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77954213873
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2O twice. The yield was 35% based on Ca.
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43
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77954216884
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-1: 3410 (mb), 2924 (w), 1601 (s), 1470 (s), 1455 (s), 1349 (s), 1236 (w), 1144 (m), 1122 (w), 1037 (w), 844 (w), 757 (m), 688 (w), 594 (w).
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44
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note
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- 1, R1 [I > 2σ(I)] = 0.0603, wR2 (for all data) = 0.1971. The structure was solved by direct methods and refined by full-matrix least-squares fitting on F2 by SHELXL-97.
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