Polyoxometallate-thiosemicarbazone hybrid compounds

European Journal of Inorganic Chemistry

Volumn , Issue 28, 2010, Pages 4513-4525

  Gil García, Rubén ^a   Zichner, René ^a   Díez Gómez, Virginia ^b   Donnadieu, Bruno ^c   Madariaga, Gotzon ^d   Insausti, Maite ^d   Lezama, Luis ^d   Vitoria, Pablo ^d   Pedrosa, María R ^a   García Tojal, Javier ^a  

^a UNIVERSITY OF BURGOS   (Spain)

^b INSTITUTO DE CIENCIA DE MATERIALES DE MADRID   (Spain)

^c UNIVERSITY OF CALIFORNIA   (United States)

^d UNIVERSITY OF THE BASQUE COUNTRY UPV EHU   (Spain)

Author keywords

Copper; Molybdenum; Polyoxometallates; Thiosemicarbazone complexes; Vanadium

Indexed keywords

COPPER; COPPER COMPOUNDS; MOLYBDENUM; NEGATIVE IONS; PYRIDINE; SYNTHESIS (CHEMICAL); VANADIUM; VANADIUM COMPOUNDS;

CARBALDEHYDES; DECAVANADATE ANION; HEXAMOLYBDATES; HYBRID COMPOUNDS; OCTAMOLYBDATES; POLYOXOMETALLATES; PYRIDINE-2; SYNTHESISED; THIOSEMICARBAZONE COMPLEXES; THIOSEMICARBAZONES;

PHENOLS;

EID: 77957813964     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.201000484     Document Type: Article

References (90)

