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note
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Details of the refinements: 1: AU non-hydrogen atoms were refined using anisotropic displacement parameters. Hydrogen atoms of the chloroform molecules could not be located on the Fourier map and were therefore not included in the final refinement. All remaining hydrogen atoms were positioned with idealized geometry and were refined using a riding model. 2: All non-hydrogen atoms were refined using anisotropic displacement parameters. Hydrogen atoms of the chloroform molecules were refined using isotropic displacement parameters. All remaining hydrogen atoms were positioned with idealized geometry and were refined using a riding model. 3: All non-hydrogen atoms were refined using anisotropic displacement parameters. Hydrogen atoms of the water molecule were refined using isotropic displacement parameters. All remaining hydrogen, atoms were positioned with, idealized geometry and were refined using a riding model. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-763275, -763276, and -763277. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [Fax: + 44-1223-336-033; EMail: deposi.t@ccdc.cam.ac.uk].
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21
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77952661099
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Due to the nature of the crystals of 1, we were unable to obtain a dataset of better quality than the one used to determine this structure
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Due to the nature of the crystals of 1, we were unable to obtain a dataset of better quality than the one used to determine this structure.
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22
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