Validated spectrofluorimetric method for the determination of lamotrigine in tablets and human plasma through derivatization with o-phthalaldehyde

Journal of Fluorescence

Volumn 20, Issue 2, 2010, Pages 463-472

  El Enany, Nahed M ^a   El Sherbiny, Dina T ^a   Abdelal, Amina A ^a   Belal, Fathalla F ^a  

^a MANSOURA UNIVERSITY   (Egypt)

Author keywords

Lamotrigine; O phthalaldehyde; Spectrofluorimetry; Spiked and real human plasma; Tablets

Indexed keywords

2-MERCAPTOETHANOL; ACCURACY AND PRECISION; BIOLOGICAL FLUIDS; BORATE BUFFER; DERIVATIZATIONS; EXPERIMENTAL PARAMETERS; HUMAN PLASMAS; IN-VITRO; IN-VIVO; LAMOTRIGINE; LIMIT OF QUANTIFICATIONS; LOWER LIMIT OF DETECTIONS; MEAN PERCENTAGE; O-PHTHALALDEHYDE; PHARMACEUTICAL FORMULATION; REACTION PATHWAYS; REFERENCE METHOD; SPECTROFLUORIMETRIC METHODS; SPECTROFLUORIMETRY; STATISTICAL COMPARISONS;

DRUG PRODUCTS; FLUORESCENCE; PLASMA (HUMAN); SULFUR COMPOUNDS;

PLASMAS;

LAMOTRIGINE; MERCAPTOETHANOL; PHTHALALDEHYDE; TRIAZINE DERIVATIVE;

ARTICLE; BLOOD; BLOOD ANALYSIS; CHEMICAL MODEL; CHEMISTRY; CHILD; EPILEPSY; FLUORESCENCE; HUMAN; MALE; METHODOLOGY; PH; PLASMA; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SPECTROFLUOROMETRY; STATISTICAL MODEL; TABLET; TIME; VALIDATION STUDY;

BLOOD CHEMICAL ANALYSIS; CHILD; EPILEPSY; FLUORESCENCE; HUMANS; HYDROGEN-ION CONCENTRATION; LINEAR MODELS; MALE; MERCAPTOETHANOL; MODELS, CHEMICAL; O-PHTHALALDEHYDE; PLASMA; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROMETRY, FLUORESCENCE; TABLETS; TIME FACTORS; TRIAZINES;

EID: 77950857872     PISSN: 10530509     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10895-009-0568-6     Document Type: Article

References (28)

