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21
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77953871476
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-
3ClNi (%): C, 68.90; H, 5.06; N, 11.48. Found: C, 68.82; H, 5.02; N, 11.52.
-
3ClNi (%): C, 68.90; H, 5.06; N, 11.48. Found: C, 68.82; H, 5.02; N, 11.52.
-
-
-
-
22
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33748323483
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Dobrzańska L., Lloyd G.-O., Jacobs T., Rootman I., Oliver C.-L., Bredenkamp M.-W., and Barbour L.-J. J. Mol. Struct. 796 (2006) 107
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Barbour, L.-J.7
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23
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77953870002
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-
Crystallographic data for 1 (C56H49N8O3ClNi, Mr, 976.19, space group P4/nnc, a, 15.703(7) Å, b, 15.703(7) Å, c, 20.4699(9) Å, V, 5047.4(3) Å3, Z, 4, ρ, 1.285 g cm- 3, μ, 0.490 mm- 1, T, 293(2)K, reflections collected: 3165, independent reflections: 2421, S, 1.063, R1, 0.0456, wR2, 0.1422
-
- 1, T = 293(2)K, reflections collected: 3165, independent reflections: 2421, S = 1.063, R1 = 0.0456, wR2 = 0.1422.
-
-
-
-
24
-
-
77953870368
-
-
3ClCu (%): C, 68.56; H, 5.03; N, 11.42. Found: C, 68.52; H, 5.06; N, 11.37.
-
3ClCu (%): C, 68.56; H, 5.03; N, 11.42. Found: C, 68.52; H, 5.06; N, 11.37.
-
-
-
-
25
-
-
77953871719
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-
Crystallographic data for 2 (C56H49N8O3ClCu, Mr, 981.0, space group P4/nnc, a, 15.7078(14) Å, b, 15.7078(14) Å, c, 20.465(3) Å, V, 5049.4(10) Å3, Z, 4, ρ, 1.290 g cm- 3, μ, 0.538 mm- 1, T, 293(2) K, reflections collected: 2239, independent reflections:1176, S, 0.990, R1, 0.0638, wR2, 0.1611
-
- 1, T = 293(2) K, reflections collected: 2239, independent reflections:1176, S = 0.990, R1 = 0.0638, wR2 = 0.1611.
-
-
-
-
26
-
-
77953869792
-
-
oC to remove solvent molecules (%): C, 64.91; H, 4.65; N, 9.89.
-
oC to remove solvent molecules (%): C, 64.91; H, 4.65; N, 9.89.
-
-
-
-
27
-
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77953872583
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-
Crystallographic data for 3 (C95H94N12O13Cd2, Mr, 1834.61, space group Pī, a, 14.8147(17)Å, b, 17.055(2)Å, c, 21.370(3)Å, V, 4831.4(10) Å3, Z, 2, ρ, 1.261 g cm- 3, μ, 0.504 mm- 1, T, 293(2) K, reflections collected: 21318, independent reflections: 12306, S, 1.056, R1, 0.0709, wR2, 0.2103
-
- 1, T = 293(2) K, reflections collected: 21318, independent reflections: 12306, S = 1.056, R1 = 0.0709, wR2 = 0.2103.
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-
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28
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33846018090
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