Development and validation of an ultra-high performance liquid chromatography tandem mass spectrometry method for quantifying thyreostats in urine without derivatisation

Journal of Chromatography A

Volumn 1217, Issue 26, 2010, Pages 4285-4293

  Vanden Bussche, J ^a   Vanhaecke, L ^a   Deceuninck, Y ^b   Verheyden, K ^a   Wille, K ^a   Bekaert, K ^a   Le Bizec, B ^b   De Brabander, H F ^a  

^a GHENT UNIVERSITY   (Belgium)

^b Waters Corporation   (France)

Author keywords

2002 657 EC; Thiouracil; Thyreostats; Triple quadrupole mass analyzer; UHPLC; Validation

Indexed keywords

2002/657/EC; ANALYTICAL METHOD; ANALYTICAL PROCEDURE; DECISION LIMIT; DERIVATISATION; DETECTION CAPABILITY; DITHIOTHREITOL; ETHYL ACETATES; EU CRITERIA; EUROPEAN UNION; LIQUID-LIQUID EXTRACTION; MINIMUM REQUIRED PERFORMANCE LIMITS; PERFORMANCE CHARACTERISTICS; QUANTITATIVE ANALYSIS; RELATIVE STANDARD DEVIATIONS; SAMPLE PRETREATMENT; THYREOSTATS; TRIPLE QUADRUPOLE; ULTRA-HIGH PERFORMANCE;

AGRICULTURE; BODY FLUIDS; ESTERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY;

SOLVENT EXTRACTION;

ACETIC ACID ETHYL ESTER; DITHIOTHREITOL; METHYLTHIOURACIL; PROPYLTHIOURACIL; THIAMAZOLE; THIOURACIL; XENOBIOTIC AGENT;

ACCURACY; ARTICLE; CONCENTRATION PROCESS; CONTROLLED STUDY; DENATURATION; DERIVATIZATION; LIQUID LIQUID EXTRACTION; NONHUMAN; PRIORITY JOURNAL; PROCESS DEVELOPMENT; QUANTITATIVE ANALYSIS; TANDEM MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; URINALYSIS; VALIDATION PROCESS;

ANIMALS; ANTITHYROID AGENTS; CATTLE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; SHEEP; SWINE; TANDEM MASS SPECTROMETRY; THIOURACIL;

EID: 77953541513     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.04.030     Document Type: Article

References (45)

