Rapid analysis of constituents of Radix Cyathulae using hydrophilic interaction-reverse phase LC-MS

Journal of Separation Science

Volumn 32, Issue 22, 2009, Pages 3988-3995

  Ren, Mei Ting ^a   Li, Hui Jun ^a   Sheng, Long Sheng ^a   Liu, Peng ^a   Li, Ping ^a  

^a CHINA PHARMACEUTICAL UNIVERSITY   (China)

Author keywords

Cyathula officinalis; Hydrophilic interaction chromatography; Qualitative analysis; Reverse phase liquid chromatography; Time of flight mass spectrometry

Indexed keywords

ANALYSIS AND CHARACTERIZATION; BUFFER PH; COLLISION-INDUCED DISSOCIATION; CYASTERONE; ELECTROSPRAYS; FRAGMENTATION PATHWAYS; HERBAL DRUG; HYDROPHILIC INTERACTION; HYDROPHILIC INTERACTION CHROMATOGRAPHY; MOBILE PHASE; OLEANANE; ORGANIC MODIFIER; QUALITATIVE ANALYSIS; RAPID ANALYSIS; REVERSE PHASE; REVERSE PHASE LIQUID CHROMATOGRAPHY; SEPARATION PARAMETERS; STRUCTURE INFORMATION; TIME OF FLIGHT MASS SPECTROMETRY;

CHROMATOGRAPHIC ANALYSIS; GLUCOSE; HYDROPHILICITY; LIQUIDS; MASS SPECTROMETERS; MASS SPECTROMETRY; PH EFFECTS; QUALITY CONTROL; SUGAR (SUCROSE);

LIQUID CHROMATOGRAPHY;

3 O [ALPHA LEVO RHAMNOPYRANOSYL(1-2) BETA DEXTRO GLUCURONOPYRANOSYL] 28 O [BETA DEXTRO GLUCOPYRANOSYL(1-6) BETA DEXTRO GLUCOPYRANOSYL]HEDERAGENIN; 3 O ALPHA DEXTRO RHAMNOPYRANOSYL(1-3) BETA DEXTRO GALACTOPYRANOSYL(1-3) [BETA DEXTRO GLUCOPYRANOSYL(1-2)] BETA DEXTRO GLUCURONOPYRANOSYL OLEANOLIC ACID; 3 O ALPHA DEXTRO RHAMNOPYRANOSYL(1-3) BETA DEXTRO GALACTOPYRANOSYL(1-3) BETA DEXTRO GLUCURONOPYRANOSYL HEDERAGENIN; 3 O ALPHA LEVO RHAMNOPYRANOSYL BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL GYPSOGMIN; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-2) [BETA DEXTRO GLUCOPYRANOSYL(1-3)] BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL OLEANOLIC ACID; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-3) BETA DEXTO GLUCURONOPYRANOSYL OLEANOLIC ACID; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-3) BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL HEDERAGENIN; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-3) BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL OLEANOLIC ACID; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-3)[BETA DEXTRO GLUCOPYRANOSYL(1-2)] BETA DEXTRO GLUCURONOPYRANOSYL OLEANOLIC ACID; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-4) BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL HEDERAGENIN; 3 O ALPHA LEVO RHAMNOPYRANOSYL(1-4)[BETA DEXTRO GLUCOPYRANOSYL(1-2)] BETA DEXTRO GLUCURONOPYRANOSYL OLEANOLIC ACID; 3 O ALPHA LEVO XYLOPYRANOSYL(1-3) BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO RHAMNOPYRANOSYL OLEANOLIC ACID; 3 O BETA D GLUCOPYRANOSYL(1-2) ALPHA LEVO RHAMNOPYRANOSYL(1 3) BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL OLEANOLIC ACID; 3 O BETA DEXTRO GLUCOPYRANOSYL ALPHA LEVO RHAMNOPYRANOSYL BETA DEXTRO GLUCURONOPYRANOSYL 28 O ALPHA LEVO XYLOPYRANOSYL HEDERAGENIN; 3 O BETA DEXTRO GLUCOPYRANOSYL ALPHA LEVO RHAMNOPYRANOSYL BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL GYPSOGMIN; 3 O BETA DEXTRO GLUCOPYRANOSYL(1-2) ALPHA LEVO RHAMNOPYRANOSYL(1-3) BETA DEXTRO GLUCURONOPYRANOSYL OLEANOLIC ACID; 3 O BETA DEXTRO GLUCOPYRANOSYL(1-2)[ALPHA LEVO RHAMNOPYRANOSL(1-3)] BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL OLEANOLIC ACID; 3 O BETA DEXTRO GLUCOPYRANOSYL(1-2)[ALPHA LEVO RHAMNOPYRANOSYL(1-3)] BETA DEXTRO GLUCURONOPYRANOSYL GYPSOGMIN; 3 O BETA DEXTRO GLUCURONOPYRANOSYL 28 O ALPHA LEVO RHAMNOPYRANOSYL HEDERAGENIN; 3 O BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL HEDERAGENIN; 3 O BETA DEXTRO GLUCURONOPYRANOSYL 28 O BETA DEXTRO GLUCOPYRANOSYL OLEANOLIC ACID; 3 O BETA DEXTRO GLUCURONOPYRANOSYL OLEANOLIC ACID; BUFFER; CYASTERONE; ECDYSTEROID; FRUCTOSE; GLUCOSE; SAPONIN; SCOPARONE; SUCROSE; UNCLASSIFIED DRUG;

