Solid-phase microextraction for the detection of codeine, morphine and 6-monoacetylmorphine in human hair by gas chromatography-mass spectrometry

Forensic Science International

Volumn 196, Issue 1-3, 2010, Pages 64-69

  Moller, M ^a,b   Aleksa, K ^a   Walasek, P ^a   Karaskov, T ^a   Koren, G ^a,b  

^a HOSPITAL FOR SICK CHILDREN   (Canada)

^b UNIVERSITY OF TORONTO   (Canada)

Author keywords

Gas chromatography mass spectrometry; Hair analysis; Opiates; Solid phase microextraction

Indexed keywords

CODEINE; METHANOL; MORPHINE; MORPHINE 6 ACETATE;

ACCURACY; ANALYTIC METHOD; ANALYTICAL ERROR; ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; CROSS REACTION; ENZYME LINKED IMMUNOSORBENT ASSAY; EXPERIMENTAL STUDY; EXTRACTION; HAIR ANALYSIS; HUMAN; HUMAN TISSUE; INCUBATION TEMPERATURE; INTERMETHOD COMPARISON; ION MONITORING; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; SENSITIVITY AND SPECIFICITY; SIGNAL NOISE RATIO; SOLID PHASE MICROEXTRACTION; VALIDATION PROCESS;

EID: 76549135304     PISSN: 03790738     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.forsciint.2009.12.046     Document Type: Article

References (33)