1. M. T. Pope, A. Müller, Polyoxometalates: From Platonic Solids to Anti-Retroviral Activity, Kluwer, Dordrecht, 1994;
2. T. Yamase, M. T. Pope, Polyoxometalate Chemistry for Nano-Composite Design, Kluwer, New York, 2002;
3. D.-L. Long, E. Burkholder, L. Cronin, Chem. Soc. Rev. 2007, 36, 105-121.
4. M. T. Pope, Heteropoly and Isopoly Oxometalates, Springer, Berlin, 1983.
5. A. Proust, R. Thouvenot, P. Gouzerh, Chem. Commun. 2008, 1837-1852.
6. Z. Shi, X. Gu, J. Peng, Z. Xin, Eur. J. Inorg. Chem. 2005, 3811-3814.
7. H.-Y. An, E.-B. Wang, D.-R. Xiao, Y.-G. Li, Z.-M. Su, L. Xu, Angew. Chem. Int. Ed. 2006, 45, 904-908;
8. Z. Shi, X. Gu, J. Peng, X. Yu, E. Wang, Eur. J. Inorg. Chem. 2006, 385-388;
9. H. Jin, Y. Qi, E. Wang, Y. Li, C. Qin, W. Wang, S. Chang, Eur. J. Inorg. Chem. 2006, 4541-4545;
10. C. Ritchie, E. Burkholder, P. Kögerler, L. Cronin, Dalton Trans. 2006, 1712-1714;
11. R.-Q. Fang, Y.-F. Zhao, X.-M. Zhang, Inorg. Chim. Acta 2006, 359, 2023-2028;
12. K. Pavani, S. E. Lofland, K. V. Ramanujachary, A. Ramanan, Eur. J. Inorg. Chem. 2007, 568-578;
13. V. Shivaiah, T. Chatterjee, K. Srinivasu, S. K. Das, Eur. J. Inorg. Chem. 2007, 231-234;
14. J. Sha, J. Peng, H. Liu, J. Chen, B. Dong, A. Tian, Z. Su, Eur. J. Inorg. Chem. 2007, 1268-1274;
15. R. P. Bontchev, E. L. Venturini, M. Nyman, Inorg. Chem. 2007, 46, 4483-4491;
16. H. An, T. Xu, E. Wang, C. Meng, Inorg. Chem. Commun. 2007, 10, 1453-1456;
17. L. Yuan, C. Qin, X. Wang, E. Wang, S. Chang, Eur. J. Inorg. Chem. 2008, 4936-4942;
18. Y.-Q. Lan, S.-L. Li, X.-L. Wang, K.-Z. Shao, Z.-M. Su, E.-B. Wang, Inorg. Chem. 2008, 47, 529-534;
19. Y.-Q. Lan, S.-L. Li, X.-L. Wang, K.-Z. Shao, D.-Y. Du, H.-Y. Zhang, Z.-M. Su, Inorg. Chem. 2008, 47, 8179-8187;
20. J.-P. Wang, H.-Y. Niu, J.-Y. Niu, Inorg. Chem. Commun. 2008, 11, 63-65;
21. Z.-H. Su, B.-B. Zhou, Z.-F. Zhao, X. Zhang, Inorg. Chem. Commun. 2008, 11, 334-337;
22. Y.-H. Chuang, H. Liu, C. J. O'Connor, J. Zubieta, Inorg. Chem. Commun. 2008, 11, 1205-1208;
23. L. Klištinková, E. Rakovský, P. Schwendt, Inorg. Chem. Commun. 2008, 11, 1140-1142;
24. Y. Zhao, W. You, L. Dai, L. Zhang, D. Song, Q. Du, Z. Anorg. Allg. Chem. 2008, 634, 2639-2642;
25. L.-M. Wang, D.-Q. Chu, Mendeleev Commun. 2008, 18, 133-134;
26. H.-J. Pang, C.-J. Zhang, J. Peng, Y.-H.Wang, J.-Q. Sha, A.-X. Tian, P.-P. Zhang, Y. Chen, M. Zhu, Z.-M. Su, Eur. J. Inorg. Chem. 2009, 5175- 5180;
27. H. Jin, B. Zhou, C. Wang, Z. Su, Z. Zhao, Y. Zhang, C. Zhu, Inorg. Chem. Commun. 2009, 12, 76-78;
28. N. G. Armatas, W. Ouellette, J. Pelcher, J. Zubieta, Inorg. Chem. Commun. 2009, 12, 747-749;
29. W. Wang, L. Xu, G. Gao, F. Li, X. Liu, L. Liu, Inorg. Chem. Commun. 2009, 12, 875-878;
30. H.-Y. Zhang, Y.-Q. Lan, Z.-M. Su, G.-S. Yang, G.-J. Xu, D.-Y. Du, L. Chen, L.-K. Yan, Inorg. Chim. Acta 2010, 363, 118-126.
31. T. S. Lobana, R. Sharma, G. Bawa, S. Khanna, Coord. Chem. Rev. 2009, 253, 977-1055.
32. D. X. West, A. E. Liberta, S. B. Padhye, R. C. Chikate, P. B. Sonawane, A. S. Kumbhar, R. G. Yerande, Coord. Chem. Rev. 1993, 123, 49-71.
