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77956905710
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note
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Elemental analysis calc(%): C 14.31, N 2.57, H 2.08, P 7.57, Mo 35.19, Zn 6.00; found(%): C 14.39, N 2.62, H 2.02, P 7.53, Mo 35.12, Zn 6.06.
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77956918765
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note
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Single-crystal X-ray data of compound 1 were collected on a Bruker SMART CCD diffractometer equipped with graphite monochromatized MoKa radiation (λ = 0.71073 Å). Semiempirical absorption corrections were applied using the SADABS program. The structure was solved by direct method and refined by the full-matrix least-squares methods on F2 using the SHELXTL-97 software package. All of the non-hydrogen atoms were refined anisotropically. Hydrogen atoms on carbon atoms and nitrogen atoms were included at calculated positions and refined with a riding model.
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Tian, A.X.6
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