Validation of the QuEChERS method for the determination of 25 priority pesticide residues in cereal-based baby foods by gas chromatography with electron capture and nitrogen phosphorous detection

Hellenic Plant Protection Journal

Volumn 3, Issue 2, 2010, Pages 71-80

  Anagnostopoulos, C J ^a   Aplada Sarli, P ^a   Miliadis, G E ^a   Haroutounian, C A ^b  

^a BENAKI PHYTOPATHOLOGICAL INSTITUTE   (Greece)

^b AGRICULTURAL UNIVERSITY OF ATHENS   (Greece)

Author keywords

GC ECD; GC NPD; Linearity; Precision; Trueness; Validation

Indexed keywords

EID: 77956719898     PISSN: 17913691     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (17)

1. Anagnostopoulos, C.J. and Miliadis, G.E. 2009. Method validation for the determination of pesticide residues in wheat fl our by gas chromatography. Hellenic Plant Protection Journal, 2: 15-22
2. Anastassiades, M., Lehotay S.J., Stajnbaher, D. and Schenck, F.J. 2003. Fast and Easy Multiresidue Method Employing Acetonitrile Extraction/ Partitioning and "Dispersive Solid-Phase Extraction" for the Determination of Pesticide Residues in Produce. Journal of the Association of Offi cial Analytical Chemists International, 86: 412-431.
3. Anastassiades, M., Tasdelen, B., Scherbaum, E., Stajnbaher, D. 2007. Recent Developments in QuEChERS Methodology for Pesticide Multiresidue Analysis. In: Ohkawa, H. Miyagawa, H. Lee, P.W. 2007. Pesticide chemistry: Crop protection, public health, environmental safety. Wiley-VCH. Weinheim. 538p.
4. European Commission. 2006. Directive 2006/ 141/EC of 22 December 2006 on infant formulae and follow-on formulae. Official Journal of European Communities L401: 1-33.
5. European Commission. 2007. Method validation and Quality control procedures for pesticide residues analysis in food and feed. Document No. SANCO/2007/3131.
6. European Communities. 2009. Foods for Infants & Young Children available in: http://ec.europa.eu/food/food/labellingnutrition/children/index_en.htm (accessed on 14/12/2009).
7. Gil Garcia, M.D., Martinez Vidal, J.L., Martinez Galera, M., Lopez Lopez, T., Almansa Lopez, E. and Cuadros Rodriguez, L. 2003. Correction of the Matrix Eff ect in the Determination of Benzoylphenylurea Insecticides in Vegetables. Journal of Liquid Chromatography & Related Technologies, 26: 297-316.
8. Kim, Dal Ho. 1998. Determination of organophosphorus pesticides in wheat fl our by supercritical fl uid extraction and gas chromatography with nitrogen-phosphorus detection. Journal of Chromatography A, 824: 63-70.
9. Lehotay, S.J., Mastovska, K. and Schenck, F.J. 2003. Abstracts of Papers, 225th ACS National Meeting.
10. Lehotay, S.J. and Mastovska, K. 2004. Abstracts of Papers, 228th ACS National Meeting
11. National Research Council. 1993. Pesticides in the Diets of Infants and Children p. 13-17.
12. Paya, P., Anastassiades, M., Mack, D., Sigalova, I., Tasdelen, B., Jose Oliva, J. and Barba, A. 2007. Analysis of pesticide residues using the Quick Easy Cheap Eff ective Rugged and Safe (QuECh-ERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection. Analytical and Bioanalytical Chemistry, 389: 1697-1714.
13. Steimer, M., Gerbl-Rieger, S., Schaff P. and Parlar, H. 2007. Current situation of the application and identifi cation of pesticides in EU bordering countries with respect to the implementation of a monitoring system. Fresenius Environmental Bulletin, 16: 443-451.
14. Schenck, F.J. and King, V.H. 2002. Determination of organochlorine and organophosphorus pesticide residues in low moisture, non-fatty products using a solid phase extraction cleanup and gas chromatography. Journal of Environmental Science and Health, Part B 35:1-12.
15. Walorczyk, S. 2007. Development of a multi-residue screening method for the determination of pesticides in cereals and dry animal feed using gas chromatography-triple quadrupole tandem mass spectrometry. Journal of Chromatography A 1165: 200-212.
16. Wang, J. and Cheung W. 2006. Determination of Pesticides in Soy-Based Infant Formula Using Liquid Chromatography with Electrospray Ionization Tandem Mass Spectrometry. Journal of AOAC International, 89: 214-224.
17. Working Group "Development and Improvement of Residue-analytical methods". 1996. Analytical Methods for Pesticde Residues in Foodstuff s. 6th Edition Part I: Multiresidue methods. Minstry of Public Health, Welfare and Sport, The Netherlands.