Characterization and identification of steroidal alkaloids in Fritillaria species using liquid chromatography coupled with electrospray ionization quadrupole time-of-flight tandem mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 45, 2010, Pages 7109-7122

  Zhou, Jian Liang ^a   Xin, Gui Zhong ^a   Shi, Zi Qi ^a   Ren, Mei Ting ^a   Qi, Lian Wen ^a   Li, Hui Jun ^a   Li, Ping ^a  

^a CHINA PHARMACEUTICAL UNIVERSITY   (China)

Author keywords

Characterization; Fragmentation; Fritillaria; LC ESI QTOF MS MS; Steroidal alkaloids

Indexed keywords

FRAGMENT IONS; FRAGMENTATION; FRAGMENTATION BEHAVIOR; FRAGMENTATION PATHWAYS; FRITILLARIA; LC/ESI-QTOF-MS/MS; NATURAL PRODUCTS; NO REFERENCES; QUADRUPOLES; REFERENCE COMPOUNDS; RELATIVE ABUNDANCE; RING CLEAVAGE; STEROIDAL ALKALOIDS; STRUCTURAL ELUCIDATION; TANDEM MASS SPECTROMETRY; TIME OF FLIGHT; TRADITIONAL CHINESE MEDICINE;

ELECTROSPRAY IONIZATION; IONIZATION; IONS; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; MEDICINE; NITROGEN COMPOUNDS; PARTICLE DETECTORS; REACTION KINETICS;

METABOLITES;

ALKALOID; EBEIEDINE; EBEIEDINONE; EBEIENINE; FRITILLARIA EXTRACT; HUPEHENINOSIDE; IMPERIALINE; IMPERIALINE 3 BETA DEXTRO GLUCOSIDE; ISOVERTICINE; N DEMETHYLPUQIETINONE; PEIMISINE; PLANT EXTRACT; PUQIEDINE; PUQIEDINE 7 OL; PUQIEDINONE; PUQIENINE A; PUQIENINE B; PUQIENINE C; PUQIENINE D; PUQIENINE E; PUQIENINE F; PUQIETINEDINONE; PUQIETINONE; PUQIETINONOSIDE; UNCLASSIFIED DRUG; UNINDEXED DRUG; VERTICINE; VERTICINE N OXIDE; VERTICINONE; VERTICINONE N OXIDE; YIBEINOSIDE A;

ARTICLE; CONTROLLED STUDY; DRUG IDENTIFICATION; DRUG ISOLATION; DRUG STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; FRITILLARIA; LIQUID CHROMATOGRAPHY; NONHUMAN; PRIORITY JOURNAL; QUADRUPOLE MASS SPECTROMETRY; TANDEM MASS SPECTROMETRY; TIME OF FLIGHT MASS SPECTROMETRY;

CHROMATOGRAPHY, LIQUID; DRUGS, CHINESE HERBAL; FRITILLARIA; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; STEROIDS; TANDEM MASS SPECTROMETRY; VERATRUM ALKALOIDS;

EID: 77957877687     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.09.019     Document Type: Article

References (36)

