Monolithic silica spin column extraction and simultaneous derivatization of amphetamines and 3,4-methylenedioxyamphetamines in human urine for gas chromatographic-mass spectrometric detection

Analytica Chimica Acta

Volumn 661, Issue 1, 2010, Pages 42-46

  Nakamoto, Akihiro ^a   Nishida, Manami ^b   Saito, Takeshi ^c   Kishiyama, Izumi ^d   Miyazaki, Shota ^d   Murakami, Katsunori ^a   Nagao, Masataka ^e   Namura, Akira ^e  

^a Scientific Investigation Laboratory   (Japan)

^b HIROSHIMA UNIVERSITY   (Japan)

^c TOKAI UNIVERSITY SCHOOL OF MEDICINE   (Japan)

^d GL SCIENCES INC   (Japan)

^e HIROSHIMA UNIVERSITY   (Japan)

Author keywords

3,4 Methylenedioxyamphetamines; Amphetamines; Derivatization; Gas chromatograph mass spectrometer; Monolithic spin column; Propyl chloroformate

Indexed keywords

AMPHETAMINES; CHLOROFORMATES; DERIVATIZATIONS; GAS CHROMATOGRAPHS; SPIN COLUMN;

BODY FLUIDS; CENTRIFUGATION; CENTRIFUGES; CHROMATOGRAPHIC ANALYSIS; COLUMN CHROMATOGRAPHY; DRUG PRODUCTS; MASS SPECTROMETERS; MASS SPECTROMETRY; SIGNAL TO NOISE RATIO; SILICA; SOFTWARE ARCHITECTURE; SPIN DYNAMICS;

GAS CHROMATOGRAPHY;

3,4 METHYLENEDIOXYAMPHETAMINE; 3,4 METHYLENEDIOXYMETHAMPHETAMINE; AMPHETAMINE; METHAMPHETAMINE; SILICON DIOXIDE;

ADSORPTION KINETICS; ARTICLE; CENTRIFUGATION; CHEMICAL ANALYSIS; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; DERIVATIZATION; ELUTION; HUMAN; HUMAN EXPERIMENT; ISOLATION PROCEDURE; LOADING TEST; MASS FRAGMENTOGRAPHY; MONOLITHIC SILICA SPIN COLUMN EXTRACTION; NORMAL HUMAN; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SEPARATION TECHNIQUE; SIGNAL NOISE RATIO; URINALYSIS; URINE LEVEL; VALIDATION PROCESS;

3,4-METHYLENEDIOXYAMPHETAMINE; AMPHETAMINES; ANALYTIC SAMPLE PREPARATION METHODS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; LIMIT OF DETECTION; MOLECULAR STRUCTURE; SILICON DIOXIDE;

EID: 74549127776     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2009.12.013     Document Type: Article

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