1. Havens J.R., Stoops W.W., Leukefeld C.G., Garrity T.F., Carlson R.G., Falck R., et al. Prescription opiate misuse among rural stimulant users in a multistate community-based study. Am. J. Drug Alcohol Abus. 35 (2009) 18-23
2. Havens J.R., Oser C.B., and Leukefeld C.G. Increasing prevalence of prescription opiate misuse over time among rural probationers. J. Opioid Manag. 3 (2007) 107-111
3. Peindl K.S., Mannelli P., Wu L.T., and Patkar A.A. Trends in nonheroin opioid abuse admissions: 1992-2004. J. Opioid Manag. 3 (2007) 215-223
4. Fischer B., Rehm J., Brissette S., Brochu S., Bruneau J., El-Guebaly N., et al. Illicit opioid use in Canada: comparing social, health, and drug use characteristics of untreated users in five cities (OPICAN study). J. Urban Health 82 (2005) 250-266
5. Fischer B., Patra J., Cruz M.F., Gittins J., and Rehm J. Comparing heroin users and prescription opioid users in a Canadian multi-site population of illicit opioid users. Drug Alcohol Rev. (2008) 1-8
6. Solbergsdottir E., Bjornsson G., Gudmundsson L.S., Tyrfingsson T., and Kristinsson J. Validity of self-reports and drug use among young people seeking treatment for substance abuse or dependence. J. Addict. Dis. 23 (2004) 29-38
7. Katz N.P., Sherburne S., Beach M., Rose R.J., Vielguth J., Bradley J., et al. Behavioral monitoring and urine toxicology testing in patients receiving long-term opioid therapy. Anesth. Analg. 97 (2003) 1097-1102 table of contents
8. Vinner E., Vignau J., Thibault D., Codaccioni X., Brassart C., Humbert L., et al. Hair analysis of opiates in mothers and newborns for evaluating opiate exposure during pregnancy. Forensic Sci. Int. 133 (2003) 57-62
9. Fendrich M., Johnson T.P., Wislar J.S., Hubbell A., and Spiehler V. The utility of drug testing in epidemiological research: results from a general population survey. Addiction 99 (2004) 197-208
10. Musshoff F., Driever F., Lachenmeier K., Lachenmeier D.W., Banger M., and Madea B. Results of hair analyses for drugs of abuse and comparison with self-reports and urine tests. Forensic Sci. Int. 156 (2006) 118-123
11. Fishbain D.A., Cutler R.B., Rosomoff H.L., and Rosomoff R.S. Validity of self-reported drug use in chronic pain patients. Clin. J. Pain 15 (1999) 184-191
12. Vinner E., Vignau J., Thibault D., Codaccioni X., Brassart C., Humbert L., et al. Neonatal hair analysis contribution to establishing a gestational drug exposure profile and predicting a withdrawal syndrome. Ther. Drug Monit. 25 (2003) 421-432
13. Pragst F., and Balikova M.A. State of the art in hair analysis for detection of drug and alcohol abuse. Clin. Chim. Acta 370 (2006) 17-49
14. Baumgartner A.M., Jones P.F., Baumgartner W.A., and Black C.T. Radioimmunoassay of hair for determining opiate-abuse histories. J. Nucl. Med. 20 (1979) 748-752
15. Pelli B., Traldi P., Tagliaro F., Lubli G., and Marigo M. Collisional spectroscopy for unequivocal and rapid determination of morphine at ppb level in the hair of heroin addicts. Biomed. Environ. Mass Spectrom. 14 (1987) 63-68
16. Marigo M., Tagliaro F., Poiesi C., Lafisca S., and Neri C. Determination of morphine in the hair of heroin addicts by high performance liquid chromatography with fluorimetric detection. J. Anal. Toxicol. 10 (1986) 158-161
17. Gambelunghe C., Rossi R., Ferranti C., Rossi R., and Bacci M. Hair analysis by GC/MS/MS to verify abuse of drugs. J. Appl. Toxicol. 25 (2005) 205-211
18. Kintz P., Ludes B., and Mangin P. Detection of drugs in human hair using Abbott ADx, with confirmation by gas chromatography/mass spectrometry (GC/MS). J. Forensic Sci. 37 (1992) 328-331
19. Lachenmeier K., Musshoff F., and Madea B. Determination of opiates and cocaine in hair using automated enzyme immunoassay screening methodologies followed by gas chromatographic-mass spectrometric (GC-MS) confirmation. Forensic Sci. Int. 159 (2006) 189-199
20. Romolo F.S., Rotolo M.C., Palmi I., Pacifici R., and Lopez A. Optimized conditions for simultaneous determination of opiates, cocaine and benzoylecgonine in hair samples by GC-MS. Forensic Sci.Int. 138 (2003) 17-26
21. Wu Y.H., Lin K.L., Chen S.C., and Chang Y.Z. Simultaneous quantitative determination of amphetamines, ketamine, opiates and metabolites in human hair by gas chromatography/mass spectrometry. Rapid Commun. Mass Spectrom. 22 (2008) 887-897
22. Klys M., Rojek S., Kulikowska J., Bozek E., and Scislowski M. Usefulness of multi-parameter opiates-amphetamines-cocainics analysis in hair of drug users for the evaluation of an abuse profile by means of LC-APCI-MS-MS. J. Chromatogr. B. Analyt. Technol. Biomed. Life. Sci. 854 (2007) 299-307
23. Miller E.I., Wylie F.M., and Oliver J.S. Simultaneous detection and quantification of amphetamines, diazepam and its metabolites, cocaine and its metabolites, and opiates in hair by LC-ESI-MS-MS using a single extraction method. J. Anal. Toxicol. 32 (2008) 457-469
24. Moore C., Marinetti L., Coulter C., and Crompton K. Analysis of pain management drugs, specifically fentanyl, in hair: application to forensic specimens. Forensic Sci. Int. 176 (2008) 47-50
25. Xiang P., Shen M., Shen B.H., Ma D., Bu J., Jiang Y., et al. Determination of opiates in biological human samples by liquid chromatography-tandem mass spectrometry. Fa Yi Xue Za Zhi 22 (2006) 52-54 57
26. Ulrich S. Solid-phase microextraction in biomedical analysis. J. Chromatogr. A. 902 (2000) 167-194
27. Arthur C.L., and Pawliszyn J. Solid-phase microextraction with thermal desorption using fused silica optical fibers. Anal. Chem. 62 (1990) 2145-2148
28. Armbruster D.A., Tillman M.D., and Hubbs L.M. Limit of detection (LQD)/limit of quantitation (LOQ): comparison of the empirical and the statistical methods exemplified with GC-MS assays of abused drugs. Clin. Chem. 40 (1994) 1233-1238
29. Kintz P., and Mangin P. Simultaneous determination of opiates, cocaine and major metabolites of cocaine in human hair by gas chromotography/mass spectrometry (GC/MS). Forensic Sci.Int. 73 (1995) 93-100
30. Sporkert F., and Pragst F. Determination of methadone and its metabolites EDDP and EMDP in human hair by headspace solid-phase microextraction and gas chromatography-mass spectrometry. J. Chromatogr. B Biomed. Sci. Appl. 746 (2000) 255-264
31. Jones J., Tomlinson K., and Moore C. The simultaneous determination of codeine, morphine, hydrocodone, hydromorphone, 6-acetylmorphine, and oxycodone in hair and oral fluid. J. Anal. Toxicol. 26 (2002) 171-175
32. Polettini A., Groppi A., and Montagna M. Rapid and highly selective GC/MS/MS detection of heroin and its metabolites in hair. Forensic Sci.Int. 63 (1993) 217-225
33. Balabanova S., and Albert W. Accumulation and stability of drugs in hair. Arch. Kriminol. 193 (1994) 100-112