Novel derivatisation technique for the determination of chlorophenoxy acid type herbicides by gas chromatography-mass spectrometry

Analytical and Bioanalytical Chemistry

Volumn 397, Issue 2, 2010, Pages 537-548

  Maloschik, Erik ^a   Mörtl, Mária ^a   Székács, András ^a  

^a INSTITUTE OF EXPERIMENTAL MEDICINE   (Hungary)

Author keywords

Chlorophenoxy acids; Derivatisation; Gas chromatography; Mass spectrometry; Residue analysis; Silyl carbamates; Silylation

Indexed keywords

CHLOROPHENOXY ACIDS; DERIVATISATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; RESIDUE ANALYSIS; SILYLATIONS;

ACIDS; BIOLOGICAL MATERIALS; CHEMICAL DETECTION; ESTERS; GASES; GROUNDWATER; HERBICIDES; IMPACT IONIZATION; IONIZATION OF LIQUIDS; MASS SPECTROMETERS; MASS SPECTROMETRY; WEED CONTROL;

GAS CHROMATOGRAPHY;

CARBOXYLIC ACID; HERBICIDE;

CHEMISTRY; CONFERENCE PAPER; EVALUATION; MASS FRAGMENTOGRAPHY; METHODOLOGY; STATISTICAL PARAMETERS; WATER POLLUTANT;

CARBOXYLIC ACIDS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HERBICIDES; LIMIT OF DETECTION; WATER POLLUTANTS, CHEMICAL;

EID: 77951257600     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-010-3486-1     Document Type: Conference Paper

References (34)

