New and unique methods of solid-phase extraction for use before instrumental analysis of xenobiotics in human specimens

Forensic Toxicology

Volumn 28, Issue 2, 2010, Pages 61-68

  Kumazawa, Takeshi ^a   Hasegawa, Chika ^b   Lee, Xiao Pen ^a   Sato, Keizo ^a  

^a SHOWA UNIVERSITY SCHOOL OF MEDICINE   (Japan)

^b TOHO UNIVERSITY SCHOOL OF MEDICINE   (Japan)

Author keywords

Molecularly imprinted polymer; Monolithic silica; Pipette tip; Solid phase extraction; Spin column; Xenobiotic

Indexed keywords

AMPHETAMINE; MOLECULARLY IMPRINTED POLYMER; POLYMER; SILICON DIOXIDE; SORBENT; UNCLASSIFIED DRUG; XENOBIOTIC AGENT;

ANALYTIC METHOD; CENTRIFUGATION; CHEMICAL ANALYSIS; MASS FRAGMENTOGRAPHY; MATERIAL STATE; PIPETTE; PRIORITY JOURNAL; REPRODUCIBILITY; REVIEW; SOLID PHASE EXTRACTION; SURFACE PROPERTY; SYNTHESIS;

EID: 77956095194     PISSN: 18608965     EISSN: 18608973     Source Type: Journal    
DOI: 10.1007/s11419-010-0097-7     Document Type: Review

References (29)

