Molecular silicate and aluminate species in anhydrous and hydrated cements

Journal of the American Chemical Society

Volumn 132, Issue 21, 2010, Pages 7321-7337

  Rawal, Aditya ^a   Smith, Benjamin J ^a   Athens, George L ^a   Edwards, Christopher L ^b   Roberts, Lawrence ^c   Gupta, Vijay ^d   Chmelka, Bradley F ^a  

^a University of California   (United States)

^b Halliburton Company   (United States)

^c Roberts Consulting Group   (United States)

^d RTI INTERNATIONAL   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CEMENT HYDRATION; HETERONUCLEAR CORRELATION; HIGH MAGNETIC FIELDS; HYDRATED CEMENT; HYDRATED SILICATE; HYDRATION BEHAVIORS; HYDROXYL MOIETY; MAGIC ANGLE SPINNING; MOLECULAR CHARACTERISTICS; MOLECULAR SPECIES; NMR SPECTRUM; OIL WELL CEMENTS; SINGLE-PULSE; SOLID STATE NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; WHITE PORTLAND; X RAY FLUORESCENCE;

ALUMINUM; CALCIUM; CEMENTS; HYDRATES; HYDRATION; MAGNETIC FIELDS; MAGNETIC PROPERTIES; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RESONANCE; SETTING; SILICATES; SILICON; SPECTROSCOPIC ANALYSIS;

CALCIUM SILICATE;

ALUMINUM DERIVATIVE; CEMENT; HYDROXYL GROUP; SILICATE; WATER;

ANISOTROPY; ARTICLE; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; HYDRATION; MAGNETIC FIELD; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUANTITATIVE ANALYSIS; SOLID STATE; X RAY FLUORESCENCE;

ALUMINUM; FLUORESCENCE; MAGNETIC RESONANCE SPECTROSCOPY; SILICATE CEMENT; WATER; X-RAY DIFFRACTION;

EID: 77952846236     PISSN: 00027863     EISSN: 15205126     Source Type: Journal    
DOI: 10.1021/ja908146m     Document Type: Article

References (68)

