Determination of carbamate, phenylurea and phenoxy acid herbicide residues by gas chromatography after potassium tert-butoxide/dimethyl sulphoxide/ethyl iodide derivatization reaction

Journal of Chromatography A

Volumn 1209, Issue 1-2, 2008, Pages 22-28

  Crespo Corral, E ^a   Santos Delgado, M J ^a   Polo Diez L M ^a   Soria, A C ^b  

^a UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

^b INSTITUTO DE QUÍMICA ORGÁNICA GENERAL   (Spain)

Author keywords

Derivatization reaction; GC MS; Herbicides; Natural water samples; Optimization

Indexed keywords

ACIDS; CATALYST ACTIVITY; CHEMICAL REACTIONS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; DIMETHYL SULFOXIDE; EXTRACTION; GAS CHROMATOGRAPHY; GAS HAZARDS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; OPTIMIZATION; PEST CONTROL; PESTICIDES; POTASSIUM; SODIUM; SOLVENT EXTRACTION; WEED CONTROL;

DERIVATIZATION; DERIVATIZATION REACTION; DETECTION LIMITS; DIMETHYL SULPHOXIDE; FACTORIAL DESIGN OPTIMIZATION; GAS CHROMATOGRAPHY - MASS SPECTROMETRY; GC-MS; MULTI COMPONENTS; NATURAL WATER SAMPLES; PHENOXY ACIDS; PHENYL UREAS; PHENYLUREA HERBICIDES; RELATIVE STANDARD DEVIATION; SOLID-PHASE EXTRACTION METHODS; WATER SAMPLES;

HERBICIDES;

CARBAMIC ACID; CARBANILAMIDE; DIMETHYL SULFOXIDE; ETHYL IODIDE; HERBICIDE; IODIDE; METHYL IODIDE; PHENOXYALKANOIC ACID; POTASSIUM DERIVATIVE; POTASSIUM TERT BUTOXIDE; SODIUM DERIVATIVE; SODIUM HYDRIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; DERIVATIZATION; FACTORIAL DESIGN; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; VALIDITY; WATER SAMPLING;

BUTANOLS; CARBAMATES; CHROMATOGRAPHY, GAS; DIMETHYL SULFOXIDE; HERBICIDES; MOLECULAR STRUCTURE; PESTICIDE RESIDUES; PHENYLUREA COMPOUNDS; REPRODUCIBILITY OF RESULTS; WATER POLLUTANTS, CHEMICAL;

EID: 53749096911     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2008.09.016     Document Type: Article

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