N-Ethoxycarbonylation combined with (S)-1-phenylethylamidation for enantioseparation of amino acids by achiral gas chromatography and gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1214, Issue 1-2, 2008, Pages 151-156

  Paik, Man Jeong ^a,b   Lee, Jinwoo ^c   Kim, Kyoung Rae ^c  

^a University School of Medicine   (South Korea)

^b Ajou University School of Medicine   (South Korea)

^c Sungkyunkwan University   (South Korea)

Author keywords

Amino acids; Beans; d Pipecolic acid; Diastereomeric N ethoxycarbonyl (S) 1 phenylethylamides; Enantiomeric separation; Gas chromatography mass spectrometry in selected ion monitoring mode

Indexed keywords

AMINATION; AMINES; AMINO ACIDS; CHEMICAL ANALYSIS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; GASES; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION CHROMATOGRAPHY; MAGNESIUM PRINTING PLATES; MASS SPECTROMETERS; MASS SPECTROMETRY; ORGANIC ACIDS; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS;

BEANS; D-PIPECOLIC ACID; DIASTEREOMERIC N-ETHOXYCARBONYL/(S)-1-PHENYLETHYLAMIDES; ENANTIOMERIC SEPARATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY IN SELECTED ION MONITORING MODE;

GAS CHROMATOGRAPHY;

2 AMINO 2 METHYLPROPIONIC ACID; 4 AMINOBUTYRIC ACID; ALANINE; ALPHA METHYLBENZYLAMINE; AMINO ACID; ASPARTIC ACID; ISOLEUCINE; NORLEUCINE; NORVALINE; PIPECOLIC ACID; PROLINE; VALINE;

AMIDATION; AMINO ACID ANALYSIS; AMINO ACID COMPOSITION; ARTICLE; CARBONYLATION; CHIRALITY; DIASTEREOISOMER; ENANTIOSELECTIVITY; GAS CHROMATOGRAPHY; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL;

AMINO ACIDS; CHROMATOGRAPHY, GAS; FABACEAE; FORMIC ACID ESTERS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LEAST-SQUARES ANALYSIS; PHASEOLUS; PHENETHYLAMINES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; STEREOISOMERISM;

PHASEOLUS VULGARIS; VIGNA ANGULARIS;

EID: 56549130190     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2008.10.068     Document Type: Article

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