1. Gadalla, M. Pyramid Illusions; Bastet Publishing: Erie, PA, 1997.
2. Sharp, J. H. Adv. Appl. Ceram. 2006, 105, 162-174
3. Aspdin, J. British Patent 5022, 1824.
4. Skibsted, J., Jakobsen, H. J., and Hall, C. J. Chem. Soc., Faraday Trans. 1994, 90, 2095-2098
5. Skibsted, J., Jakobsen, H. J., and Hall, C. Adv. Cem. Based Mater. 1998, 7, 57-59
6. Taylor, H. F. W. Cement Chemistry; Academic Press: London, 1990.
7. Hamad, B. S. Adv. Cem. Based Mater. 1995, 2, 161-167
8. Meredith, P., Donald, A. M., Meller, N., and Hall, C. J. Mater. Sci. 2004, 39, 997-1005
9. Jons, E. S. and Osbaeck, B. Cem. Concr. Res. 1982, 12, 167-78
10. Sigmund, W. M., Bell, N. S., and Bergström, L. J. Am. Ceram. Soc. 2000, 83, 1557-1574
11. Bill, J. and Aldinger, F. Adv. Mater. 1995, 7, 775
12. Lee, Y., Vogt, T., Hriljac, J. A., Parise, J. B., Hanson, J. C., and Kim, S. J. Nature 2002, 420, 485-489
13. Hass, K. C., Schneider, W. F., Curioni, A., and Andreoni, W. Science 1998, 282, 882-882
14. Corma, A. J. Catal. 2003, 216, 298-312
15. Taguchi, A. and Schüth, F. Microporous Mesoporous Mater. 2005, 77, 1-45
16. Ying, J. Y., Mehnert, C. P., and Wong, M. S. Angew. Chem., Int. Ed. 1999, 38, 56-77
17. Baccile, N., Babonneau, F., Thomas, B., and Coradin, T. J. Mater. Chem. 2009, 19, 8537-8559
18. Livage, J. Curr. Opin. Solid State Mater. Sci. 1997, 2, 132-138
19. Aizenberg, J., Weaver, J. C., Thanawala, M. S., Sundar, V. C., Morse, D. E., and Fratzl, P. Science 2005, 309, 275-278
20. Heuer, A. H., Fink, D. J., Laraia, V. J., Arias, J. L., Calvert, P. D., Kendall, K., Messing, G. L., Blackwell, J., Rieke, P. C., Thompson, D. H., Wheeler, A. P., Veis, A., and Caplan, A. I. Science 1992, 255, 1098-1105
21. Pietak, A. M., Reid, J. W., Stott, M. J., and Sayer, M. Biomaterials 2007, 28, 4023-4032
22. Komnitsas, K. and Zaharaki, D. Miner. Eng. 2007, 20, 1261-1277
23. Brown, G. E. Science 2001, 294, 67-69
24. Skibsted, J. and Hall, C. Cem. Concr. Res. 2008, 38, 205-225
25. Colombet, P. Nuclear Magnetic Resonance Spectroscopy of Cement-Based Materials: Springer-Verlag: Berlin, 1999; Vol. 37.
26. Skibsted, J., Hall, C., and Jakobsen, H. J. In Structure and Performance of Cements; Bensted, J. and Barnes, P., Eds.; Spon Press: New York, 2002.
27. Zanni, H., Rassem-Bertolo, R., Masse, S., Fernandez, L., Nieto, P., and Bresson, B. Magn. Reson. Imag. 1996, 14, 827-831
28. Edwards, C. L., Alemany, L. B., and Barron, A. R. Ind. Eng. Chem. Res. 2007, 46, 5122-5130
29. Engelhardt, G. and Michel, D. High-Resolution Solid-State NMR of Silicates and Zeolites; John Wiley & Sons: Chichester, 1987.
30. Le Saout, G., Lecolier, E., Rivereau, A., and Zanni, H. Cem. Concr. Res. 2006, 36, 428-433
31. Sun, G. K., Young, J. F., and Kirkpatrick, R. J. Cem. Concr. Res. 2006, 36, 18-29
32. Andersen, M. D., Jakobsen, H. J., and Skibsted, J. Cem. Concr. Res. 2006, 36, 3-17
33. Brunet, F., Bertani, P., Charpentier, T., Nonat, A., and Virlet, J. J. Phys. Chem. B 2004, 108, 15494-15502
34. Rottstegge, J., Wilhelm, M., and Spiess, H. W. Cem. Concr. Comp. 2006, 28, 417-426
35. Faucon, P., Charpentier, T., Bertrandie, D., Nonat, A., Virlet, J., and Petit, J. C. Inorg. Chem. 1998, 37, 3726-3733
36. Skibsted, J. and Jakobsen, H. J. J. Chem. Soc., Faraday Trans. 1995, 91, 4423-4430
37. Mao, J. D. and Schmidt-Rohr, K. Solid State Nucl. Magn. Reson. 2004, 26, 36-45
38. Gullion, T. and Schaefer, J. J. Magn. Reson. 1989, 81, 196-200
39. Christiansen, S. C., Hedin, N., Epping, J. D., Janicke, M. T., del Amo, Y., Demarest, M., Brzezinski, M., and Chmelka, B. F. Solid State Nucl. Magn. Reson. 2006, 29, 170-182
40. Massiot, D., Fayon, F., Capron, M., King, I., Le Calve, S., Alonso, B., Durand, J. O., Bujoli, B., Gan, Z. H., and Hoatson, G. Magn. Reson. Chem. 2002, 40, 70-76
41. Ernst, R. R., Bodenhausen, G., and Wokaun, A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions; Oxford University Press: New York, 1997.
42. Janicke, M. T., Landry, C. C., Christiansen, S. C., Kumar, D., Stucky, G. D., and Chmelka, B. F. J. Am. Chem. Soc. 1998, 120, 6940-6951
43. Schmidt-Rohr, K., Clauss, J., and Spiess, H. W. Macromolecules 1992, 25, 3273-3277
44. Massiot, D., Bessada, C., Coutures, J. P., and Taulelle, F. J. Magn. Reson. 1990, 90, 231-242
45. Poulsen, S. L., Kocaba, V., Le Saout, G., Jakobsen, H. J., Scrivener, K. L., and Skibsted, J. Solid State Nucl. Magn. Reson. 2009, 36, 32-44
46. Brown, P. W. J. Am. Ceram. Soc. 1987, 70, 493-496
47. Bishop, M., Bott, S. G., and Barron, A. R. Chem. Mater. 2003, 15, 3074-3088
48. Millogo, Y., Hajjaji, M., Ouedraogo, R., and Gomina, M. Constr. Build. Mater. 2008, 22, 2078-2086
49. 2 symmetry, with correspondingly larger CSAs, respectively.
50. 28Si atoms in cements as well.
51. Fleischer, U., Kutzelnigg, W., Bleiber, A., and Sauer, J. J. Am. Chem. Soc. 1993, 115, 7833-7838
52. Hunger, M. Solid State Nucl. Magn. Reson. 1996, 6, 1-29
53. Hunger, M., Freude, D., and Pfeifer, H. J. Chem. Soc., Faraday Trans. 1991, 87, 657-662
54. Stebbins, J. F. and Kanzaki, M. Science 1991, 251, 294-298
55. Duffy, J. A. and Macphee, D. E. J. Phys. Chem. B 2007, 111, 8740-8745
56. Skibsted, J., Rasmussen, S., Herfort, D., and Jakobsen, H. J. Cem. Concr. Compos. 2003, 25, 823-829
57. Schmidt, T., Lothenbach, B., Romer, M., Scrivener, K., Rentsch, D., and Figi, R. Cem. Concr. Res. 2008, 38, 337-349
58. Schmidt-Rohr, K. and Spiess, H. W. Multidimensional Solid-State NMR and Polymers; Academic Press Limited: London, 1994.
59. Pellenq, R. J. M., Kushima, A., Shahsavari, R., Van Vliet, K. J., Buehler, M. J., Yip, S., and Ulm, F. J. Proc. Nat. Acad. Sci. U.S.A. 2009, 106, 16102-16107
60. Allen, A. J., Thomas, J. J., and Jennings, H. M. Nat. Mater. 2007, 6, 311-316
61. Xu, Z. and Viehland, D. Phys. Rev. Lett. 1996, 77, 952-955
62. Le Saout, G., Lecolier, E., Rivereau, A., and Zanni, H. Cem. Concr. Res. 2006, 36, 71-78
63. Skibsted, J., Henderson, E., and Jakobsen, H. J. Inorg. Chem. 1993, 32, 1013-1027
64. 27Al environments that likely arise from distributions of Al sites substituted for Si within these phases.
65. Chan, C. J., Kriven, W. M., and Young, J. F. J. Am. Ceram. Soc. 1988, 71, 713-719
66. Faucon, P., Delagrave, A., Petit, J. C., Richet, C., Marchand, J. M., and Zanni, H. J. Phys. Chem. B 1999, 103, 7796-7802
67. Shertukde, P. V., Hall, W. K., Dereppe, J. M., and Marcelin, G. J. Catal. 1993, 139, 468-481
68. Hall, C. and Scrivener, K. L. Adv. Cem. Based Mater. 1998, 7, 28-38