The coordinated use of synchrotron spectroelectrochemistry for corrosion studies on heritage metals

Accounts of Chemical Research

Volumn 43, Issue 6, 2010, Pages 927-935

  Adriaens, Annemie ^a   Dowsett, Mark ^b  

^a GHENT UNIVERSITY   (Belgium)

^b UNIVERSITY OF WARWICK   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 77953676640     PISSN: 00014842     EISSN: 15204898     Source Type: Journal    
DOI: 10.1021/ar900269f     Document Type: Article

References (29)

1. Lahanier, Ch.; Amsel, G.; Heitz, Ch.; Menu, M.; Andersen, H. H. Nucl. Instrum. Methods Phys. Res., Sect. B 1986, 14 (1 entire issue
2. Dran, J. C.; Salomon, J.; Calligaro, T.; Walter, Ph. Ion Beam Analysis of Art Works: 14 Years of Use in the Louvre Nucl. Instrum. Methods Phys. Res., Sect. B B 2004, 219-220, 7-15
3. Andersen, H. H.; Demortier, G. Nucl. Instrum. Methods Phys. Res., Sect. B 2004, 226 (1-2 entire issue
4. Smit, Z. Nucl. Instrum. Methods Phys. Res., Sect. B 2005, 239 (1-2 entire issue (Archaeometry with IBA and Related Methods-Proceedings of the Workshop of the COST G8 Action "Non-destructive Analysis and Testing of Museum Objects", held in conjunction with the "10th International Conference on PIXE and its Analytical Applications")
5. Respaldiza, M. A.; Gómez-Camacho, J., Eds. Applications of Ion Beam Analysis Techniques to Arts and Archaeometry; Secretariado de Publicaciones de la Universidad de Sevilla: Seville, 1997.
6. Demortier, G.; Adriaens, A., Eds. Ion Beam Study of Art and Archaeological Objects (EUR 19218); Office for Official Publications of the European Communities: Luxembourg, 2000.
7. http://www.eu-artech.org.
8. Harbottle, G.; Gordon, B. M.; Jones, K. W. Use of Synchrotron Radiation in Archaeometry Nucl. Instrum. Methods Phys. Res., Sect. B 1986, 14 (1) 116-122
9. http://srs.dl.ac.uk.
10. Bertrand, L.; Vantelon, D.; Pantos, E. Novel Interface for Cultural Heritage at SOLEIL Appl. Phys. A: Mater. Sci. Process. 2006, 83, 225-228
11. Lehmann, E. H.; Vontobel, P.; Deschler-Erb, E.; Soares, M. Non-invasive Studies of Objects from Cultural Heritage Nucl. Instrum. Methods Phys. Res., Sect. A 2005, 542, 68-75
12. Oddy, W. A.; Hughes, M. J. The Stabilization of Active Bronze and Iron Antiquities by the Use of Sodium Sesquicarbonate Stud. Conserv. 1970, 15, 183-189
13. MacLeod, I. D. Conservation of Corroded Copper Alloys: A Comparison of New and Traditional Methods for removing Chloride Ions Stud. Conserv. 1987, 32, 25-40
14. Pollard, A. M.; Thomas, R. G.; Williams, P. A. Mineralogical Changes Arising from the Aqueous Sodium Carbonate Solutions for the Treatment of Archaeological Copper Objects Stud. Conserv. 1990, 35, 148-152
15. Hughes, R.; Rowe, M. The Colouring, Bronzing and Patination of Metals; Thames and Hudson Ltd.: London, 2006.
16. Scott, D. A. Copper and Bronze in Art, Corrosion, Colorants, Conservation; Getty Publications: Los Angeles, 2002.
17. Horie, C. V.; Vint, J. A. Chalconatronite: A By-product of Conservation Stud. Conserv. 1982, 27, 185-186
18. Dowsett, M.; Adriaens, A. Cell for Simultaneous Synchrotron Radiation X-ray and Electrochemical Corrosion Measurements on Cultural Heritage Metals and other Materials Anal. Chem. 2006, 78, 3360-3365
19. Leyssens, K.; Adriaens, A.; Degrigny, C.; Pantos, E. Evaluation of Corrosion Potential Measurements as a Means to Monitor the Storage and Stabilization Processes of Archaeological Copper-Based Artifacts Anal. Chem. 2006, 78, 2794-2801
20. Lamy, C. Stabilisation dobjets Archéologiques Chlorurés en Alliage Cuivreux-Définition des Conditions dune Polarisation Cathodique à Potentiel Constant en Solution de Sesquicarbonate de Sodium 1%; Unpublished Rapport du Stage, Université de Nantes ISITEM, 1997.
21. Pollard, A. M.; Thomas, R. G.; Williams, P. A. Synthesis and Stabilities of the Basic Copper(II) Chlorides Atacamite, Paratacamite, and Botallackite Mineral. Mag. 1989, 53, 557-563
22. Leyssens, K.; Adriaens, A.; Dowsett, M.; Schotte, B.; Oloff, I.; Pantos, E.; Bell, A. M. T.; Thompson, S. Simultaneous In Situ Time Resolved SR-XRD and Corrosion Potential Analyses to Monitor the Corrosion on Copper Electrochem. Commun. 2005, 7, 1265-1270
23. Adriaens, A.; Dowsett, M.; Leyssens, K.; Van Gasse, B. Insights into the Electrolytic Stabilization with Weak Polarization as Treatment for Archaeological Copper Objects Anal. Bioanal. Chem. 2007, 387, 861-868
24. Lewis, R. A.; Helsby, W. I.; Jones, A. O.; Hall, C. J.; Parker, B.; Sheldon, J.; Clifford, P.; Hillen, M.; Sumner, I.; Fore., N. S.; Jones, R. W. M.; Roberts, K. M. The "RAPID" High Rate Large Area X-ray Detector System Nucl. Instrum. Methods Phys. Res., Sect. A 1997, 392, 32-41
25. Adriaens, A.; Dowsett, M.; Jones, G. K. C.; Leyssens, K.; Nikitenko, S. An In-situ X-ray Absorption Spectroelectrochemistry Study of the Response of Artificial Chloride Corrosion Layers on Copper to Remedial Treatment J. Anal. At. Spectrom. 2009, 24 (1) 62-68
26. Adriaens, A.; Dowsett, M. Time-resolved Spectroelectrochemistry Studies for the Protection of Heritage Metals Surf. Eng. 2008, 24 (2) 84-89
27. Kear, G.; Barker, B. D.; Walsh, F. C. Electrochemical Corrosion of Unalloyed Copper in Chloride Media-A Critical Review Corros. Sci. 2004, 46, 109-135
28. Costa, V. private communication.
29. Dowsett, M.; Adriaens, A.; Jones, G. K. C.; Poolton, N. R. J.; Fiddy, S.; Nikitenko, S. Optically Detected X-ray Absorption Spectroscopy (ODXAS) Measurements as a Means to Monitor Corrosion Layers on Copper Anal. Chem. 2008, 80, 8717-8724