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Volumn 9, Issue 9, 2009, Pages 3821-3824

Solvothermal syntheses of two novel layered quaternary silver-antimony(III) sulfides with different strategies

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EID: 70049113880     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg9000335     Document Type: Article
Times cited : (44)

References (39)
  • 26
    • 70049091116 scopus 로고    scopus 로고
    • Note
    • 3 (0.015 g), about 0.2 mL of mixed solvent of glycol/pyridine (v/v = 1:3), and 0.2 mL of ethylenediamine. The mixture was sealed in a Pyrex glass tube with ca. 10% filling at air atmosphere, placed into a stainless-steel autoclave, and then heated at 150 °C for 7 days. After being cooled naturally to ambient temperature, the products were washed with ethanol and water, respectively, and pure yellow needlelike crystals were obtained in 83% yield based on silver.
  • 29
    • 70049117853 scopus 로고    scopus 로고
    • 3 (8.576 g, 0.51 mol) dissolved in acetonitrile was added slowly to a well-stirred solution of thiophenol (6.385 g, 0.59 mol) and triethylamine (6, 177 g, 0.61 mol) in ethanol. The pale-yellow precipitate was filtered, washed with ethanol and diethyl ether, respectively, and vacuum-dried.
    • 3 (8.576 g, 0.51 mol) dissolved in acetonitrile was added slowly to a well-stirred solution of thiophenol (6.385 g, 0.59 mol) and triethylamine (6, 177 g, 0.61 mol) in ethanol. The pale-yellow precipitate was filtered, washed with ethanol and diethyl ether, respectively, and vacuum-dried.
  • 30
    • 70049087075 scopus 로고    scopus 로고
    • -3, R = 0.0262,. RW = 0.0650, reflections used 1286 with I > 2σ(I). Data collection was performed on Bruker Smart APEX II diffraetometer equipped with graphite monochromitized Mo Ka radiation (λ = 0.71073 Å.) at 293 K.
    • -3, R = 0.0262,. RW = 0.0650, reflections used 1286 with I > 2σ(I). Data collection was performed on Bruker Smart APEX II diffraetometer equipped with graphite monochromitized Mo Ka radiation (λ = 0.71073 Å.) at 293 K.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.