1. M Rompa E Kremer B Zygmunt 2003 Derivatization in gaschromatographic determination of acidic herbicides in aqueous environmental samples Anal Bioanal Chem 377 590 599 10.1007/s00216-003-2117-5 1:CAS:528:DC%2BD3sXnsFGrtLg%3D (Pubitemid 40890273)
2. TCR Santos JC Rocha D Barcelo 2000 Determination of rice herbicides, their transformation products and clofibric acid using on-line solid-phase extraction followed by liquid chromatography with diode array and atmospheric pressure chemical ionization mass spectrometric detection J Chromatogr A 879 3 12 10.1016/S0021-9673(00)00100-X 1:CAS:528:DC%2BD3cXjt1alurg%3D (Pubitemid 30246032)
3. Rathore HS (2010) Methods of and problems in analyzing pesticide residues in the environment. In: Nollet LML, Rathore HS (eds) Handbook of pesticides: methods of pesticide residues analysis. CRC, Boca Raton, pp 7-46
4. C Aprea C Colosio T Mammone C Minoia M Maroni 2002 Biological monitoring of pesticide exposure: a review of analytical methods J Chromatogr B 769 190 219 (Pubitemid 34219253)
5. RB Geerdink WMA Niessen UATh Brickman 2002 Trace-level determination pesticides in water by means of liquid and gas chromatography J Chromatogr A 970 65 93 10.1016/S0021-9673(02)00234-0 1:CAS:528:DC%2BD38XnsF2ku7o%3D (Pubitemid 35286570)
6. DH Craston M Saeed 1998 Analysis of carboxylic and related acids in the environment by capillary electrophoretic techniques J Chromatogr A 827 1 12 10.1016/S0021-9673(98)00750-X 1:CAS:528:DyaK1cXns1Kqtbw%3D (Pubitemid 28543240)
7. JC Chuang JM Van Emon J Durnford K Thomas 2005 Development and evaluation of an enzyme-linked immunosorbent assay (ELISA) method for the measurement of 2, 4-dichlorophenoxyacetic acid in human urine Talanta 67 658 666 10.1016/j.talanta.2005.04.063 1:CAS:528:DC%2BD2MXpsFylu78%3D (Pubitemid 41244731)
8. KR Rogers AB Apostol WC Brumley 2000 Capillary electrophoresis immunoassay for 2, 4-dichlorophenoxyacetic acid Anal. Lett. 33 443 453 10.1080/00032710008543064 1:CAS:528:DC%2BD3cXhslOmtL4%3D (Pubitemid 30127709)
9. I Navrátilová P Skladal 2004 The immunosensors for measurement of 2, 4-dichlorophenoxyacetic acid based on electrochemical impedance spectroscopy Bioelectrochem 62 11 18 10.1016/j.bioelechem.2003.10.004 (Pubitemid 38283500)
10. M Dequaire G Degrand B Limoges 1999 An immunomagnetic electrochemical sensor based on a perfluorosulfonate-coated screen-printed electrode for the determination of 2, 4-dichlorophenoxyacetic acid Anal Chem 71 2571 2577 10.1021/ac990101j 1:CAS:528:DyaK1MXjtlCmu7g%3D (Pubitemid 29307628)
11. MI Catalina J Dallüge RJJ Vreuls UATh Brinkman 2000 Determination of chlorophenoxy acid herbicides in water by in situ esterification followed by in-vial liquid-liquid extraction combined with large volume on-column injection and gas chromatography-mass spectrometry J Chromatogr A 877 153 166 10.1016/S0021-9673(00)00242-9 1:CAS:528:DC%2BD3cXivVCquro%3D (Pubitemid 30227453)
12. A Ranz A Eberl E Maier E Lankmayr 2008 Microwave-assisted derivatization of acidic herbicides for gas chromatography-mass spectrometry J Chromatogr A 1192 282 288 10.1016/j.chroma.2008.03.076 1:CAS:528:DC%2BD1cXlslynurk%3D
13. ALS Pena MIN Silveira 1997 Determination of chlorophenoxy herbicides in waters by capillary gas chromatography with ion trap detection J Chromatogr A 758 324 331 10.1016/S0021-9673(96)00732-7 1:CAS:528:DyaK2sXht1Sju78%3D (Pubitemid 27061115)
14. AE Field K Monohan 1996 Chlorinated acid herbicides in water by strong anion-exchange disk extraction and in-vial elution and derivatization J Chromatogr A 741 85 90 10.1016/0021-9673(96)00148-3 1:CAS:528:DyaK28XltVOmsLY%3D (Pubitemid 26290372)
15. T Nilsson D Baglio I Galdo-Miguez J∅ Madsen S Facchetti 1998 Derivatisation/solid-phase microextraction followed by gas chromatography-mass spectrometry for the analysis of phenoxy acid herbicides in aqueous samples J Chromatogr A 826 211 216 10.1016/S0021-9673(98)00740-7 1:CAS:528:DyaK1MXjslGk (Pubitemid 28543142)
16. DJ Munch AM Pawlecki-Vonderheide 1998 Application of the base-promoted esterification procedure to the chlorophenoxy acid herbicides of US EPA method 515.3 J Chomatogr Sci 36 272 283
