First microwave synthesis of multiple metal-metal bond paddlewheel compounds

Green Chemistry

Volumn 12, Issue 6, 2010, Pages 965-96

  Herrero, Santiago ^a   Jiménez Aparicio, Reyes ^a   Perles, Josefina ^a   Priego, José L ^a   Urbanos, Francisco A ^a  

^a UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 77953295505     PISSN: 14639262     EISSN: 14639270     Source Type: Journal    
DOI: 10.1039/c003411h     Document Type: Article

References (25)

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24. 1/c, with a = 9.6596(4), b = 38.896(2), and c = 12.5248(5) Å, and β = 102.989(1)°. The, structure was solved by the Patterson method. The final cycles of refinement were carried out by full-matrix least-squares analyses with anisotropic thermal parameters for all non-hydrogen atoms. Calculations were carried out by using the SMART program for data collection and data reduction, and SHELX for refinement, with a final R factor of 0.0459 and a Goodness of Fit of 1.012. CCDC 766373 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre viawww.ccdc.cam.ac.uk/data_request/cif.
25. S. Herrero, R. Jiménez-Aparicio, J. Perles, J. L. Priego, F. A. Urbanos, unpublished results.