Mineralizer effect on the synthesis of two types of one-dimensional chains silver-selenogermanate and selenostannate

Inorganic Chemistry Communications

Volumn 13, Issue 11, 2010, Pages 1296-1298

  Yao, Hua Gang ^a,b   Zhang, Ren Chun ^a   Ji, Shou Hua ^a   Ji, Min ^a   An, Yong Lin ^a   Ning, Gui Ling ^a  

^a DALIAN UNIVERSITY OF TECHNOLOGY   (China)

^b GUANGDONG PHARMACEUTICAL UNIVERSITY   (China)

Author keywords

Mineralizer; Selenidogermanate; Selenidostannate; Solvothermal synthesis

Indexed keywords

EID: 77956927106     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.07.020     Document Type: Article

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28. 3 (0.014 g, 0.10 mmol), about 0.3 mL pyridine (v/v = 1:3) and 0.2 mL triethylamine after 7 days at 170 °C. Yellow square crystals were obtained in 33% yield based on Sn. Compound 4 was obtained with a procedure similar to the synthesis of 3, except that 0.3 mL mixed solvent of thiophenol/pyridine (v/v = 1:3) instead of 0.3 mL of pyridine. Red block crystals were obtained in 68% yields based on silver.
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