33. A. G. Bingham, H. Bögge, A. Müller, E. W. Ainscough, A. M. Brodie, J. Chem. Soc., Dalton Trans. 1987, 493-499;
34. C. F. Bell, C. R. Theocharis, Acta Crystallogr., Sect. C 1987, 43, 26-29;
35. E. W. Ainscough, E. N. Baker, A. M. Brodie, R. J. Cresswell, J. D. Ranford, J. M. Waters, Inorg. Chim. Acta 1990, 172, 185-190;
36. E. W. Ainscough, A. M. Brodie, J. D. Ranford, J. M. Waters, J. Chem. Soc., Dalton Trans. 1991, 1737-1742;
37. E. W. Ainscough, A. M. Brodie, J. D. Ranford, J. M. Waters, J. Chem. Soc., Dalton Trans. 1991, 2125-2131;
38. E. W. Ainscough, A. M. Brodie, J. D. Ranford, J. M. Waters, K. S. Murray, Inorg. Chim. Acta 1992, 197, 107-115;
39. J. Garcia- Tojal, M. K. Urtiaga, R. Cortes, L. Lezama, M. I. Arriortua, T. Rojo, J. Chem. Soc., Dalton Trans. 1994, 2233-2238;
40. E. W. Ainscough, A. M. Brodie, J. D. Ranford, J. M. Waters, J. Chem. Soc., Dalton Trans. 1997, 1251-1255;
41. J. García-Tojal, L. Lez ama, J. L. Pizarro, M. Insausti, M. I. Arriortua, T. Rojo, Polyhedron 1999, 18, 3703-3711;
42. D. X. West, J. K. Swearingen, T. J. Romack, I. S. Billeh, J. P. Jasinski, Y. Li, R. J. Staples, J. Mol. Struct. 2001, 570, 129-136;
43. P. Gómez-Saiz, J. García-Tojal, M. A. Maestro, F. J. Arnaiz, T. Rojo, Inorg. Chem. 2002, 41, 1345-1347;
44. P. Gómez-Saiz, J. García-Tojal, A. Mendía, B. Donnadieu, L. Lezama, J. L. Pizarro, M. I. Arriortua, T. Rojo, Eur. J. Inorg. Chem. 2003, 518-527;
45. P. Gómez-Saiz, J. García-Tojal, M. A. Maestro, J. Mahía, L. Lezama, T. Rojo, Eur. J. Inorg. Chem. 2003, 2123-2132;
46. P. Gómez-Saiz, J. García-Tojal, M. A. Maestro, J. Mahía, F. J. Arnaiz, L. Lezama, T. Rojo, Eur. J. Inorg. Chem. 2003, 2639-2650;
47. P. Gómez-Saiz, R. Gil-García, M. A. Maestro, J. L. Pizarro, M. I. Arriortua, L. Lezama, T. Rojo, J. García-Tojal, Eur. J. Inorg. Chem. 2005, 3409-3413;
48. P. Gómez-Saiz, J. García-Tojal, V. Díez- Gómez, R. Gil-García, J. L. Pizarro, M. I. Arriortua, T. Rojo, Inorg. Chem. Commun. 2005, 8, 259-262;
49. P. F. Rapheal, E. Manoj, M. R. P. Kurup, Polyhedron 2007, 26, 818-828;
50. B. García, J. García-Tojal, R. Ruiz, R. Gil-García, S. Ibeas, B. Donnadieu, J. M. Leal, J. Inorg. Biochem. 2008, 102, 1892-1900;
51. P. Gómez-Saiz, R. Gil-García, M. A. Maestro, J. L. Pizarro, M. I. Arriortua, L. Lezama, T. Rojo, M. González-Álvarez, J. Borrás, J. García-Tojal, J. Inorg. Biochem. 2008, 102, 1910-1920.
52. V. Vrdoljak, B. Prugovečki, D. Matković- Čalogović, R. Dreos, P. Siega, C. Tavagnacco, Cryst. Growth Des. 2010, 10, 1373-1382.
53. 2] (acac = acetylacetonate) and HL or HL' ligands in different solvents such as acetone, acetonitrile, ethanol and dichloromethane, controlling other factors like temperature and light incidence.
54. M. K. Urtiaga, M. I. Arriortua, J. Garcia-Tojal, T. Rojo, Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1995, 51, 2172-2174;
55. A. Morsali, A. Ramazani, F. Jamali, F. Gouranlou, Z. Kristallogr. 2001, 216, 607-608.
56. V. N. Byushkin, Y. M. Chumakow, N. M. Samus, Zh. Strukt. Khim. 1987, 28, 140-142;
57. H. Taishang, X. D. Xuebao, Zir. Kex. (Chin.) [J. Xiamen Univ. (Nat. Sci.)] 1993, 32, 741;
