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Volumn 51, Issue 47, 2010, Pages 6177-6180

A new catalytic method for the synthesis of boroxanes

Author keywords

Boronic acids; Homogenous catalysis; Ruthenium coupling reactions; Vinylboronates

Indexed keywords

BORONIC ACID DERIVATIVE; ETHYLENE; HYDROGEN; RUTHENIUM;

EID: 77958506535     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2010.09.094     Document Type: Article
Times cited : (10)

References (36)
  • 35
    • 77958501521 scopus 로고    scopus 로고
    • note
    • 3)] (II) (2 mol%) was dissolved in 1,4-dioxane and placed in a glass ampoule. Dodecane (used as internal standard, 5% by volume all components), boronic acid (0.5 mmol), and 2-vinyl-1,3,2-dioxaborinane (1-2 mmol) were added. The ampoule was heated at 80 °C for 24 h. The conversion of boronic acid was determined by GC. After the reaction, the solvent and excess borane were removed under vacuum and the crude product was purified by column chromatography (silica gel modified with HMDS) with hexane/EtOAc as eluent.
  • 36
    • 77958464403 scopus 로고    scopus 로고
    • note
    • 1H NMR spectroscopy.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.