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note
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Selected data for 8: monoclinic space group P 121/ n 1 with a = 15.1272(5) Å, b = 5.4965(2) Å, c = 16.8300(8) Å, β = 114.777(2)° at 293(2) K with Z = 4. Refinement of 3015 reflections, and 190 parameters, yielded R 2 = 0.1268 for all data (1767 reflections with I > 2σ(I)).
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