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77949540205
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Elemental analyses calc. (%): H 2.14, C 3.29, N 3.83, O 37.23, P 8.48, Mn 5.64, Mo 39.39. Found: H 2.38, C 3.41, N 3.97, O 37.41, P 8.23, Mn 5.49, Mo 39.11.
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Elemental analyses calc. (%): H 2.14, C 3.29, N 3.83, O 37.23, P 8.48, Mn 5.64, Mo 39.39. Found: H 2.38, C 3.41, N 3.97, O 37.41, P 8.23, Mn 5.49, Mo 39.11.
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32
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77949542431
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2 using the SHELXTL-97 software package. All of the non-hydrogen atoms were refined anisotropically. Hydrogen atoms on carbon atoms and nitrogen atoms were included at calculated positions and refined with a riding model.
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2 using the SHELXTL-97 software package. All of the non-hydrogen atoms were refined anisotropically. Hydrogen atoms on carbon atoms and nitrogen atoms were included at calculated positions and refined with a riding model.
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33
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77949541400
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G.M. Sheldrick, SHELXS-97, Program for X-ray Crystal Structure Solution, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXS-97, Program for X-ray Crystal Structure Solution, University of Göttingen, Germany, 1997.
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34
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77949542335
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G.M. Sheldrick, SHELXL-97, Program for X-ray Crystal Structure Refinement, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXL-97, Program for X-ray Crystal Structure Refinement, University of Göttingen, Germany, 1997.
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