Validation of an analytical method for analysis of cannabinoids in hair by headspace solid-phase microextraction and gas chromatography-ion trap tandem mass spectrometry

Analytica Chimica Acta

Volumn 670, Issue 1-2, 2010, Pages 63-71

  Emídio, Elissandro Soares ^a   de Menezes Prata, Vanessa ^a   Dórea, Haroldo Silveira ^a  

^a FEDERAL UNIVERSITY OF SERGIPE   (Brazil)

Author keywords

Cannabinoids; Gas chromatography ion trap tandem mass spectrometry; Hair analysis; Headspace solid phase microextraction

Indexed keywords

ALKALINE SOLUTIONS; ANALYTICAL METHOD; CANNABINOIDS; CANNABINOL; CUT-OFF VALUE; DESORPTION TIME; EXTRACTION TEMPERATURES; EXTRACTION TIME; FIBER TYPES; GC-MS/MS; HAIR ANALYSIS; HEAD-SPACE SOLID-PHASE MICROEXTRACTION; HUMAN HAIR; ION TRAP TANDEM MASS SPECTROMETRY; LIMITS OF DETECTION; LINEAR RANGE; LOWER LIMITS; PETROLEUM ETHER; REGRESSION COEFFICIENT;

DEIONIZED WATER; DESORPTION; DICHLOROMETHANE; ETHERS; GAS CHROMATOGRAPHY; ION CHROMATOGRAPHY; IONIC STRENGTH; IONIZATION OF LIQUIDS; MASS SPECTROMETRY; OPTIMIZATION;

EXTRACTION;

CANNABIDIOL; CANNABINOID; CANNABINOL; DICHLOROMETHANE; DRONABINOL; PETROLEUM ETHER; WATER;

ACCURACY; ADULT; ALKALINITY; ANALYTIC METHOD; ARTICLE; CANNABIS ADDICTION; CHEMICAL STRUCTURE; CLINICAL ARTICLE; CONTROLLED STUDY; DESORPTION; EXTRACTION; GAS CHROMATOGRAPHY; HAIR ANALYSIS; HUMAN; ION TRAP MASS SPECTROMETRY; IONIC STRENGTH; MALE; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; QUANTITATIVE ANALYSIS; REFERENCE VALUE; SOLID PHASE MICROEXTRACTION; TANDEM MASS SPECTROMETRY; TEMPERATURE; ULTRASOUND; VALIDATION STUDY;

CANNABIDIOL; CANNABINOL; CHROMATOGRAPHY, GAS; HAIR; HUMANS; MALE; SENSITIVITY AND SPECIFICITY; SOLID PHASE MICROEXTRACTION; TANDEM MASS SPECTROMETRY; TETRAHYDROCANNABINOL; YOUNG ADULT;

CANNABIS;

EID: 77953808569     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2010.04.023     Document Type: Article

References (45)