1. H.F. De Brabander, Thesis Ghent University, Ghent Belgium (1984).
2. Courtheyn D., Le Bizec B., Brambilla G., De Brabander H.F., Cobbaert E., de Wiele A.V., Vercammen J., De Wasch K. Anal. Chim. Acta 2002, 473:71.
3. Mackenzie C.G., Mackenzie J.B. Endocrinology 1943, 32:185.
4. Kotter L., Terplan G., Schulz J. Arch. Lebensmittelhyg. 1959, 10:145.
5. Derblom H., Johansson H., Nylander G. Acta Chir. Scand. 1963, 10:1.
6. International Agency for Research on Cancer, http://monographs.iarc.fr/ENG/Classification/index.php.
7. Council Directive 81/602/EC Off. J. Eur. Commun. 1981, L222:32.
8. CRL Guidance Document (December 2007), http://www.rivm.nl/bibliotheek/digitaaldepot/crlguidance2007.pdf.
9. Commission Regulation 2377/90 Off. J. Eur. Commun. 1990, L224:1.
10. De Brabander H.F., Verbeke R. J. Chromatogr. 1975, 108:141.
11. De Brabander H.F., Smets F., Pottie G. J. Planar Chromatogr. 1988, 1:369.
12. De Brabander H.F., Rasschaert G., Vanneste W. J. Planar Chromatogr. 1989, 2:484.
13. De Brabander H.F., Batjoens P., Van Hoof J. J. Planar Chromatogr. 1992, 5:124.
14. Floberg S., Lanbeck K., Lindstrom B. J. Chromatogr. 1980, 182:63.
15. Yu G.Y.F., Murby E.J., Wells R.J. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 1997, 703:159.
16. Schilt R., Weseman J.M., Hooijerink H., Korbee H.J., Traag W.A., Vansteenbergen M.J., Haasnoot W. J. Chromatogr. B Biomed. Appl. 1989, 489:127.
17. N. Le Marrec, Thèse d'université, Nantes France (1995) p. 185.
18. Le Bizec B., Monteau F., Maume D., Montrade M.P., Gade C., Andre F. Anal. Chim. Acta 1997, 340:201.
19. Zou Q.H., Liu Y., Xie M.X., Han J., Zhang L. Anal. Chim. Acta 2005, 551:184.
20. Zhang L., Liu Y., Xie M.X., Qiu Y.M. J. Chromatogr. A 2005, 1074:1.
21. Pinel G., Maume D., Deceuninck Y., Andre F., Le Bizec B. Rapid Commun. Mass Spectrom. 2006, 20:3183.
22. Le Bizec B., Antignac J.P., Bichon E., Pinel G., Worrall K. Waters Appl. Note 2005, 720001124EN.
23. De Wasch K., De Brabander H.F., Impens S., Vandewiele M., Courtheyn D. J. Chromatogr. A 2001, 912:311.
24. Pinel G., Bichon E., Pouponneau K., Maume D., Andre F., Le Bizec B. J. Chromatogr. A 2005, 1085:247.
25. Lõhmus M., Kallaste K., Le Bizec B. J. Chromatogr. A 2009, 1216:8080.
26. Vanden Bussche J., Noppe H., Verheyden K., Wille K., Pinel G., Le Bizec B., De Brabander H.F. Anal. Chim. Acta 2009, 637:2.
27. Kuijpers C.J.P.F., Sterk S.S., Herbold H.A., Van Ginkel L.A. Conference on Residues of Veterinary Drugs in Food VI Egmond aan Zee 2008, 605.
28. Pinel G., Mathieu S., Cesbron N., Maume D., De Brabander H.F., Andre F., Le Bizec B. Food Addit. Contam. 2006, 23:974.
29. Abuin S., Centrich F., Rubies A., Companyo R., Prat M.D. Anal. Chim. Acta 2008, 617:184.
30. Abuin S., Companyo R., Centrich F., Rubies A., Prat M.D. J. Chromatogr. A 2008, 1207:17.
31. Commission Decision 2002/657/EC Off. J. Eur. Commun. 2002, L221:8.
32. Antignac J.P., De Wasch K., Monteau F., De Brabander H.F., Andre F., Le Bizec B. Anal. Chim. Acta 2005, 529:129.
33. Wren S.A.C. J. Pharm. Biomed. Anal. 2005, 38:337.
34. Blanchflower W.J., Hughes P.J., Cannavan A., McCoy M.A., Kennedy D.G. Analyst 1997, 122:967.
35. Mabon N., Wathelet J.-P., Marlier M. Talanta 1999, 49:199.
36. Odani A., Kozlowski H., Swiatek-Kozlowska J., Brasun J., Operschall B.P., Sigel H. J. Inorg. Biochem. 2007, 101:727.
37. Song D.D., Jasques N.A. Anal. Biochem. 1997, 248:300.
38. Ramakrishnan N.R., Tau C.L., Arbakariya B.A. Biotechnol. Bioprocess. Eng. 2008, 13:613.
39. Huang J., Whitman S. J. Liq. Chromatogr. Rel. Technol. 2006, 29:2513.
40. Cawley D.B., Houston L.L. Biochim. Biophys. Acta 1979, 581:51.
41. Ros-Chumillas M., Egea-Cortines M., Lopez-Gomez A., Weiss J. Food Control 2007, 18:33.
42. Yamamoto N., Matsuzaka Y., Kimura M., Matsuki M., Yanagisawa Y. J. Biosci. Bioeng. 2009, 107:464.
43. Antignac J.P., Le Bizec B., Monteau F., Andre F. Anal. Chim. Acta 2003, 483:325.
44. Council Directive 96/23/EC Off. J. Eur. Commun. 1996, L125:10.
45. Buick R.K., Barry C., Traynor I.M., McCaughey W.J., Elliott C.T. J. Chromatogr. B 1998, 720:71.