Asymmetrical modification of Wells-Dawson POMs by Cu-phnz coordination polymers

Inorganic Chemistry Communications

Volumn 13, Issue 7, 2010, Pages 840-843

  Sha, Jingquan ^a   Liang, Liye ^a   Yang, Zhiwei ^a   Wang, Cheng ^b   Qu, Youle ^c   Lv, Yuguang ^a  

^a JIAMUSI UNIVERSITY   (China)

^b HEILONGJIANG UNIVERSITY   (China)

^c ZHEJIANG OCEAN UNIVERSITY   (China)

Author keywords

Asymmetrically modification; Electrochemical properties; Hydrothermal synthesis; Wells Dawson polyoxometalate

Indexed keywords

EID: 77954212533     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.04.008     Document Type: Article

References (33)

1. A. Müller, M.T. Pope, F. Peters, and D. Gatteschi Chem. Rev. 98 1998 239
2. V. Artero, A. Proust, P. Herson, F. Villain, C. Moulin, and P. Gouzerh J. Am. Chem. Soc. 125 2003 11156
3. E. Coronado, J.R. Galán-Mascarós, C. Giménez-Saiz, C.J. Gómez-García, E. Martínez-Ferrero, M. Almeida, and E.B. Lopes Adv. Mater. 16 2004 324
4. P. Kögerler, and L. Cronin Angew. Chem. Int. Ed. Engl. 44 2005 844
5. D.L. Long, H. Abbas, P. Kögerler, and L. Cronin Angew. Chem. Int. Ed. 44 2005 3415
6. D. Velessiotis, N. Glezos, and V. Ioannou-Sougleridis J. Appl. Phys. 2005 98
7. H.X. Jin, Q.Y. Wu, and W.Q. Pang J. Hazard. Mater. 141 2007 123
8. L. Lisnard, P. Mialane, A. Dolbecq, J. Marrot, J.M. Clemente-Juan, E. Coronado, B. Keita, P. Oliveira, L. Nadjo, and F. Secheresse Chem. Eur. J. 13 2007 3525
9. Q. Li, Y.G. Wei, J. Hao, Y.L. Zhu, and L.S. Wang J. Am. Chem. Soc. 129 2007 5810
10. J. Lehmann, A. Galta-arino, E. Coronado, and D. Loss Nat. Nanotechnol. 2 2007 312
11. C. Boglio, K. Micoine, T. Derat, R. Thouvenot, B. Hasenknopf, S. Thorimbert, E. Lacte, and M. Malacria J. Am. Chem. Soc. 130 2008 4553
12. G.G. Gao, F.Y. Li, L. Xu, X.Z. Liu, and Y.Y. Yang J. Am. Chem. Soc. 130 2008 10838
13. J. Zhang, Y.F. Song, L. Cronin, and T.B. Liu J. Am. Chem. Soc. 130 2008 14408
14. G.G. Gao, L. Xu, X.S. Qu, H. Liu, and Y.Y. Yang Inorg. Chem. 47 2008 3402
15. C.Y. Sun, S.X. Liu, D.D. Liang, K.Z. Shao, Y.H. Ren, and Z.M. Su J. Am. Chem. Soc. 131 2009 1883
16. J. Kang, B.B. Xu, Z.H. Peng, X.D. Zhu, Y.G. Wei, and D.R. Powell Angew. Chem. Int. Ed. 44 2005 6902
17. H. Yasuda, L.N. He, T. Sakakura, and C.W. Hu J. Catal. 233 2005 119
18. Z. Xian-Ming, T. Ming-Liang, and C. Xiao-Ming Chem. Commun. 2000 1817
19. P.J. Hagrman, D. Hagrman, and J. Zubieta Angew. Chem. Int. Ed. 38 1999 2638
20. S. Masahiro, M.H. Dickman, and M.T. Pope Angew. Chem. Int. Ed. 39 2000 2914
21. H.Y. An, D.R. Xiao, E.B. Wang, Y.G. Li, Z.M. Su, and L. Xu Angew. Chem. Int. Ed. 45 2006 904
22. Y.P. Ren, X.J. Kong, L.S. Long, R.B. Huang, and L.S. Zheng Cryst. Growth Des. 6 2006 572
23. J.P. Wang, P.T. Ma, and J.Y. Niu Inorg. Chem. Commun. 9 2006 1049
24. J.Q. Sha, J. Peng, H.S. Liu, J. Chen, A.X. Tian, and P.P. Zhang Inorg. Chem. 46 2007 11183
25. J.Q. Sha, J. Peng, Y.Q. Lan, Z.M. Su, H.J. Pang, A.X. Tian, P.P. Zhang, and M. Zhu Inorg. Chem. 47 2008 5145
26. J.Q. Sha, J. Peng, A.X. Tian, H.S. Liu, J. Chen, P.P. Zhang, and Z.M. Su Cryst. Growth Des. 7 2007 2535
27. J.Q. Sha, C. Wang, J. Peng, J. Chen, A.X. Tian, and P.P. Zhang Inorg. Chem. Commun. 10 2007 1321
28. J.Q. Sha, J. Peng, H.S. Liu, J. Chen, B.X. Dong, A.X. Tian, and Z.M. Su Eur. J. Inorg. Chem. 2007 1268 1274
29. C. Ritchie, E. Burkholder, P. Kögerler, and L. Cronin Dalton Trans. 2006 1712
30. 2O was neutralized to 3.5-4 with 1 M HCl solution, then kept at 170 ° for 6 days and harvested the red block crystals of 1 (34% yield based on Cu). Elemental analysis found: C18.14, H 1.36, N 3.50, Cu 4.31 (%). Calc. for compound 1, C90 H62 Cu4 N15 O62 P2 W18 (5970.75): C18.09, H 1.04, N 3.52, Cu 4.29 (%).
31. 2. All calculations were performed using the SHELXL-97 program package. Absorption effects were empirically collected. All atoms except hydrogen atoms were refined anisotropically.
32. I.D. Brown, and D. Altermatt Acta Crystallogy. Sect. B 41 1985 244
33. Cyclic voltammograms were obtained with a CHI 660 electrochemical workstation at room temperature. Platinum gauze was used as counter electrode and Ag/AgCl electrode was referenced. A chemically bulk-modified carbon paste electrode (CPE) was used as working electrode, which was prepared as the following: 48 mg of graphite powder and 8 mg of the title compound was mixed and ground together by agate mortar and pestle to achieve a uniform mixture, and then it was added 0.6 mL nujol with stirring. The homogenized mixture was packed into a glass tube with 1.2 mm inner diameter, and the tube surface was wiped with paper. Electrical contact was established with copper rod through the back of the electrode.