17. E Crespo-Corral MJ Santos-Delgado LM Polo-Diez AC Soria 2008 Determination of carbamate, phenylurea and phenoxy acid herbicide residues by gas chromatography after potassium tert-butoxide/dimethyl sulphoxide/ethyl iodide derivatization reaction J Chromatogr A 1209 2 28
18. O Chienthavorn S Pengpumkiat A Noomhorm RM Smith 1997 Superheated water extraction and phase transfer methylation of phenoxy acid herbicides from solid matrices J Chromatogr A 1152 268 273 10.1016/j.chroma.2006.12.055
19. W-H Ding C-H Liu S-P Yeh 2000 Analysis of chlorophenoxy acid herbicides in water by large-volume on-line derivatization and gas chromatography-mass spectrometry J Chromatogr A 896 111 116 10.1016/S0021-9673(00)00576-8 1:CAS:528:DC%2BD3cXntlGqtL4%3D
20. A Ranz E Lankmayr 2006 Screening and optimization of the dervatization of polar herbicides with trimethylanilinium hydroxide for GC-MS analysis J Biochem Biophys Methods 69 3 14 10.1016/j.jbbm.2006.02.007 1:CAS:528:DC%2BD28XhtVGjt7bE (Pubitemid 44486420)
21. M Rompa E Kremer B Zygmunt 2004 Derivatization of acidic herbicides with selected tetraalkyl ammonium and trimethyl sulfonium hydroxides for their GC analysis Anal Lett 37 3299 3312 10.1081/AL-200040368 1:CAS:528: DC%2BD2cXhtVyisb%2FJ (Pubitemid 40075769)
22. X Lou DJ Miller SB Hawthorne 2000 Static subcritical water extraction combined with anion exchange disk sorption for determining chlorinated acid herbicides in soil Anal Chem 72 481 488 10.1021/ac990787f 1:CAS:528: DC%2BD3cXmtVWmtA%3D%3D (Pubitemid 33595282)
23. T Heberer HJ Stan 1997 Detection of more than 50 substituted phenols as their t-butyldimethylsilyl derivatives using gas chromatograph-mass spectrometry Anal Chim Acta 341 21 34 10.1016/S0003-2670(96)00557-0 1:CAS:528: DyaK2sXht1Kit74%3D (Pubitemid 27163409)
24. I Rodríguez-Pereiro RG Irimina ER Cano RC Torrijos 2004 Optimisation of a gas chromatography-mass spectrometric method for the determination of phenoxy acid herbicides in water samples as silyl derivatives Anal Chim Acta 524 249 256 10.1016/j.aca.2004.03.091 (Pubitemid 39244049)
25. Á Kovács A Kende M Mörtl G Volk T Rikker K Torkos 2008 Determination of phenols and chlorophenols as trimethylsilyl derivatives using gas chromatography-mass spectrometry J Chromatogr A 1194 139 142 10.1016/j.chroma.2008.04.043
26. D Knausz A Meszticzky L Szakács B Csákvári K Újszászy 1983 Trimethylsilylated N-alkyl-substituted carbamates 1. Preparation and some reactions J Organomet Chem 256 11 18 10.1016/S0022- 328X(00)99291-X 1:CAS:528:DyaL2cXhtVensbk%3D
27. A Di Corcia M Marchetti 2001 Multiresidue method for pesticides in drinking water using a graphitized carbon black cartridge extraction and liquid chromatographic analysis Anal Chem 63 580 585 10.1021/ac00006a007
28. E Majzik-Solymos É Visi G Károly B Beke-Berczi L Györfi 2001 Comparison of extraction methods to monitor pesticide residues in surface water J Chrom Sci 39 325 331 1:CAS:528:DC%2BD3MXlvVCqtr8%3D (Pubitemid 34984112)
29. Hungarian Standards Institution (1995) Water quality. Sampling: Part 1. Guidance on the design of sampling programmes and sampling techniques (ISO 5667-1:2006). Hungarian Standard (MSZ ISO) 5667-6:1995, Budapest, Hungary (in Hungarian)
30. Tomlin CDS (ed) (2000) The pesticide manual, 12th edn. British Crop Protection Council, Farnham
31. IV Tetko VY Tanchuk 2002 Application of associative neural networks for prediction of lipophilicity in ALOGPS J Chem Inf Comput Sci 42 1136 1145 1:CAS:528:DC%2BD38XlvFSmtrY%3D (Pubitemid 35360297)
32. International Union of Pure and Applied Chemistry (2008) IUPAC Global availability of information on agrochemicals. IUPAC, Research Triangle Park, NC, USA ( http://www.iupac.org/web/ins/2008-041-1-600 )
33. MG Cabral CA Viegas MC Teixeira I Sá-Correia 2003 Toxicity of chlorinated phenoxyacetic acid herbicides in the experimental eukaryotic model Saccharomyces cerevisiae: role of pH and of growth phase and size of the yeast cell population Chemosphere 51 47 54 10.1016/S0045-6535(02)00614-8 1:CAS:528:DC%2BD3sXhtVelu7c%3D (Pubitemid 36267840)
34. N Loffhagen G Härtig W Babel 2003 Energization of Comamonas testosteroni ATCC 17454 for indicating toxic effects of chlorophenoxy herbicides Arch Environ Contam Toxicol 45 317 323 10.1007/s00244-003-2142-6 1:CAS:528:DC%2BD3sXos1Ggtbs%3D (Pubitemid 37158862)