Analysis of trans-cis fatty acids in fatty acid steryl esters isolated from soybean oil deodoriser distillate

Food Chemistry

Volumn 121, Issue 3, 2010, Pages 752-757

  Gunawan, Setiyo ^a   Melwita, Elda ^a   Ju, Yi Hsu ^a  

^a NATIONAL TAIWAN UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Taiwan)

Author keywords

Boron trifluoridel; Fatty acid steryl esters; Modified silica gel column chromatography; Modified soxhlet extraction; Soybean oil deodoriser distillate; Trans fatty acids

Indexed keywords

ELAIDIC ACID; ESTER DERIVATIVE; FATTY ACID DERIVATIVE; FATTY ACID STERYL ESTER; LINOLEAIDIC ACID; LINOLEIC ACID; OLEIC ACID; PALMITIC ACID; SOYBEAN OIL; STEARIC ACID; TRANS FATTY ACID; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL COMPOSITION; DISTILLATION; ESTERIFICATION; GAS CHROMATOGRAPHY; PURIFICATION; SAPONIFICATION; SOXHLET EXTRACTION; THIN LAYER CHROMATOGRAPHY; TRANSESTERIFICATION;

GLYCINE MAX;

EID: 77649179683     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2009.12.079     Document Type: Article

References (30)

1. Bartok, L., Hilaly, A., Schuette, C. M., & Shukla, R. (2005). Process for separation of tocopherols. US Patent no. 6,867,308.
2. Billheimer J.T., Avart S., and Milani B. Separation of steryl esters by reversed-phase liquid chromatography. Journal of Lipid Research 24 (1983) 1646-1651
3. Copeland, D., & Belcher, M. (2004). Methods for treating deodorizer distillate. US Patent no. 6,750,359.
4. De Greyt W.F., Kellens M., and Huyghebaert A.D. Effect of physical refining on selected minor components in vegetable oils. Fett/Lipid 101 (1999) 428-432
5. Evershed R.P., Male V.L., and Goad L.J. Strategy for the analysis of steryl esters from plant and animal tissues. Journal of Chromatography A 400 (1987) 187-205
6. Fizet, C. (1996). Process for tocopherols and sterols from natural sources. US Patent no. 5,487,817.
7. Fried B. Lipids. In: Sherma J., and Fried B. (Eds). Handbook of thin-layer chromatography (1996), Marcel Dekker Press, New York 704-705
8. Gordon M.H., and Griffith R.E. Steryl esters analysis as an aid to the identification of oils in blends. Food Chemistry 43 (1992) 71-78
9. Gunawan S., Fabian C., and Ju Y.H. Isolation and purification of fatty acid steryl esters from soybean oil deodorizer distillate. Industrial and Engineering Chemistry Research 47 (2008) 7013-7018
10. Gunawan S., Ismadji S., and Ju Y.H. Design and operation of a modified silica gel column chromatography. Journal of the Chinese Institute of Chemical Engineers 39 (2008) 625-633
11. Gunawan S., Kasim N.S., and Ju Y.H. Separation and purification of squalene from soybean oil deodorizer distillate. Separation and Purification Technology 60 (2008) 128-135
12. Gunawan S., Vali S.R., and Ju Y.H. Purification and identification of rice bran oil fatty acid steryl and wax esters. Journal of the American Oil Chemists Society 83 (2006) 449-456
13. Hirota Y., Nagao T., Watanabe Y., Suenaga M., Nakai S., Kitano M., et al. Purification of steryl esters from soybean oil deodorizer distillate. Journal of the American Oil Chemists Society 80 (2003) 341-346
14. Jacobs, L. (2005). Process for the production of tocotrienols. US Patent no. 6,838,104.
15. Judd J.T., Clevidence B.A., and Meusing R.A. Dietary trans fatty acids: Effect on plasma lipids and lipoprotein of healthy men and women. American Journal Clinical Nutrition 59 (1994) 861-868
16. Kamm W., Dionisi F., Fay L.B., Hischenhuber C., Schmarr H.G., and Engel K.H. Analysis of steryl esters in cocoa butter by on-line liquid chromatography-gas chromatography. Journal of Chromatography A 918 (2001) 341-349
17. Kasim N.S., Tsai T.H., Gunawan S., and Ju Y.H. Biodiesel production from rice bran oil and supercritical methanol. Bioresource Technology 100 (2009) 2007-2011
18. 2. Journal of Supercritical Fluids 23 (2002) 257-265
19. Mensink R.P., and Katan M.B. Effect of dietary trans fatty acids on high-density and low-density lipoprotein cholesterol levels in healthy subjects. New England Journal Medicine 323 (1990) 439-445
20. Metclafe L.D., and Schmitz A.A. The rapid preparation of fatty acid esters for gas chromatographic analysis. Analytical Chemistry 33 (1961) 363-364
21. Metclafe L.D., Schmitz A.A., and Pelka J.R. Rapid preparation of fatty acid esters from lipids for gas chromatographic analysis. Analytical Chemistry 38 (1961) 514-515
22. Montgomery D.C. Design and analysis of experiments. 6th ed. (2005), John Wiley and Sons, New York
23. Moreau R.A. Plant sterols in functional food. In: Dutta P.C. (Ed). Phytosterols as functional food components and nutraceuticals (2004), Marcel Dekker Press, New York 317-345
24. Morrison W.R., and Smith L.M. Preparation of fatty acid methyl esters and dimethylacetals from lipids with boron fluoride-methanol. Journal of Lipid Research 5 (1964) 600-608
25. Ostlund R.E. Phytosterols in human nutrition. Annual Review Nutrition 22 (2002) 533-549
26. Piironen V., Lindsay D., Miettinen T.A., Toivo J., and Lampi A.M. Plant sterols: Biosynthesis, biological function and their importance to human nutrition. Journal of the Science of Food and Agriculture 80 (2000) 939-966
27. Sloan A.E. Good for you fats and oils, new nutraceutical opportunities for fats and oils. Inform 17 (2006) 68-70
28. Top, A. G., Leong, L. W., Ong, A. S. H., Kawada, T., Watanabe, H., & Tsuchiya, N. (1993). Production of high concentration tocopherols and tocotrienols from palm oil by-products. US Patent no. 5,190,618.
29. Tsuzuki W., Nagata R., Yunoki R., Nakajima M., and Nagata T. Cis/trans-isomerization of triolein, trilinolein, and trilinolenin induced by heat treatment. Food Chemistry 108 (2008) 75-80
30. Willet W.C., Stampfer J.M., and Manson J.E. Intake of trans fatty acids and risk of coronary heart disease among woman. Lancet 341 (1993) 581-586