Synthesis of deuterium-labelled, optically active, ferroelectric liquid crystals

Tetrahedron

Volumn 66, Issue 19, 2010, Pages 3472-3477

  Marini, A ^a,b   Domenici, V ^a   Malanga, C ^a   Menicagli, R ^a   Veracini, C A ^a  

^a UNIVERSITY OF PISA   (Italy)

^b SCUOLA NORMALE SUPERIORE   (Italy)

Author keywords

Deuterium labelling; Ferroelectric liquid crystal; Organic synthesis

Indexed keywords

BIPHENYL DERIVATIVE; CARBONYL DERIVATIVE; CARBOXYLIC ACID DERIVATIVE; DEUTERIUM; IRON DERIVATIVE;

ARTICLE; BIOTRANSFORMATION; CATALYSIS; CATALYST; LIQUID CRYSTAL; OPTICAL ROTATION; PRIORITY JOURNAL; QUANTUM YIELD; REACTION ANALYSIS; REACTION TIME; STEREOCHEMISTRY; SYNTHESIS;

EID: 77950593922     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tet.2010.03.025     Document Type: Article

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23. Previously prepared according to the usual procedure starting from 10a (2.56 g, 12.92 mmol), freshly distilled thionyl chloride (25 mL, 0.34 mol) and dimethylformamide (DMF) (300 μL).
24. Previously prepared according to the usual procedure starting from 9a (2.57 g, 12.97 mmol), freshly distilled thionyl chloride (25 mL, 0.34 mol) and dimethylformamide (DMF) (300 μL).