ARTICLE; CHINESE MEDICINE; CHROMATOGRAPHY; COLLISIONALLY ACTIVATED DISSOCIATION; CONTROLLED STUDY; CYATHULA OFFICINALIS; DRUG IDENTIFICATION; ELECTROSPRAY MASS SPECTROMETRY; FRAGMENTATION REACTION; HYDROPHILIC INTERACTION CHROMATOGRAPHY; HYDROPHILICITY; PH; PLANT ROOT; PRIORITY JOURNAL; REVERSED PHASE LIQUID CHROMATOGRAPHY; TIME OF FLIGHT MASS SPECTROMETRY;

CHROMATOGRAPHY, LIQUID; MEDICINE, CHINESE TRADITIONAL; MOLECULAR STRUCTURE; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

CYATHULA;

EID: 76649113117     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200900390     Document Type: Article

References (31)

1. The State Pharmacopoeia Commission of PR China, Pharmacopoeia of the People's Republic of China, vol. I, 2005 ed., Chemical Industry Press, Beijing 2005, p. 26.
2. Okuzumi, K., Hara, N., Uekusa, H., Fujimoto, Y., Org. Biomol. Chem. 2005, 3, 1227-1232.
3. Zhou, R., Li, B. G., Zhang, G. L., J. Asian Nat. Prod. Res. 2005, 7, 245-252.
4. Zhou, R., Li, B. G., Zhang, G. L., J. Integr. Plant. Biol. 2005, 47, 368-372.
5. Chen, X. M., Tian, G. Y., Chin. J. Chem. 2003, 21, 858-863.
6. Chen, X. M., Tian, G. Y., Carbohydr. Res. 2003, 338, 1235-1241.
7. Chen, Q. Y., Zhan, X. C., He, L. G., Zhang, Y. D., J. Chin. Med. 2001, 12, 203-210.
8. Qiao, C. F., Han, Q. B., Song, J. Z., Mo, S. F., Kong, L. D., Kung, H. F., Xu, H. X., J. Sep. Sci. 2007, 30, 813-818.
9. Song, J. Z., Mo, S. F., Yip, Y. K., Qiao, C. F., Han, Q. B., Xu, H. X., J. Sep. Sci. 2007, 30, 819-824.
10. Zhao, J., Zhang, X. Q., Li, S. P., Yang, F. Q., Wang, Y. T., Ye, W. C., J. Sep. Sci. 2006, 29, 2609-2615.
11. Ali, M. S., Ghori, M., Rafiuddin, S., Khatri, A. R., J. Pharm. Biomed. Anal. 2007, 43, 158-167.
12. Peru, K. M., Kuchta, S. L., Headley, J. V., Cessna, A. J., J. Chromatogr. A 2006, 1107, 152-158.
13. Ji, H. Y., Jeong, D. W., Kim, Y. H., Kim, H. H., Yoon, Y. S., Lee, K. C., Lee, H. S., Rapid Commun. Mass Spectrom. 2006, 20, 2127-2132.
14. Cohen, S., Lhuillier, F., Mouloua, Y., Vignal, B., Favetta, P., Guitton, J., J. Chromatogr. B 2007, 854, 165-172.
15. Guo, Y., Gaiki, S., J. Chromatogr. A 2005, 1074, 71-80.
16. Li, X. Q., Ji, C., Sun, Y. Y., Yang, M. L., Chu, X. G., Food Chem. 2009, 113, 692-700.
17. Chen, J. H., Liu, X. P., Xu, X. Q., Lee, F. S.-C., Wang, X. R., J. Pharm. Biomed. Anal. 2007, 43, 879-885.
18. Kumar, V., Shah, R. P., Malik, S., Singh, S., J. Pharm. Biomed. Anal. 2009, 49, 880-888.
19. Xie, G. X., Plumb, R., Su, M. M., Xu, Z. H., Zhao, A. H., Qiu, M. F., Long, X. b., Liu, Z., Jia, W., J. Sep. Sci. 2008, 31, 1015-1026.
20. Liu, X. X., Wang, L., Chen, X. Q., Deng, X. T., Cao, Y., Wang, Q., J. Sep. Sci. 2008, 31, 3834-3846.
21. Sun, H., Lv, H. T., Zhang, Y. M., Wang, X. J., Bi, K. S., Cao, H. X., J. Sep. Sci. 2007, 30, 3202-3206.
22. Geng, Q. M., Jin, C. X., Wang, X., Chin. J. Inform. TCM 2000, 7, 49-49.
23. Chen, X., Li, W. S., Zhu, J. W., Cui, H. M., Chin. J. Pharm. Anal. 2000, 20, 234-237.
24. Abdel-Gawad, M. M., EI-Nahas, H. A., El-Sayed, M. M., Abdel-Hameed, E. S., Bull. Pharm. Sci. 2004, 27, 99-111.
25. Melek, F. R., Toshio, M., Abdel Khalik, S. M., EI-Gindi, M. R., Phytochemistry 2003, 63, 401-407.
26. Christian, B., Kurt, H., Helv. Chim. Acta 1987, 70, 570-576.
27. Tabatadze, N., Elias, R., Robert, F., Pascal, G., De Pauw-Gillet, M. C., Kemertelidze, E., Chea, A., Ollivier, E., Chem. Pharm. Bull. 2007, 55, 102-105.
28. Okawa, M., Yamaguchi, R., Delger, H., Tsuchihashi, R., Nohara, T., Kinjo, J., Isoda, S., Ida, Y., Chem. Pharm. Bull. 2002, 50, 1097-1099.
29. Crespin, F., Ollivier, E., Lavaud, C., Babadjamian, A., Fame, R., Debrauwer, L., Bahursard, G., Phytochemistry 1993, 33, 657-661.
30. Crespin, F., Ollivier, E., Elias, R., Maillard, C., Balansard, G., J. Chromatogr. 1993, 644, 404-406.
31. Kinjo, J., Suyama, K., Nohara, T., Phytochemistry 1995, 40, 1765-1767.