Artifacts related to N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide derivatization of citrulline revealed by gas chromatography-mass spectrometry using both electron and chemical ionization

Journal of Chromatography A

Volumn 1217, Issue 33, 2010, Pages 5444-5448

  Smith, Philip A ^a   Villa, Vilmar ^b   King, Gregory L ^b  

^a Uniformed Services University of the Health Sciences and the Walter Reed National Military Medical Center   (United States)

^b ARMED FORCES RADIOBIOLOGY RESEARCH INSTITUTE   (United States)

Author keywords

Arginine; Artifact; Citrulline; Derivatization; MTBSTFA; Ornithine

Indexed keywords

CHEMICAL IONIZATION; CITRULLINE; DERIVATIZATION OF; DERIVATIZATIONS; ELECTRON IONIZATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; MASS SPECTRA; MTBSTFA; N-ALKANES; POSITIVE CHEMICAL IONIZATIONS; PROGRAMMED TEMPERATURE; RETENTION INDEX; TERT-BUTYLDIMETHYLSILYL; TRIFLUOROACETAMIDES; WATER MOLECULE;

AMINO ACIDS; IONIZATION OF GASES; IONIZATION OF LIQUIDS; MASS SPECTROMETRY; PARAFFINS; PARTICLE DETECTORS;

GAS CHROMATOGRAPHY;

ALKANE DERIVATIVE; CITRULLINE; ISOCYANATE; ORNITHINE; TRIFLUOROACETAMIDE DERIVATIVE; ACETAMIDE DERIVATIVE; ARGININE; FLUOROACETIC ACID; N-METHYL-N-(TERT-BUTYLDIMETHYLSILYL)TRIFLUOROACETAMIDE; ORGANOSILICON DERIVATIVE; TRIFLUOROACETIC ACID;

AMINO ACID ANALYSIS; ARTICLE; ARTIFACT; CONTROLLED STUDY; DERIVATIZATION; IONIZATION; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; CHEMISTRY; PROCEDURES; TEMPERATURE;

ARGININE; ARTIFACTS; CITRULLINE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; ORGANOSILICON COMPOUNDS; ORNITHINE; TEMPERATURE; TRIFLUOROACETIC ACID; ACETAMIDES; FLUOROACETATES;

TETRA;

EID: 77955054085     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.06.043     Document Type: Article

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