Development of single-drop microextraction and simultaneous derivatization followed by GC-MS for the determination of aliphatic amines in tobacco

Journal of Separation Science

Volumn 33, Issue 9, 2010, Pages 1283-1287

  Sha, Yunfei ^a   Meng, Jiaoran ^b   Lin, Huaqing ^a   Deng, Chunhui ^b   Liu, Baizhan ^a  

^a Shanghai Tobacco Group Corp   (China)

^b FUDAN UNIVERSITY   (China)

Author keywords

Aliphatic amines; GC MS; Headspace single drop microextraction; Simultaneous derivatization; Tobacco

Indexed keywords

ALIPHATIC AMINES; ANALYTES; BENZYL ALCOHOL; DERIVATIZATION OF; DERIVATIZATION REAGENT; DERIVATIZATIONS; EXPERIMENT CONDITION; EXTRACTION PROCEDURE; EXTRACTION SOLVENTS; EXTRACTION TIME; FAST EXTRACTION; HEADSPACE SINGLE DROP MICROEXTRACTION; HEADSPACES; IN-SITU DERIVATIZATION; LIMIT OF DETECTION; METHOD VALIDATIONS; MICRODROPS; OPTIMAL CONDITIONS; SAMPLE PREPARATION; SINGLE DROP MICROEXTRACTION; SINGLE-STEP; TOBACCO SAMPLES;

AMINES; OPTIMIZATION; ORGANIC SOLVENTS; TOBACCO;

SOLVENT EXTRACTION;

3 PENTYLAMINE; ALIPHATIC AMINE; BENZALDEHYDE DERIVATIVE; BENZYL ALCOHOL; BUTYLAMINE; ORGANIC SOLVENT; PROPYLAMINE; UNCLASSIFIED DRUG;

ARTICLE; CONTROLLED STUDY; EXTRACTION AND EXTRACTS; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; SINGLE DROP MICROEXTRACTION; TOBACCO; VALIDATION STUDY;

AMINES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMIT OF DETECTION; REPRODUCIBILITY OF RESULTS; TOBACCO;

NICOTIANA TABACUM;

EID: 77952145130     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200900840     Document Type: Article

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