1. KL Goa SR Ross P Chrisp 1993 Lamotrigine: a review of its pharmacological properties and clinical efficacy in epilepsy Drugs 46 152 176 10.2165/00003495-199346010-00009 1:STN:280:DyaK2c%2FgvVGltg%3D%3D 7691504
2. J Messenheimer EL Mullens L Giorgi F Young 1998 Safety review of adult clinical expeiance with lamotrigine Drug Saf 18 281 296 10.2165/00002018- 199818040-00004 1:CAS:528:DyaK1cXislCjs7Y%3D 9565739 (Pubitemid 28177292)
3. M Pellock 1997 Overview of lamotrigine and the new antiepileptic drugs: the challenge J Child Neurol 12 S48 S52 10.1177/0883073897012001111 9429131
4. A Sabers I Ohman J Christensen T Tomson 2003 Oral contraceptives reduce lamotrigine plasma levels Neurology 61 570 571 1:CAS:528:DC%2BD3sXmtVemtr8%3D 12939444
5. NF Youssef EA Taha 2007 Development and validation of spectrophotometric, TLC and HPLC methods for the determination of lamotrigine in presence of its impurity Chem Pharm Bull 55 541 545 10.1248/cpb.55.541 1:CAS:528: DC%2BD2sXls1arsrk%3D 17409544 (Pubitemid 46570829)
6. ME Burgoa Calvo OD Renedo MJ Arcos Martínez 2007 Determination of lamotrigine by adsorptive stripping voltammetry using silver nanoparticle-modified carbon screen-printed electrodes Talanta 74 59 64 10.1016/j.talanta.2007.05.026 1:CAS:528:DC%2BD2sXht1GitrbE 18371613 (Pubitemid 47632734)
7. ME Burgoa Calvo OD Renedo MJ Arcos Martínez 2005 Optimization of the experimental parameters in the determination of lamotrigine by adsorptive stripping voltammetry Anal Chim Acta 549 74 80 10.1016/j.aca.2005.06.010 1:CAS:528:DC%2BD2MXpt1WrsL8%3D (Pubitemid 41160514)
8. J Emami N Ghassami F Ahmadi 2006 Development and validation of a new HPLC method for determination of lamotrigine and related compounds in tablet formulations J Pharm Biomed Anal 40 999 1005 10.1016/j.jpba.2005.07.045 1:CAS:528:DC%2BD28Xhs1Sgtbw%3D 16176866 (Pubitemid 43257908)
9. MA Saracino F Bugamelli M Conti M Amore MA Raggi 2007 Rapid HPLC analysis of the antiepileptic lamotrigine and its metabolites in human plasma J Sep Sci 30 2249 2255 10.1002/jssc.200700110 1:CAS:528:DC%2BD2sXhtFelu7%2FF 17683041 (Pubitemid 47497026)
10. O Beck I Ohman HK Nordgren 2006 Determination of lamotrigine and its metabolites in human plasma by liquid chromatography-mass spectrometry Ther Drug Monit 28 603 607 10.1097/01.ftd.0000245779.64080.30 1:CAS:528: DC%2BD28XhtVKrtLzJ 17038873 (Pubitemid 44564057)
11. L Zufía A Aldaz N Ibáñez C Viteri 2009 LC method for the therapeutic drug monitoring of lamotrigine: evaluation of the assay performance and validation of its application in the routine area J Pharm Biomed Anal 49 547 553 10.1016/j.jpba.2008.11.030 19131204
12. C Greiner E Haen 2007 Development of a simple column-switching high- performance liquid chromatography (HPLC) method for rapid and simultaneous routine serum monitoring of lamotrigine, oxcarbazepine and 10- monohydroxycarbazepine (MHD) J Chromatogr B 854 338 344 10.1016/j.jchromb.2007. 04.006 1:CAS:528:DC%2BD2sXntFygsb4%3D (Pubitemid 46962369)
13. E Greiner-Sosanko S Giannoutsos DR Lower MA Virji MD Krasowski 2007 Drug monitoring: simultaneous analysis of lamotrigine, oxcarbazepine, 10-hydroxycarbazepine, and zonisamide by HPLC-UV and a rapid GC method using a nitrogen-phosphorus detector for levetiracetam J Chromatogr Sci 45 616 622 1:CAS:528:DC%2BD2sXht1WnsLzK 17988451
14. C Ching-Ling C Chen-His O Yoa-Pu Hu 2005 Determination of lamotrigine in small volumes of plasma by high-performance liquid chromatography J Chromatogr B 817 199 206 10.1016/j.jchromb.2004.12.004 (Pubitemid 40430984)
15. S Bompadre A Tagliabracci M Battino R Giorgetti 2008 Determination of lamotrigine in whole blood with on line solid phase extraction J Chromatogr B 863 177 180 10.1016/j.jchromb.2007.12.020 1:CAS:528:DC%2BD1cXitVSjtLs%3D
16. J Zheng MW Jann YY Hon SA Shamsi 2004 Development of capillary zone electrophoresis-electrospray ionization-mass spectrometry for the determination of lamotrigine in human plasma Electrophoresis 25 2033 2043 10.1002/elps. 200305823 1:CAS:528:DC%2BD2cXmtFKltL4%3D 15237404 (Pubitemid 39136324)
17. V Pucci F Bugamelli C Baccini MA Raggi 2005 Analysis of lamotrigine and its metabolites in human plasma and urine by micellar electrokinetic capillary chromatography Electrophoresis. 26 935 942 10.1002/elps.200410208 1:CAS:528:DC%2BD2MXisVWit7o%3D 15669009 (Pubitemid 40424926)
18. R Kand'ár P Záková H Lotková O Kucera Z Cervinková M Yoshitake N Sejima H Yoshida K Todoroki H Nohta M Yamaguchi 2007 Determination of reduced and oxidized glutathione in biological samples using liquid chromatography with fluorimetric detection J Pharm Biomed Anal 43 1382 1387 10.1016/j.jpba.2006.11.028 17182211 (Pubitemid 46282398)
19. A Korös R Hanczkó A Jámbor Y Qian A Perl I Molnár-Perl 2007 Analysis of amino acids and biogenic amines in biological tissues as their o-phthalaldehyde/ethanethiol/fluorenylmethyl chloroformate derivatives by high-performance liquid chromatography. A deproteinization study J Chromatogr A 1149 46 55 10.1016/j.chroma.2006.11.018 17145062 (Pubitemid 46627624)
20. M Yoshitake N Sejima H Yoshida K Todoroki H Nohta M Yamaguchi 2007 Selective determination of tryptophan-containing peptides through precolumn derivatization and liquid chromatography using intramolecular fluorescence resonance energy transfer detection Anal Sci 8 949 953 10.2116/analsci.23.949
21. A El-Gindy A Ashour L Abdel-Fattah MM Shabana 2001 Spectrophotometric, septrofluorimetric and LC determination of lisinopril J Pharm Biomed Anal 25 913 922 10.1016/S0731-7085(01)00376-4 1:CAS:528:DC%2BD3MXjslektrg%3D 11377074 (Pubitemid 32488956)
22. PD Tzanavaras CK Zacharis P Rigas 2008 Novel automated assay for the quality control of mexiletine hydrochloride formulations using sequential injection and on-line dilution J Pharm Biomed Anal 48 1254 1260 10.1016/j.jpba.2008.09.017 1:CAS:528:DC%2BD1cXhsFClsbfE 18930618
23. Munson JW (1981) Pharmaceutical analysis Part A., NY, p 284
24. Y Sun MN Nakashima M Takahashi N Kuroda K Nakashima 2002 Determination of bisphenol A in rat brain by microdialysis and column switching high- performance liquid chromatography with fluorescence detection Biomed Chromatogr 16 319 326 10.1002/bmc.161 1:CAS:528:DC%2BD38XmvFWht78%3D 12210505 (Pubitemid 34982343)
25. Moffat AC, Osselton MD, Widdop B, Galichet LY (2006) Clark's analysis of drugs and poisons in pharmaceuticals, body fluids and postmortem material, 4th edn. Pharmaceutical, London Electronic version
26. International Conference on Harmonization Notes on "Validation of analytical procedures: text and methadology", Q2(R1) Approval on November 2005 http://www.ich.org/LOB/media/MEDIA417.pdf
27. Miller JC, Miller JN (2005) Statistics and chemometrics for analytical chemistry, 5th edn. Prentice Hall, England, p 256
28. Rose J (1964) Advanced physico-chemical experiments. Pitman, London