Determination of synthetic phenolic antioxidants and their metabolites in water samples by downscaled solid-phase extraction, silylation and gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 41, 2010, Pages 6428-6435

  Rodil, Rosario ^a   Quintana, José Benito ^a   Basaglia, Giulia ^b   Pietrogrande, Maria Chiara ^b   Cela, Rafael ^a  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

^b UNIVERSITY OF FERRARA   (Italy)

Author keywords

Butylated hydroxyanisole (BHA); Butylated hydroxytoluene (BHT); Derivatisation; Gas chromatography mass spectrometry (GC MS); Phenolic antioxidants; Solid phase extraction (SPE); Water analysis

Indexed keywords

BUTYLATED HYDROXYANISOLE (BHA); BUTYLATED HYDROXYTOLUENE; DERIVATISATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS); PHENOLIC ANTIOXIDANT; SOLID-PHASE EXTRACTION (SPE);

BIOMOLECULES; ESTERS; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLISM; METABOLITES; OLEFINS; ORGANIC SOLVENTS; PHENOLS; SEWAGE; WASTEWATER;

EXTRACTION;

2,6 DI TERT BUTYLCYCLOHEXA 2,5 DIENE 1,4 DIONE; 3,5 DI TERT BUTYL 4 HYDROXYBENZALDEHYDE; 3,5 DI TERT BUTYL 4 HYDROXYBENZOIC ACID; ANTIOXIDANT; BENZALDEHYDE; BUTYLCRESOL; HYDROXYBENZOIC ACID; PHENOL DERIVATIVE; RIVER WATER; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DERIVATIZATION; MASS FRAGMENTOGRAPHY; METABOLITE; PH; PRIORITY JOURNAL; PROCESS DEVELOPMENT; SEWAGE; SILYLATION; SOLID PHASE EXTRACTION; STRUCTURE ANALYSIS; WASTE WATER; WATER ANALYSIS; WATER SAMPLING;

ANTIOXIDANTS; BUTYLATED HYDROXYANISOLE; BUTYLATED HYDROXYTOLUENE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROGEN-ION CONCENTRATION; RIVERS; SENSITIVITY AND SPECIFICITY; SEWAGE; SOLID PHASE EXTRACTION; WATER POLLUTANTS, CHEMICAL; WATER PURIFICATION;

EID: 77956721726     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.08.020     Document Type: Article

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