data.
18. 8: K, 0.53; N, 4.39; H, 2.58; Mo, 52.33; S, 3.49. Found: K, 0.57; N, 4.19; H, 2.23; Mo, 52.72; S, 3.70. Elemental analyses were carried out by the Laboratoire Central d'Analyse du CNRS, Solaize, France.
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