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(or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, U.K.; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk)
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Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-782237-782239. Copies of the data can be obtained free of charge via www.ccdc.cam. ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, U.K.; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).
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Supporting Information is available electronically on the CSJJournal Web site
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Supporting Information is available electronically on the CSJJournal Web site, http://www.csj.jp/joum.als/chem-lett/index.html.
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1HNMR spectrum, because facile isomerization on separation procedures prevented exact isolated yield
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1HNMR spectrum, because facile isomerization on separation procedures prevented exact isolated yield.
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Thermolysis of 6 in the absence of Zn also afforded 7, but in low yield. The role of Zn remains unclear
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Thermolysis of 6 in the absence of Zn also afforded 7, but in low yield. The role of Zn remains unclear.
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