Simultaneous quantification of the organophosphorus pesticides dimethoate and omethoate in porcine plasma and urine by LC-ESI-MS/MS and flow-injection-ESI-MS/MS

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 878, Issue 17-18, 2010, Pages 1234-1245

  Johna, Harald ^a   Eddleston, Michael ^b   Clutton, R Eddie ^c   Worek, Franz ^a   Thiermann, Horst ^a  

^a BUNDESWEHR INSTITUTE OF PHARMACOLOGY AND TOXICOLOGY   (Germany)

^b UNIVERSITY OF EDINBURGH   (United Kingdom)

^c UNIVERSITY OF EDINBURGH   (United Kingdom)

Author keywords

Matrix effects; Organophosphorus compounds; Toxicokinetics

Indexed keywords

ANIMALS; CHROMATOGRAPHIC ANALYSIS; MAMMALS; PESTICIDES; PHOSPHORUS COMPOUNDS;

CHROMATOGRAPHIC METHODS; FLOW INJECTION METHOD; LOWER LIMITS OF DETECTIONS; MATRIX EFFECTS; ORGANOPHOS-PHORUS PESTICIDES; ORGANOPHOSPHORUS COMPOUNDS; ORGANOPHOSPHORUS TOXICANTS; TOXICOKINETICS;

BODY FLUIDS;

DIMETHOATE; OMETHOATE; ORGANOPHOSPHATE PESTICIDE; DRUG DERIVATIVE; INSECTICIDE;

ACCURACY; ANALYTIC METHOD; ANIMAL EXPERIMENT; ANIMAL MODEL; ARTICLE; CALIBRATION; DILUTION; ELECTROSPRAY MASS SPECTROMETRY; FLOW INJECTION ANALYSIS; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; MALE; NONHUMAN; PLASMA; PRECIPITATION; PRIORITY JOURNAL; QUANTITATIVE ASSAY; RELIABILITY; SWINE; TANDEM MASS SPECTROMETRY; URINE LEVEL; VALIDITY; ANIMAL; BLOOD; CHEMISTRY; DRUG STABILITY; METHODOLOGY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; STATISTICAL MODEL; URINE;

ANIMALIA; MAMMALIA; SUS;

ANIMALS; CHROMATOGRAPHY, LIQUID; DIMETHOATE; DRUG STABILITY; FLOW INJECTION ANALYSIS; INSECTICIDES; LINEAR MODELS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SWINE; TANDEM MASS SPECTROMETRY;

EID: 77955491121     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2010.01.003     Document Type: Article

References (50)