1. Gambaroa V., Dell'Acqua L., Farè F., Froldi R., Saligari E., Tassoni G. Anal. Chim. Acta 2002, 468:245.
2. Huestis M.A. Principles of Forensic Toxicology 2003, 229. AACC Press, Washington. second ed. B. Levine (Ed.).
3. Baptista M.J., Monsantoa P.V., Marques E.G.P., Bermejo A., Ávila S., Castanheira A.M., Margalho C., Barroso M., Vieira D.N. Forensic Sci. Int. 2002, 128:66.
4. Carlini E.A. J. Bras. Psiquiatr. 2006, 55:317.
5. Pélissier A.L. Thérapie 1997, 52:213.
6. Astley S.J., Little R.E. Neurotoxicol. Teratol. 1990, 12:161.
7. Manolis A., McBurney L.J., Bobbie B.A. Clin. Biochem. 1983, 16:229.
8. Huestis M.A., Cone E.J.J. Anal. Toxicol. 2004, 28:394.
9. Huestis M.A., Scheidweiler K.B., Saito T., Fortner N., Abraham T., Gustafson R.A., Smith M.L. Forensic Sci. Int. 2008, 174:173.
10. Lemos N.P., Anderson R.A., Robertson J.R. J. Anal. Toxicol. 1999, 23:147.
11. Sachs H., Dressler U. Forensic Sci. Int. 2000, 107:239.
12. Nakahara Y. J. Chromatogr. B 1999, 733:162.
13. Pragst F., Balikova M.A. Clin. Chim. Acta 2006, 370:18.
14. Gallardo E., Queiroz J.A. Biomed. Chromatogr. 2008, 22:795.
15. Kintz P. Ther. Drug Monit. 1996, 18:450.
16. Henderson G.L. Forensic Sci. Int. 1993, 63:19.
17. Auwärter V., Wohlfarth A., Traber J., Thieme D., Weinmann W. Forensic Sci. Int. 2010, 196:10.
18. Cirimele V., Kintz P., Mangin P. Forensic Sci. Int. 1995, 70:175.
19. Cirimele V., Sachs H., Kintz P., Mangin P. J. Anal. Toxicol. 1996, 20:13.
20. Skopp G., Strohbeck-Kuehner P., Mann K., Hermann D. Forensic Sci. Int. 2007, 170:46.
21. Koide I., Noguchi O., Okada K., Yokoyama A., Oda H., Yamamoto S., Kataoka H. J. Chromatogr. B 1998, 707:99.
22. Musshoff F., Madea B. Forensic Sci. Int. 2007, 165:208.
23. Arthur C.L., Pawliszyn J. Anal. Chem. 1990, 62:2145.
24. Gaujac A., Emídio E.S., Navickiene S., Ferreira S.L.C., Dórea H.S. J. Chromatogr. A 2008, 1203:99.
25. Nadulski T., Pragst F. J. Chromatogr. B 2007, 846:78.
26. Ulrich S. J. Chromatogr. A 2000, 902:186.
27. United States National Library of Medicine, http://toxnet.nlm.nih.gov/cgi%20bin/sis/htmlgen%3FCHEM.
28. Kanazawa J. Environ. Toxicol. Chem. 1989, 8:477.
29. Lord H., Pawliszyn J. J. Chromatogr. A 2000, 885:173.
30. Mester Z., Sturgeona R., Pawliszyn J. Spectrochim. Acta B 2001, 56:242.
31. Uhl M. Analytical and Practical Aspects of Drug Testing in Hair 2006, 128. CRC Press, Boca Raton. first ed. P. Kintz (Ed.).
32. Musshoff F., Junker H.P., Lachenmeier D.W., Kroener L., Madea B. J. Anal. Toxicol. 2002, 26:554.
33. Lee M.R., Yeh Y.C., Hsiang W.S., Chen C.C. J. Chromatogr. B 1997, 707:91.
34. Harkey M.R. Forensic Sci. Int. 1993, 63:9.
35. Gorecki T., Pawliszyn J. Anal. Chem. 1995, 67:3265.
36. Peters F.T., Hartung M., Herbold M., Schmitt G., Daldrup T., Musshoff F. Toxichem. Krimtech. 2004, 71:146.
37. Sporkert F., Pragst F. Forensic Sci. Int. 2000, 107:129.
38. Musshoff F., Lachenmeier D.W., Kroener L., Madea B. Forensic Sci. Int. 2003, 133:32.
39. Nishida M., Yashiki M., Namera A., Kimura K. J. Chromatogr. B 2006, 842:110.
40. Society of hair testing. Forensic Sci. Int. 1997, 84:3.
41. Society of hair testing. Forensic Sci. Int. 2004, 145:83.
42. Pragst F., Nadulski T. Ann. Toxicol. Anal. 2005, 17:237.
43. Wicks J., Tsanaclis L.M.T. Ann. Toxicol. Anal. 2005, 17:120.
44. de Oliveira C.D.R., Yonamine M., Moreau R.L.M. J. Sep. Sci. 2007, 30:133.
45. Strano-Rossi S., Chiarotti M. J. Anal. Toxicol. 1999, 23:7.