Trace headspace sampling for quantitative analysis of explosives with cryoadsorption on short alumina porous layer open tubular columns

Analytical Chemistry

Volumn 82, Issue 13, 2010, Pages 5621-5627

  Lovestead, Tara M ^a   Bruno, Thomas J ^a  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CRYO-ADSORPTION; DETECTION OF EXPLOSIVES; ENERGETIC MATERIAL; EXPLOSIVE DETECTION; HEADSPACE SAMPLING; HEADSPACES; LINEAR RELATIONSHIPS; PLASTIC BONDED EXPLOSIVES; POROUS LAYER OPEN TUBULAR COLUMN; POROUS LAYERS; PREDICTIVE CAPABILITIES; PURGE AND TRAP; QUANTITATIVE ANALYSIS; TRACE COMPOUNDS; VAN'T HOFF EQUATION;

EXPLOSIVES; NITRATION; TRACE ANALYSIS; TUBULAR STEEL STRUCTURES;

EXPLOSIVES DETECTION;

EID: 77954199846     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac1005926     Document Type: Article

References (59)

1. Yinon, J. and Zitrin, S. Modern Methods and Applications in Analysis of Explosives; John Wiley & Sons Ltd.: West Sussex, 1993.
2. Linstrom, P. J. and Mallard, W. G. NIST Chemistry WebBook, NIST Standard Reference Database Number 69; National Institute of Standards and Technology: Gaithersburg, MD; http://webbook.nist.gov; June 2005.
3. Rowley, R. L., Wilding, W. V., Oscarson, J. L., Zundel, N. A., Marshall, T. L., Daubert, T. E., and Danner, R. P. DIPPR(R) Data Compilation of Pure Compound Properties; Design Institute for Physical Properties, A.: New York, Sept 2008.
4. Frenkel, M., Chirico, R. D., Diky, V. V., Muzny, C., Kazakov, A. F., and Lemmon, E. W. NIST ThermoData Engine, NIST Standard Reference Database 103b-Pure Compounds and Binary Mixtures, Version 3.0; National Institute of Standards and Technology, Standard Reference Data Program: Gaithersburg, MD, 2005.
5. Yinon, J. Counterterrorist Detection Techniques of Explosives; Elsevier B.V.: Amsterdam, 2007.
6. Widegren, J. and Bruno, T. J. J. Chem. Eng. Data 2010, 55, 159-164
7. Perr, J. M., Furton, K. G., and Almirall, J. R. J. Sep. Sci. 2005, 28, 177-183
8. Certain commercial equipment, instruments, or materials are identified in this paper in order to specify adequately the experimental procedure. Such identification does not imply recommendation or endorsement by the National Institute of Standards and Technologies, nor does it imply that the materials or equipment identified are necessarily the best available for the purpose
9. Existing and Potential Standoff Explosives Detection Techniques; The National Academies Press: Washington, DC, 2004.
10. Conder, J. M., La Point, T. W., Lotufo, G. R., and Steevens, J. A. Environ. Sci. Technol. 2003, 37, 1625-1632
11. Halasz, A., Groom, C., Zhou, E., Paquet, L., Beaulieu, C., Deschamps, S., Corriveau, A., Thiboutot, S., Ampleman, G., Dubois, C., and Hawari, J. J. Chromatogr., A 2002, 963, 411-418
12. Harper, R. J., Almirall, J. R., and Furton, K. G. Talanta 2005, 67, 313-327
13. Hodyss, R. and Beauchamp, J. L. Anal. Chem. 2005, 77, 3607-3610
14. Wu, Z. C. and Fung, Y. S. Int. J. Environ. Anal. Chem. 2002, 82, 431-442
15. Moore, D. Rev. Sci. Instrum. 2004, 75, 2499-2512
16. Schulte-Ladbeck, R. and Karst, U. Anal. Chim. Acta 2003, 482, 183-188
17. Teranish, R., Robinson, A. B., Cary, P., Mon, T. R., and Pauling, L. Anal. Chem. 1972, 44, 18
18. Cumming, C. J., Aker, C., Fisher, M., Fox, M., la Grone, M. J., Reust, D., Rockley, M. G., Swager, T. M., Towers, E., and Williams, V. IEEE Trans. Geosci. Remote Sensing 2001, 39, 1119-1128
19. Fisher, M., Sikes, J., and Schultz, K. J. Mine Action 2003, (7.3), http://maic.jmu.edu/journal/7.3/focus/fisher/fisher.htm.
20. Trace Explosives Detection Meeting; National Institute of Standards and Technology: Gaithersburg, MD, Feb 2008.
21. Macias, M. S., Guerra-Diaz, P., Almirall, J. R., and Furton, K. G. Forensic Sci. Int. 2010, 195, 132-138