1. Hazardous Substances Data Bank (HSDB), United States National Library of Medicine: data for dimethoate: http://toxnet.nlm.nih.gov/cgibin/sis/search/f?/temp/~0s8cSN:1.
2. A.O. Olsson, J.V. Nguyen, M.A. Sadowski, D.B. Barr, Anal. Bioanal. Chem. 376 (2003) 808.
3. F.A. Tarbah, A.M. Shaheen, F.A. Benomran, A.I. Hassan, Th. Daldrup, Forensic Sci. Int. 170 (2007) 129.
4. FAO Specifications and evaluations for agricultural pesticides, dimethoate, Food and Agriculture Organization of The United Nations, 2005: www.fao.org/ag/AGP/AGPP/Pesticid/Specs/docs/Pdf/new/dimethoa.pdf.
5. R.I. Krieger, T. Thongsinthusak, Food Chem. Toxicol. 31 (1993) 177.
6. F.M. Buratti, E. Testai, Toxicology 241 (2007) 33.
7. Hazardous Substances Data Bank (HSDB), United States National Library of Medicine: data for omethoate: http://toxnet.nlm.nih.gov/cgibin/sis/search/f?/temp/~98Mpvb:1.
8. Y. Bai, J. Chen, H. Mu, C. Zhang, B. Li, J. Agric. Food Chem. 57 (2009) 6238.
9. H. John, F. Worek, H. Thiermann, Anal. Bioanal. Chem. 391 (2008) 97.
10. M. Eddleston, P. Eyer, F. Worek, F. Mohammed, L. Senarathna, L. von Meyer, E. Juszczak, A. Hittarage, S. Azher, W. Dissanayake, M.H.R. Sheriff, L. Szinicz, A.H. Dawson, N.A. Buckley, Lancet 366 (2005) 1452.
11. M. Eddleston, F. Mohammed, J.O.J. Davies, P. Eyer, F. Worek, M.H.R. Sheriff, N.A. Buckley, QJM 99 (2006) 513.
12. M. Eddleston, N.A. Buckley, P. Eyer, A.H. Dawson, Lancet 369 (2007) 169.
13. U. Hoffmann, T. Papendorf, Intensive Care Med. 32 (2006) 464.
14. M. Pavlic, A. Haidekker, P. Grubwieser, W. Rabl, Int. J. Legal Med. 116 (2002) 238.
15. R. Regenthal, M. Krueger, H. Trauer, R. Boehm, R. Preiss, Ther. Drug Monit. 24 (2002) 297.
16. M. Eddleston, L. Karalliedde, N. Buckley, R. Fernando, G. Hutchinson, G. Isbister, F. Konradsen, D. Murray, J.C. Piola, N. Senanayake, R. Sheriff, S. Singh, S.B. Siwach, L. Smit, Lancet 360 (2002) 1163.
17. P. Eyer, Toxicol. Rev. 22 (2003) 165.
18. S. Meyer, M. Eddleston, B. Bailey, H. Desel, S. Gottschling, L. Gortner, Klin. Paediatr. 219 (2007) 254.
19. G. Yang, X. Xu, M. Shen, W. Wang, L. Xu, G. Chen, F. Fu, Electrophoresis 30 (2009) 1718.
20. Y. Tao, Y. Wang, L. Ye, H. Li, Q. Wang, Bull. Environ. Contam. Toxicol. 81 (2008) 210.
21. F.A. Tarbah, H. Mahler, O. Temme, T. Daldrup, Forensic Sci. Int. 121 (2001) 126.
22. C. Ferrer, M.J. Gomez, J.F. Garcia-Reyes, I. Ferrer, E.M. Thurman, A.R. Fernandez-Alba, J. Chromatogr. A 1069 (2005) 183.
23. C. Aprea, G. Sciarra, P. Sartorelli, R. Mancini, V. Di Luca, J. Toxicol. Environ. Health A 53 (1998) 263.
24. P. Athanasopoulos, N.B. Kyriakidis, I. Georgitsanakou, J. Agric. Food Chem. 48 (2000) 4896.
25. ChemIDplus Lite, United States National Library of Medicine: data for dimethoate: http://chem.sis.nlm.nih.gov/chemidplus/ProxyServlet?objectHandle=DBMaint&actionHandle=default&nextPage=jsp/chemidheavy/ResultScreen.jsp&ROW_NUM=0&TXTSUPERLISTID=000060515.
26. ChemIDplus Lite, United States National Library of Medicine: data for omethoate: http://chem.sis.nlm.nih.gov/chemidplus/ProxyServlet?objectHandle=DBMaint&actionHandle=default&nextPage=jsp/chemidheavy/ResultScreen.jsp&ROW_NUM=0&TXTSUPERLISTID=001113026.
27. C. Leseur, M. Gartner, A. Mentler, M. Fuerhacker, Int. J. Environ. Anal. Chem. 87 (2007) 1013.
28. D. Perret, A. Gentili, S. Marchese, M. Sergi, G. Dáscenzo, J. AOAC Int. 85 (2002) 724.
29. J. Pan, X.X. Xia, J. Liang, Ultrason. Sonochem. 15 (2008) 25.
30. F. Mazotti, L. Di Donna, B. Macchione, L. Maiuolo, E. Perri, G. Sindona, Rapid Commun. Mass Spectrom. 23 (2009) 1515.
31. B.A. Inglese, R.C.J. van Dam, R.J. Vreeken, H.G.J. Mol, O.M. Steijger, J. Chromatogr. A 918 (2001) 67.
32. M.A. Montesano, A.O. Olsson, P. Kuklenyik, L.L. Needham, A. Bradman, D.B. Barr, J. Expo. Sci. Environ. Epidemiol. 17 (2007) 321.
33. G.F. Pang, Y.Z. Cao, J.J. Zhang, C.L. Fan, Y.M. Liu, X.M. Li, G.Q. Jia, Z.Y. Li, Y.Q. Shi, Y.P. Wu, T.T. Guo, J. Chromatogr. A 1125 (2006) 1.
34. H. John, K.D. Huynh, C. Hedtmann, M. Walden, A. Schulz, F.B. Anspach, W.G. Forssmann, Anal. Biochem. 341 (2005) 173.
35. H. John, Anal. Bioanal. Chem. 381 (2005) 51.
36. M. Eddleston, A. Dawson, L. Karalliedde, W. Dissanayake, A. Hittarage, S. Azher, N.A. Buckley, Crit. Care 8 (2004) R391.
37. P. Eyer, M. Eddleston, H. Thiermann, F. Worek, N.A. Buckley, Brit. J. Clin. Pharmacol. 66 (2008) 451.
38. E.M. Thurman, I. Ferrer, O.J. Pozo, J.V. Sancho, F. Hernandez, Rapid Commun. Mass Spectrom. 21 (2007) 3855.
39. H. John, M. Walden, S. Schäfer, S. Genz, W.G. Forssmann, Anal. Bioanal. Chem. 378 (2004) 883.
40. H. John, W. Schlegel, Chem. Phys. Lipids 99 (1999) 95.
41. F.T. Peters, O.H. Drummer, F. Musshoff, Forensic Sci. Int 165 (2007) 216.
42. Guidance for Industry: Bioanalytical Method Validation, U.S. Department of Health and Human Services, Food and Drug Administration, Center for Drug Evaluation and Research, Center for Veterinary Medicine, May 2001.
43. W.M.A. Niessen, P. Manini, R. Andreoli, Mass Spectrom. Rev. 25 (2006) 881.
44. B.K. Matuszewski, J. Chromatogr. B 830 (2006) 293.
45. Y. Fujikawa, T. Satoh, A. Suganuma, S. Suzuki, Y. Niikura, S. Yui, Y. Yamaura, Hum. Exp. Toxicol. 24 (2005) 333.
46. H. Li, L. Tong, L.M. Schopfer, P. Masson, O. Lockridge, Chem. Biol. Interact. 175 (2008) 68.
47. M.H. Tarhoni, T. Lister, D.E. Ray, W.G. Carter, Biomarkers 13 (2008) 343.
48. H. John, T. Binder, H. Höchstetter, H. Thiermann, Anal. Bioanal.Chem.396(2010) 751.
49. F. Worek, N. Aurbek, N.M. Herkert, H. John, M. Eddleston, P. Eyer, H. Thiermann, Chem. Biol. Interact., doi:10.1016/j.cbi.2009.11.009.
50. J. Martens-Lobenhoffer, E. Schwedhelm, D. Tsikas, J. Chromatogr. B 877 (2009) 3261.