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77952327492
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note
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N -Phenyldiethanolamine 2-pyridylboronate is prepared as a structurally undefined complex containing variable quantities of isopropyl and N -phenyldiethanolamine groups and a stoichiometric quantity of lithium
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77952383300
-
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Solid-supported diethanolamine adducts
-
Solid-supported diethanolamine adducts
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41
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0037059434
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3242758159
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A solid-supported diethanolamine-bound 2-pyridyl reagent has also been reported
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77952350881
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note
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2-Pyridyl stannanes represent stable and effective alternatives, but these reagents suffer from substantial toxicity
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53
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Cragg, S.T.1
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55
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77952352458
-
-
note
-
2O to afford 1a (11 g, 55%).
-
-
-
-
56
-
-
77952401259
-
-
note
-
3B can be purchased on the kilogram scale for <20/mol (Spectrum Chemicals, Gardena, CA, USA), <31/mol (Beta Pharma, New Haven, CT, USA), and <28/mol (Matrix Scientific, Columbia, SC, USA), respectively.
-
-
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57
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37049150255
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Childs, A. F.; Goldsworthy, L. J.; Harding, G. F.; King, F. E.; Nineham, A. W.; Norris, W. L.; Plant, S. G. P.; Selton, B.; Tompsett, A. L. L. J. Chem. Soc. 1948, 2174-2177
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60
-
-
77952324139
-
-
note
-
Iminodiacetic acid can be purchased on the kilogram scale for <5.50/mol (City Chemical, West Haven, CT, USA).
-
-
-
-
62
-
-
77952367167
-
-
Sigma-Aldrich: 1a 719390, 1b 723959, 1e 723053
-
Sigma-Aldrich: 1a 719390, 1b 723959, 1e 723053.
-
-
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63
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66949157122
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For the recent synthesis and reactivity of 5-thiazol pinacol boronic ester, see
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Reece, M.17
Saadi, M.18
Selwood, D.L.19
Stratton, G.C.20
Surry, D.21
Todd, R.22
Tong, X.23
Ruston, V.24
Upton, R.25
Weiss, S.M.26
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