1. M.-C. Hennion 1999 Solid-phase extraction: method development, sorbents, and coupling with liquid chromatography J Chromatogr A 856 3 54 10.1016/S0021-9673(99)00832-8 1:CAS:528:DyaK1MXmt1ent7g%3D 10526783
2. C.W. Huck G.K. Bonn 2000 Recent developments in polymerbased sorbents for solid-phase extraction J Chromatogr A 885 51 72 10.1016/S0021-9673(00)00333-2 1:CAS:528:DC%2BD3cXktlKnu7w%3D 10941667
3. D.T. Rossi N. Zhang 2000 Automating solid-phase extraction: current aspects and future prospects J Chromatogr A 885 97 113 10.1016/S0021-9673(99) 00984-X 1:CAS:528:DC%2BD3cXktlKnu7o%3D 10941669
4. A. Marumo T. Kumazawa X.-P. Lee C. Hasegawa O. Suzuki K. Sato 2008 Utility of disk solid-phase extraction for whole blood samples: analysis of some tetracyclic antidepressants by gas chromatography with nitrogen-phosphorus detection Forensic Toxicol 26 13 18 10.1007/s11419-008-0045-y 1:CAS:528:DC%2BD1cXptFyhsb0%3D
5. J. Wise T. Danielson A. Mozayani R. Li 2008 Analysis of amphetamine, methamphetamine, methylenedioxyamphetamine, and methylenedioxymethamphetamine in whole blood using in-matrix ethyl chloroformate derivatization and automated headspace solid-phase microextraction followed by GC-MS Forensic Toxicol 26 66 70 10.1007/s11419-008-0048-8 1:CAS:528:DC%2BD1MXotFKqtw%3D%3D
6. 9-tetrahydrocannabinol in urine by LCMS- MS after stir-bar sorptive extraction and liquid desorption Forensic Toxicol 28 38 42 10.1007/s11419-009-0081-2 1:CAS:528:DC%2BC3cXhtleit7s%3D
7. S. Miyazaki K. Morisato N. Ishizuka H. Minakuchi Y. Shintani M. Furuno K. Nakanishi 2004 Development of a monolithic silica extraction tip for the analysis of proteins J Chromatogr A 1043 19 25 10.1016/j.chroma.2004.03.025 1:CAS:528:DC%2BD2cXlsVSlu7c%3D 15317408
8. R.N. Xu L. Fan M.J. Rieser T.A. El-Shourbagy 2007 Recent advances in high-throughput quantitative bioanalysis by LC-MS/MS J Pharm Biomed Anal 44 342 355 10.1016/j.jpba.2007.02.006 1:CAS:528:DC%2BD2sXmtlagur0%3D 17360141
9. K.C. Saunders A. Ghanem W. Boon Hon E.F. Hilder P.R. Haddad 2009 Separation and sample pre-treatment in bioanalysis using monolithic phases: a review Anal Chim Acta 652 22 31 10.1016/j.aca.2009.05.043 1:CAS:528: DC%2BD1MXhtF2htbvN 19786168
10. H. Liu J. Stupak J. Zheng B.O. Keller B.J. Brix L. Fliegel L. Li 2004 Open tubular immobilized metal ion affi nity chromatography combined with MALDI MS and MS/MS for identification of protein phosphorylation sites Anal Chem 76 4223 4232 10.1021/ac035231d 1:CAS:528:DC%2BD2cXks1agtrk%3D 15253667
11. C. Hasegawa T. Kumazawa X.-P. Lee M. Fujishiro A. Kuriki A. Marumo H. Seno K. Sato 2006 Simultaneous determination of ten antihistamine drugs in human plasma using pipette tip solid-phase extraction and gas chromatography/mass spectrometry Rapid Commun Mass Spectrom 20 537 543 10.1002/rcm.2335 1:CAS:528:DC%2BD28XhslOnsrs%3D 16419026
12. C. Hasegawa T. Kumazawa X.-P. Lee A. Marumo N. Shinmen H. Seno K. Sato 2007 Pipette tip solid-phase extraction and gas chromatography-mass spectrometry for the determination of methamphetamine and amphetamine in human whole blood Anal Bioanal Chem 389 563 570 10.1007/s00216-007-1460-3 1:CAS:528: DC%2BD2sXpsFSjtLw%3D 17641881
13. T. Kumazawa C. Hasegawa X.-P. Lee A. Marumo N. Shimmen A. Ishii H. Seno K. Sato 2006 Pipette tip solid-phase extraction and gas chromatography-mass spectrometry for the determination of mequitazine in human plasma Talanta 70 474 478 10.1016/j.talanta.2006.02.059 1:CAS:528:DC%2BD28XotlWgtrY%3D 18970795
14. T. Kumazawa C. Hasegawa X.-P. Lee K. Hara H. Seno O. Suzuki K. Sato 2007 Simultaneous determination of methamphetamine and amphetamine in human urine using pipette tip solid-phase extraction and gas chromatography-mass spectrometry J Pharm Biomed Anal 44 602 607 10.1016/j.jpba.2006.12.025 1:CAS:528:DC%2BD2sXmtlans7g%3D 17267160
15. X.-P. Lee C. Hasegawa T. Kumazawa N. Shinmen Y. Shoji H. Seno K. Sato 2008 Determination of tricyclic antidepressants in human plasma using pipette tip solid-phase extraction and gas chromatography-mass spectrometry J Sep Sci 31 2265 2271 10.1002/jssc.200700627 1:CAS:528:DC%2BD1cXptVaqsb8%3D 18546392
