Development and validation of a rapid multi-class method for the confirmation of fourteen prohibited medicinal additives in pig and poultry compound feed by liquid chromatography-tandem mass spectrometry

Journal of Pharmaceutical and Biomedical Analysis

Volumn 53, Issue 4, 2010, Pages 929-938

  Cronly, Mark ^a,b   Behan, P ^a   Foley, B ^a   Malone, E ^b   Earley, S ^b   Gallagher, M ^b   Shearan, P ^b   Regan, L ^b  

^a DUBLIN INSTITUTE OF TECHNOLOGY   (Ireland)

^b Backweston Laboratory Complex   (Ireland)

Author keywords

Antibiotics; LC MS MS; Pig and poultry compound feed; Validation

Indexed keywords

ACETONITRILE; ANTIBIOTIC AGENT; AVILAMYCIN; CARBADOX; CHLORAMPHENICOL; CLOPIDOL; DIMETRIDAZOLE; DINITOLIMIDE; ETHOPABATE; HEXANE; IMIDE; IPRONIDAZOLE; METRONIDAZOLE; RONIDAZOLE; SODIUM SULFATE; SULFADIAZINE; SULFADIMIDINE; TYLOSIN; UNCLASSIFIED DRUG; VIRGINIAMYCIN;

ANIMAL FOOD; ARTICLE; CONTROLLED STUDY; ELECTROSPRAY; EVAPORATION; LIQUID CHROMATOGRAPHY; NONHUMAN; POULTRY; PRIORITY JOURNAL; PURIFICATION; QUANTITATIVE ANALYSIS; SWINE; TANDEM MASS SPECTROMETRY; ULTRACENTRIFUGATION; VALIDATION PROCESS;

ANIMAL FEED; ANIMALS; CHROMATOGRAPHY, LIQUID; PHARMACEUTICAL PREPARATIONS; POULTRY; REPRODUCIBILITY OF RESULTS; SWINE; TANDEM MASS SPECTROMETRY;

EID: 77955589399     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2010.06.027     Document Type: Article

References (22)

1. Commission Recommendation 2005/925/EC of 14 December 2005 on the coordinated inspection programme in the field of animal nutrition for the year 2006 in accordance with Council Directive 95/53/EC, Off. J. Eur. Commun. 2005, L337/51.
2. Commission Regulation (EU) No. 37/2010 of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin, Off. J. Eur. Commun. 1990, L15/1.
3. Vincent U., Chedin M., Yasar S., von Holst C. Determination of ionophore coccidiostats in feedingstuffs by liquid chromatography-tandem mass spectrometry. Part I. Application to targeted feed. J. Pharm. Biomed. Anal. 2008, 47:750-757.
4. Galarini R., Fioroni L., Angelucci F., Tovo G.R., Cristofani E. Simultaneous determination of eleven quinolones in animal feed by liquid chromatography with fluorescence and ultraviolet absorbance detection. J. Chromatogr. A 2009, 1216:8158-8164.
5. Pecorelli I., Galarini R., Bibi R., Floridi Al., Casciarri E., Floridi A. Simultaneous determination of 13 quinolones from feeds using accelerated solvent extraction and liquid chromatography. Anal. Chim. Acta 2003, 483:81-89.
6. Barbosa J., Moura S., Barbosa R., Ramos F., Noronha da Silveira M.I. Determination of nitrofurans in animal feeds by liquid chromatography-UV photodiode array detection and liquid chromatography-ionspray tandem mass spectrometry. Anal. Chim. Acta 2007, 586:359-365.
7. van Holthoon F., Mulder P.P.J., van Bennekom E.O., Heskamp H., Zuidema T., van Rhijn H.(J.)A. Quantitative analysis of penicillins in porcine tissues, milk and animal feed using derivatisation with piperidine and stable isotope dilution liquid chromatography tandem mass spectrometry. Anal. Bioanal. Chem. 2010, 396:3027-3040.
8. Capitan-Vallvey L.F., Ariza A., Checa R., Navas N. Liquid chromatography-mass spectrometry determination of six 5-nitroimidazoles in animal feedstuff. Chromatographia 2007, 65:283-290.
9. Vinas P., Balsalobre N., Hernandez-Cordoba M. Determination of chloramphenicol residues in animal feeds by liquid chromatography with photo-diode array detection. Anal. Chim. Acta 2006, 558:11-15.
10. Council Regulation (EC) No. 2821/98 of 17 December 1998 amending, as regards withdrawal of the authorisation of certain antibiotics, Directive 70/524/EEC concerning additives in feedingstuffs, Off. J. Eur. Commun. 1998, L351/4.
11. Van Poucke C., De Keyser K., Baltusnikiene A., McEvoy J.D.G., Van Peteghem C. Liquid chromatographic-tandem mass spectrometric detection of banned antibacterial growth promoters in animal feed. Anal. Chim. Acta 2003, 483:99-109.
12. Van Poucke C., Dumoulin F., Van C., Peteghem Detection of banned antibacterial growth promoters in animal feed by liquid chromatography-tandem mass spectrometry: optimisation of the extraction solvent by experimental design. Anal. Chim. Acta 2005, 529:211-220.
13. Civitareale C., Fiori M., Ballerini A., Brambilla G. Identification and quantification method of spiramycin and tylosin in feedingstuffs with HPLC-UV/DAD at 1ppm level. J. Pharm. Biomed. Anal. 2004, 36:317-325.
14. Dusi G., Faggionato E., Gamba V., Baiguera A. Determination of nicarbazin and clopidol in poultry feeds by liquid chromatography. J. Chromatogr. A 2000, 882:79-84.
15. Tan H.S.I., Ramachandran P., Cacini W. High performance liquid chromatographic assay of amprolium and ethopabate in chicken feed using solid-phase extraction. J. Pharm. Biomed. Anal. 1996, 15:259-265.
16. Kesiunaite G., Naujalisb E., Padarauskasa A. Matrix solid-phase dispersion extraction of carbadox and olaquindox in feed followed by hydrophilic interaction ultra-high-pressure liquid chromatographic analysis. J. Chromatogr. A 2008, 1209:83-87.
17. Hutchinson M.J., Young P.B., Kennedy D.G. Confirmatory method for the analysis of carbadox and olaquindox in porcine feedingstuffs using LC-electrospray MS-MS. Food Addit. Contam. 2005, 22:113-119.
18. J. de Jong, Screening and identification methods for official control of banned antibiotics and growth promoters in feedingstuffs, Final Technical Report (2005) 1-78.
19. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and interpretation of results, Off. J. Eur. Commun. 2002, L221/8.
20. Stubbings G., Bigwood T. The development and validation of a multiclass liquid chromatography tandem mass spectrometry (LC-MS/MS) procedure for the determination of veterinary drug residues in animal tissue using a QuEChERS (QUick, Easy, CHeap, Effective, Rugged and Safe) approach. Anal. Chim. Acta 2009, 637:68-78.
21. McDonald M., Mannion C., Rafter P. A confirmatory method for the simultaneous extraction, separation, identification and quantification of tetracycline, sulfonamide, trimethoprim and dapsone residues in muscle by ultra-high-performance liquid chromatography-tandem mass spectrometry according to Commission Decision 2002/657/EC. J. Chromatogr. A 2009, 1216:8110-8116.
22. Guidelines for the implementation of Decision 2002/657/EC SANCO/2004/2726rev4 (2008) 1-10.