58. Z. M. Jin, L. Shen, L. He, H. Guo, H. T. Wang, Acta Crystallogr., Sect. E: Struct. Rep. Online 2003, 59, o1909.
59. pyridinium atoms play an important role allows their positions to be ratified.
60. A. W. Addison, T. N. Rao, J. Reedijk, J. Van Rijn, G. C. Verschoor, J. Chem. Soc., Dalton Trans. 1984, 1349-1356.
61. I. Paulat-Böschen, J. Chem. Soc., Chem. Commun. 1979, 780-782;
62. B. Krebs, S. Stiller, K. H. Tytko, J. Mehmke, Eur. J. Solid State Inorg. Chem. 1991, 28, 883-903;
63. R. Atencio, A. Briceño, X. Galindo, Chem. Commun. 2005, 637-639;
64. K. Eda, Y. Iriki, Chem. Lett. 2005, 34, 612-613;
65. D.-L. Long, C. Streb, P. Kögerler, L. Cronin, J. Cluster Sci. 2006, 17, 257-266.
66. K. Eda, Y. Iriki, K. Kawamura, T. Ikuki, M. Hayashi, J. Solid State Chem. 2007, 180, 3588-3593.
67. D.-D. Liang, S.-X. Liu, C.-L. Wang, Y.-H. Ren, J. Solid State Chem. 2007, 180, 558-563.
68. N. V. Izarova, M. N. Sokolov, D. G. Samsonenko, A. Rothenberger, D. Y. Naumov, D. Fenske, V. P. Fedin, Eur. J. Inorg. Chem. 2005, 4985-4996;
69. N. V. Izarova, M. N. Sokolov, F. M. Dolgushin, M. Y. Antipin, D. Fenske, V. P. Fedin, C. R. Chim. 2005, 8, 1922-1926.
70. J. García-Tojal, T. Rojo, Polyhedron 1999, 18, 1123-1130.
71. D. Hernández, F. Rodríguez, J. García-Jaca, H. Ehrenberg, H. Weitzel, Physica B+C 1999, 265, 181-185;
72. H. Ehrenberg, H. Weitzel, H. Paulus, M. Wiesmann, G. Wltschek, M. Geselle, H. Fuess, J. Phys. Chem. Solids 1997, 58, 153-160.
73. 3J = 8.0 Hz, 1 H, 4-H), 8.16 (br. s, 1 H, N4-H), 8.05 (s, 1 H, 6-H), 7.79 (m, 1 H, 3-H), 7.34 (m, 1 H, 2-H) ppm.
74. 3) ppm.
75. E. Burkholder, V. Golub, C. J. O'Connor, J. Zubieta, Inorg. Chem. Commun. 2004, 7, 363-366;
76. L. San Felices, P. Vitoria, J. M. Gutierrez-Zorrilla, S. Reinoso, J. Etxebarria, L. Lezama, Chem. Eur. J. 2004, 10, 5138-5146;
77. S. Reinoso, P. Vitoria, J. M. Gutiérrez-Zorrilla, L. Lezama, L. San Felices, J. I. Beitia, Inorg. Chem. 2005, 44, 9731-9742;
78. S. Reinoso, P. Vitoria, L. San Felices, L. Lezama, J. M. Gutiérrez-Zorrilla, Inorg. Chem. 2006, 45, 108-118.
79. C.-Z. Lu, C.-D. Wu, H.-H. Zhuang, J.-S. Huang, Chem. Mater. 2002, 14, 2649-2655.
80. B. Bleaney, K. D. Bowers, Proc. R. Soc. London, Ser. A 1952, 214, 451-465.
81. F. E. Anderson, C. J. Duca, J. V. Scudi, J. Am. Chem. Soc. 1951, 73, 4967-4968;
82. D. X. West, D. L. Huffman, J. S. Sa-leda, A. E. Liberta, Transition Met. Chem. 1991, 16, 565-570;
83. F. J. Arnáiz, J. Chem. Educ. 1995, 72, A7-A8.
84. W. G. Klemperer, Inorganic Synthesis, Wiley Interscience, New York, 1990, vol. 27.
85. 4S (230.73): calcd. C 41.7, H 4.9, N 24.3, S 13.9; found C 41.2, H 4.7, N 23.9, S 14.1.
86. R. H. Blessing, Acta Crystallogr., Sect. A 1995, 51, 33-38.
87. G. M. Sheldrick, SHELXS-97, Program for Crystal Structure Solution, University of Göttingen, Göttingen, 1997.
88. G. M. Sheldrick, SHELXL-97, Program for the Refinement of Crystal Structures from Diffraction Data, University of Göttingen, Germany, 1997.
89. L. J. Farrugia, WINGX, A Windows Program for Crystal Structure Analysis, University of Glasgow, Glasgow, 1988.
90. International Tables for Crystallography, Kluwer, Dordrecht, 1992.