1. Sho I., Michiharu K., Tetsuo N. Chem. Pharm. Bull. 1963, 11:1337.
2. Kaneko K., Tanaks M., Nakaoka U., Tanaka Y., Yoshida N., Mitsuhshi H. Phytochemistry 1981, 20:327.
3. Lin G., Li P., Li S.L., Chan S.W. J. Chromatogr. A 2001, 935:321.
4. Shang Z.J., Liu X.L. Chin. J. Med. Hist. 1995, 25:38.
5. Kaneko K., Katsuhara T., Mitsuhashi H. Tetrahedron Lett. 1986, 27:2387.
6. Oh H., Kang D.G., Lee S.Y., Li Y.M., Lee H.S. Planta Med. 2003, 69:564.
7. Atta-ur-Rahman, Akhtar M.N., Choudhary M.I., Tsuda Y., Sener B., Khalid A., Parvez M. Chem. Pharm. Bull. 2002, 50:1013.
8. Atta-ur-Rahman, Farooq A., Choudhary M.I., Gilani A.H., Shaheen F., Ali R.A., Noor-e-ain F., Sener B. Planta Med. 1994, 60:377.
9. Gilani A.H., Shaheen F., Christopoulos A., Mitchelson F. Life Sci. 1997, 60:535.
10. Jiang Y., Li H.J., Li P., Cai Z.H., Ye W.C. J. Nat. Prod. 2005, 68:264.
11. Zhang Y.H., Ruan H.L., Pi H.F., Cai J.Y., Zeng F.B., Zhao W., Wu J.Z. Chin. Tradit. Herb. Drugs 2005, 36:1205.
12. Li H.J., Jiang Y., Li P. Nat. Prod. Rep. 2006, 23:735.
13. Zhou J.L., Li P., Li H.J., Jiang Y., Ren M.T., Liu Y. J. Chromatogr. A 2008, 1177:126.
14. Qi L.W., Gu X.J., Li P., Liang Y., Hao H.P., Wang G.J. Rapid Commun. Mass Spectrom. 2009, 23:2151.
15. Zhu Z.Y., Zhang H., Zhao L., Dong X., Li X., Chai Y.F., Zhang G.Q. Rapid Commun. Mass Spectrom. 2007, 21:1855.
16. Li H.L., Tang J., Liu R.H., Lin M., Wang B., Lv Y.F., Huang H.Q., Zhang C., Zhang W.D. Rapid Commun. Mass Spectrom. 2007, 21:869.
17. Miao X.S., March R.E., Metcalfe C.D. Int. J. Mass Spectrom. 2003, 230:123.
18. Li C.M., Zhang X.L., Xue X.Y., Zhang F.F., Xu Q., Liang X.M. Rapid Commun. Mass Spectrom. 2008, 22:1941.
19. Zhou Y., Han Q.B., Song J.Z., Qiao C.F., Xu H.X. J. Chromatogr. A 2008, 1206:131.
20. Lin G., Ho Y.P., Li P., Li X.G. J. Nat. Prod. 1995, 58:1662.
21. Li H.J., Jiang Y., Li P., Ye W.C. Chem. Pharm. Bull. 2006, 54:722.
22. Jiang Y., Li P., Li H.J., Yu H. Steroids 2006, 71:843.
23. Lee P., Kitamura Y., Kaneko K., Shiro M., Xu G.J., Chen Y.P., Hsu H.Y. Chem. Pharm. Bull. 1988, 36:4316.
24. Li P., Kitamura Y., Kaneko K., Shiro M., Xu G.J., Chen Y.P., Hsu H.Y. Phytochemistry 1992, 31:2190.
25. Kasprzyk-Hordem B., Dinsdale R.M., Guwy A.J. J. Chromatogr. A 2007, 1161:132.
26. Xu D.M., Zhang B., Li H.R., Xu M.L. Acta Pharm. Sin. 1982, 17:355.
27. Xu D.M., He C.H., Wang S.Q., Huang E.X., Xu M.L., Wen X.G. Acta Pharm. Sin. 1990, 25:127.
28. Yukie K., Makoto N., Koh K. Tetrahedron 1989, 45:5755.
29. Yukie K., Makoto N., Koh K. Tetrahedron 1989, 45:7281.
30. Ruan H.L., Zhang Y.H., Wu J.Z. Nat. Prod. Res. Dev. 2001, 14:80.
31. Xu D.M., Arihara S., Shoji N., Yang X.W., Huang E.X., Li C.S. Acta Pharm. Sin. 1990, 25:795.
32. Zhang J.X., Lao A.N., Xu R.S. Acta Bot. Sin. 1993, 35:238.
33. Xu D.M., Zhang B., Xiao Y.W. Acta Pharm. Sin. 1983, 18:868.
34. Xu Y.J., Xu D.M., Cui D.B., Huang E.X., Jin X.Q., Lin S.Y., Yan M.M. Acta Pharm. Sin. 1993, 28:192.
35. Zhang J.X., Lao A.N., Xu R.S. Acta Bot. Sin. 1993, 35:963.
36. Xu D.M., Xu M.L., Wang S.Q., Huang E.X., Wen X.G. J. Nat. Prod. 1990, 53:549.