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Volumn 1217, Issue 46, 2010, Pages 7255-7264

Separation of triphenyl atropisomers of a pharmaceutical compound on a novel mixed mode stationary phase: A case study involving dynamic chromatography, dynamic NMR and molecular modeling

(4) Bu, X a Skrdla, P J a Dormer, P G a Bereznitski, Y a

a MERCK RESEARCH LABORATORIES (United States)

Author keywords

Atropisomer separation; Dynamic HPLC; Interconversion kinetics; Molecular modeling; NMR

Indexed keywords

ALTERNATIVE APPROACH; ATROPISOMER SEPARATION; ATROPISOMERS; AXIAL ROTATION; CHIRAL CENTERS; CHIRAL MOLECULE; CHIRAL STATIONARY PHASIS; CHROMATOGRAPHIC CONDITIONS; COLUMN SEPARATION; DIASTEREOMERS; DYNAMIC CHROMATOGRAPHY; DYNAMIC NMR; ELUTION PROFILES; INTERCONVERSION KINETICS; INTERCONVERSION PROCESS; INTERCONVERSIONS; KINETIC DATA; KINETIC INFORMATION; LOW TEMPERATURES; MIXED MODE; MOLECULAR MODELING STUDIES; NMR; PEAK AREA; PHARMACEUTICAL COMPOUNDS; PHARMACEUTICAL INDUSTRY; STATIONARY PHASE; STATIONARY PHASIS; TEMPERATURE RANGE; THERMODYNAMIC INFORMATION; VARIABLE-TEMPERATURE NMR;

CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; DRUG PRODUCTS PLANTS; MOLECULAR MODELING; TEMPERATURE;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

BENZENE DERIVATIVE; TRIPHENYL DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; ATROPISOMER; CHEMICAL ANALYSIS; CHEMICAL REACTION KINETICS; CONTROLLED STUDY; DYNAMIC HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ENERGY TRANSFER; FLOW RATE; IONIC STRENGTH; LIQUID CHROMATOGRAPHY; MOLECULAR DYNAMICS; MOLECULAR MODEL; PH; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; SENSITIVITY AND SPECIFICITY; STEREOISOMERISM; TEMPERATURE SENSITIVITY; THERMODYNAMICS;

ALGORITHMS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HYDROGEN-ION CONCENTRATION; KINETICS; LINEAR MODELS; MODELS, MOLECULAR; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PHARMACEUTICAL PREPARATIONS; STEREOISOMERISM; TERPHENYL COMPOUNDS; THERMODYNAMICS;

EID: 77958112417 PISSN: 00219673 EISSN: None Source Type: Journal
DOI: 10.1016/j.chroma.2010.09.042 Document Type: Article

Times cited : (18)

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