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Volumn 878, Issue 15-16, 2010, Pages 1103-1112
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Comparison of derivatization and chromatographic methods for GC-MS analysis of amino acid enantiomers in physiological samples
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Author keywords
Amino acid enantiomers; GC MS; Methyl chloroformate; Pre column derivatization; Racemization; Renal failure; Serum; Urine
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Indexed keywords
ALKALINE CONDITIONS;
AMINO ACID ENANTIOMERS;
CHIRAL COLUMN;
CHLOROFORMATES;
CHROMATOGRAPHIC METHODS;
DERIVATIZATION REACTION;
DERIVATIZATIONS;
GC-MS ANALYSIS;
HUMAN SERUM;
INTERNAL STANDARDS;
LIMITS OF DETECTION;
LOWER LIMITS;
METHYL CHLOROFORMATE;
NEUTRAL PH;
PEPTIDE HYDROLYSIS;
PRECOLUMN DERIVATIZATIONS;
PROTEINOGENIC;
RELATIVE STANDARD DEVIATIONS;
RENAL FAILURE;
SERUM PROTEINS;
URINE AND SERUM;
AMINO ACIDS;
CHIRALITY;
CHROMATOGRAPHIC ANALYSIS;
ENANTIOMERS;
ISOTOPES;
ORGANIC ACIDS;
PROTEINS;
BODY FLUIDS;
ACID ANHYDRIDE;
ALANINE;
AMINO ACID DERIVATIVE;
ASPARAGINE;
ASPARTIC ACID;
DEXTRO AMINO ACID;
METHANOL;
PEPTIDE;
PLASMA PROTEIN;
PROLINE;
THREONINE;
VALINE;
ACCURACY;
ALKALINITY;
AMINO ACID ANALYSIS;
ARTICLE;
BLOOD ANALYSIS;
CHIRALITY;
CLINICAL ARTICLE;
CONTROLLED STUDY;
DERIVATIZATION;
DUAL ENERGY X RAY ABSORPTIOMETRY;
ENANTIOMER;
GAS CHROMATOGRAPHY;
HUMAN;
INTERMETHOD COMPARISON;
ISOTOPE LABELING;
KIDNEY FAILURE;
MASS SPECTROMETRY;
PH MEASUREMENT;
PRECIPITATION;
PRIORITY JOURNAL;
PROTEIN HYDROLYSIS;
QUANTUM YIELD;
RACEMIZATION;
REFERENCE VALUE;
SENSITIVITY ANALYSIS;
URINALYSIS;
AMINO ACIDS;
ANHYDRIDES;
FORMATES;
FORMIC ACIDS;
GAS CHROMATOGRAPHY-MASS SPECTROMETRY;
HUMANS;
KIDNEY FAILURE;
METHANOL;
SENSITIVITY AND SPECIFICITY;
SODIUM HYDROXIDE;
STEREOISOMERISM;
TEMPERATURE;
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EID: 77950945876
PISSN: 15700232
EISSN: None
Source Type: Journal
DOI: 10.1016/j.jchromb.2010.03.021 Document Type: Article |
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Times cited : (53)
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References (29)
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