16. T. Saito R. Yamamoto S. Inoue I. Kishiyama S. Miyazaki A. Nakamoto M. Nishida A. Namera S. Inokuchi 2008 Simultaneous determination of amitraz and its metabolite in human serum by monolithic silica spin column extraction and liquid chromatography-mass spectrometry J Chromatogr B 867 99 104 10.1016/j.jchromb.2008.03.018 1:CAS:528:DC%2BD1cXls1SnsLY%3D
17. T. Saito S. Morita I. Kishiyama S. Miyazaki A. Nakamoto M. Nishida A. Namera M. Nagao S. Inokuchi 2008 Simultaneous determination of dibucaine and naphazoline in human serum by monolithic silica spin column extraction and liquid chromatography-mass spectrometry J Chromatogr B 872 186 190 10.1016/j.jchromb.2008.07.007 1:CAS:528:DC%2BD1cXhtVensbrO
18. T. Saito T. Yamagiwa I. Kishiyama S. Miyazaki A. Nakamoto M. Nishida A. Namera S. Inokuchi 2009 Monolithic spin column extraction and GC-MS for simultaneously detecting nine cold medication compounds and the drug bromisovaleryl urea in human serum Chromatographia 70 519 526 10.1365/s10337-009-1204-y 1:CAS:528:DC%2BD1MXpvFersLo%3D
19. A. Nakamoto M. Nishida T. Saito I. Kishiyama S. Miyazaki K. Murakami M. Nagao A. Namera 2010 Monolithic silica spin column extraction and simultaneous derivatization of amphetamines and 3,4-methylenedioxyamphetamines in human urine for gas chromatographic-mass spectrometric detection Anal Chim Acta 661 42 46 10.1016/j.aca.2009.12.013 1:CAS:528:DC%2BC3cXhtlKrt7c%3D 20113714
20. O. Ramström K. Mosbach 1999 Synthesis and catalysis by molecularly imprinted materials Curr Opin Chem Biol 3 759 764 10.1016/S1367-5931(99)00037-X 10600723
21. A.G. Mayers M.J. Whitcombe 2005 Synthetic strategies for the generation of molecularly imprinted organic polymers Adv Drug Deliv Rev 57 1742 1778 10.1016/j.addr.2005.07.011
22. L.I. Andersson 2000 Molecular imprinting for drug bioanalysis: a review on the application of imprinted polymers to solidphase extraction and binding assay J Chromatogr B 739 163 173 10.1016/S0378-4347(99)00432-6 1:CAS:528:DC%2BD3cXhsVWrtLY%3D
23. M.W.J. van Hout H.A.G. Niederlander R.A. de Zeeuw G.J. de Jong 2003 Ion suppression in the determination of clenbuterol in urine by solid-phase extraction atmospheric pressure chemical ionization ion-trap mass spectrometry Rapid Commun Mass Spectrom 17 245 250 10.1002/rcm.908 12539191
24. S.G. Wu E.P.C. Lai P.M. Mayer 2004 Molecularly imprinted solid phase extraction-pulsed elution-mass spectrometry for determination of cephalexin and α-aminocephalosporin antibiotics in human serum J Pharm Biomed Anal 36 483 490 10.1016/j.jpba.2003.05.001 1:CAS:528:DC%2BD2cXptFOqurc%3D 15522521
25. N. van Hoof D. Courtheyn J.-P. Antignac M. van de Wiele S. Poelmans H. Noppe H. De Brabander 2005 Multi-residue liquid chromatography/tandem mass spectrometric analysis of beta-agonists in urine using molecular imprinted polymers Rapid Commun Mass Spectrom 19 2801 2808 10.1002/rcm.2126 16145647
26. M. Abdel-Rehim L.I. Andersson Z. Altun L.G. Blomberg 2006 Microextraction in packed syringe online with liquid chromatography-tandem mass spectrometry: molecularly imprinted polymer as packing material for MEPS in selective extraction of ropivacaine from plasma J Liq Chromatogr Relat Technol 29 1725 1736 10.1080/10826070600716843 1:CAS:528:DC%2BD28Xmslaju7c%3D
27. M.M. Ariffin E.I. Miller P.A.G. Cormack R.A. Anderson 2007 Molecularly imprinted solid-phase extraction of diazepam and its metabolites from hair samples Anal Chem 79 256 262 10.1021/ac061062w 1:CAS:528:DC%2BD28Xht1Clu7rJ 17194149
28. N. Harun R.A. Anderson P.A.G. Cormack 2010 Analysis of ketamine and norketamine in hair samples using molecularly imprinted solid-phase extraction (MISPE) and liquid chromatography-tandem mass spectrometry (LC-MS/MS) Anal Bioanal Chem 396 2449 2459 10.1007/s00216-009-3404-6 1:CAS:528: DC%2BC3cXmvFGhtw%3D%3D 20084373
29. Widstrand C, Bergstrand S, Wihlborg A-K (2007) Simple, fast and class selective extraction of amphetamine and related drugs from urine using molecularly imprinted polymer (MIP) SPE and LC/MS/MS. Technical Report, Sigma-Aldrich, http://www.sigmaaldrich.com/etc/medialib/docs/Supelco/General- Information/t407148.Par.0001.File.tmp/t407148.pdf. Cited April 2010