22. Macias, M. S., Harper, R. J., and Furton, K. G. Am. Lab. 2008, 40, 16
23. Pawliszyn, J. Solid Phase Microextraction: Theory and Practice; Wiley-VCH: New York, 1997.
24. Wercinski, S. Solid Phase Microextraction: A Practical Guide; CRC Press: Boca Raton, FL, 1999.
25. Bruno, T. J. J. Chromatogr. Sci. 2009, 47, 569-574
26. Boswell, C. E. WTQA-99-15th Annu. Waste Test. Qual. Assur. Symp. Proc. 1999, 190-194
27. Helmig, D. J. Chromatogr., A 1999, 843, 129-146
28. Ioffe, B. V., Vittenburg, A. G., and Manatov, I. A. Head-Space Analysis and Related Methods in Gas Chromatography; Wiley-Interscience, New York, 1984.
29. Namiesnik, J. and Zygmut, B. Chromatographia Suppl. 2002, 56, S9-S18
30. Preito, M. J., Berenguer, D., Marhuenda, D., and Cardone, A. J. Chromatogr., B 2000, 741, 301-306
31. Bruno, T. J. J. Chromatogr. Sci. 1994, 32, 112-115
32. Bruno, T. J., Lewandowska, A., Tsvetkov, F., Miller, K. E., and Hanley, H. J. M. J. Chromatogr., A 2002, 973, 143-149
33. Miller, K. E. and Bruno, T. J. J. Chromatogr., A 2004, 1042, 49-54
34. Furton, K. G., Harper, R. J., Perr, J. M., and Almirall, J. R. Proc. SPIE 2003, 5071, 183-192
35. Lai, H., Leung, A., Magee, M., and Almirall, J. R. Anal. Bioanal. Chem. 2010, 396, 2997-3007
36. Sanchez, C., Carlsson, H., Colmsjo, A., Crescenzi, C., and Batlle, R. Anal. Chem. 2003, 75, 4639-4645
37. Batlle, R., Carlsson, H., Tollback, P., Colmsjo, A., and Crescenzi, C. Anal. Chem. 2003, 75, 3137-3144
38. Batlle, R., Carlsson, H., Holmgren, E., Colmsjo, A., and Crescenzi, C. J. Chromatogr., A 2002, 963, 73-82
39. Sigman, M. E., Ma, C.-Y., and Ilgner, R. H. Anal. Chem. 2001, 73, 792-798
40. Bruno, T. J. and Svoronos, P. D. N. CRC Handbook of Fundamental Spectroscopic Correlation Charts; Taylor and Francis CRC Press: Boca Raton, FL, 2005.
41. NIST/EPA/NIH Mass Spectral Database, S. R. D.; SRD Program; National Institute of Standards and Technology: Gaithersburg, MD, 2005.
42. Lovestead, T. M. and Bruno, T. J. Food Chem. 2010, 121, 1274-1282
43. Lovestead, T. M. and Bruno, T. J. J. Forensic Sci. Int. 2010, doi: 10.1016/j.forsciint.2010.05.024.
44. Bruno, T. J. and Svoronos, P. D. N. CRC Handbook of Basic Tables for Chemical Analysis, 2nd ed.; CRC Press: Boca Raton, 2003.
45. Bruno, T. J. Ind. Eng. Chem. Res. 2006, 45, 4371-4380
46. Bruno, T. J. Anal. Chem. 1986, 58, 1595-1596
47. Karasek, F. W. and Clement, R. E. Basic Gas Chromatography-Mass Spectrometry: Principles and Techniques; Elsevier: Amsterdam, 1988.
48. Ribbands Explosives, England, MSDS for Semtex RX-1A, Semtex RX-1H, and Semtex RX-10SE.
49. Kim, D.-Y. and Kim, K.-J. J. Chem. Eng. Data 2007, 52, 1946-1949
50. Chen, F., Duo, Y. Q., Luo, S. G., Luo, Y. J., and Tan, H. M. Propellants, Explos., Pyrotech. 2003, 28, 7-11
51. Min, B. Propellants, Explos., Pyrotech. 2008, 33, 131-138
52. Lorenzo, N., Wan, T., Harper, R., Hsu, Y.-L., Chow, M., Rose, S., and Furton, K. Anal. Bioanal. Chem. 2003, 376, 1212, and refs. within
53. Report ND05o610/01; Screening of plastic toys for chemical composition and hazards-Market surveillance in the Netherlands; Food and Safety Authority (VWA): Netherlands, 2005.
54. Diethyl phthalate, Environ. Writer, 2006; http://www.environmentwriter. org/resources/backissues/chemicals/diethyl-phthalate.htm; Access Date: Dec, 2008.
55. Widegren, J. A. and Bruno, T. J. Environ. Sci. Technol. 2010, 44, 388-393
56. Bruno, T. J. and Mayrath, J. E. Rev. Sci. Instrum. 1997, 68, 2864-2870
57. Jones, D. E. G., Lightfoot, P. D., Fouchard, R. C., and Kwok, Q. S. M. Thermochim. Acta 2002, 388, 159-173
58. Elias, L. Montreal, Canada, AH-DE/5-WP/17 International Civil Aviation Organization (Sept. 23-27, 1991).
59. Deline, J. Personal communication, Department of Homeland Security-Transportation Security Laboratory, 2009.