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20444501948
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note
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A simpler [3 + 1] cyclization of 6 with 7 afforded a complicated reaction mixture under essentially the same reaction conditions as those used for the cross-coupling reactions 5 + 6 → 7 and 7 + 8 → 9.
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18
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0001038733
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For reviews on the palladium-catalyzed aryl animation: (a) Wolfe, J. P.; Wagaw, S.; Marcoux, J. F.; Buchwald, S. L. Acc. Chem. Res. 1998, 31, 805.
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29
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20444445655
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note
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Plus and minus signs indicate downfield and upfield shifts, respectively, compared to the chemical shift of the relevant reference compound.
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30
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20444499567
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note
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-3; CCDC 263006. See Supporting Information for crystallographic data in CIF format.
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31
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20444469421
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note
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CH⋯centroid distance and angle are omitted for the positional disorder of tert-butyl groups.
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32
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0034596789
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Messina, M. T.; Metrangolo, P. M.; Pappalardo, S.; Parisi, M. F.; Pilati, T.; Resnati, G. Chem. Eur. J. 2000, 6, 3495.
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Messina, M.T.1
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Pilati, T.5
Resnati, G.6
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34
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3242746379
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Rigaku and Rigaku/MSC: The Woodlands, TX
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CrystalStructure, version 3.6.0; Rigaku and Rigaku/MSC: The Woodlands, TX, 2004.
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CrystalStructure, Version 3.6.0
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