Synthesis of gadolinia-doped ceria gels and powders from acetylacetonate precursors

Journal of Sol-Gel Science and Technology

Volumn 53, Issue 1, 2010, Pages 1-11

  Shaw, Leon L ^a   Shen, Chunhui ^a,b   Thomas, Edwin L ^c  

^a UNIVERSITY OF CONNECTICUT   (United States)

^b WUHAN UNIVERSITY OF TECHNOLOGY   (China)

^c Massachusetts Institute of Technology Cambridge   (United States)

Author keywords

Cerium acetylacetonate; Gadolinia doped ceria oxide; Gadolinium acetylacetonate; Sol gel processing

Indexed keywords

ACETYLACETONATES; GADOLINIA DOPED CERIA; SOL-GEL PROCESSING;

CALCINATION; CERIUM; CERIUM COMPOUNDS; COAGULATION; GADOLINIUM; GELATION; GELS; GRAIN GROWTH; HYDROLYSIS; MORPHOLOGY; SOL-GELS; SOLS; SYNTHESIS (CHEMICAL);

SOL-GEL PROCESS;

EID: 74849130737     PISSN: 09280707     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10971-009-2043-x     Document Type: Article

References (40)

1. NQ Minh 1993 Ceramic fuel cells J Am Ceram Soc 76 563 588 10.1111/j.1151-2916.1993.tb03645.x 1:CAS:528:DyaK3sXls1eqsLk%3D
2. SPS Badwal K Foger 1996 Solid oxide electrolyte fuel cell review Ceram Int 22 257 265 10.1016/0272-8842(95)00101-8 1:CAS:528:DyaK28XivVWmsro%3D (Pubitemid 126337821)
3. E Wanzenberg F Tietz P Panjan D Stover 2003 Influence of pre- and post-heat treatment of anode substrates on the properties of DC-sputtered YSZ electrolyte films Solid State Ionics 159 1 8 10.1016/S0167-2738(02)00922-0 1:CAS:528:DC%2BD3sXitVKksr0%3D
4. S Souza SJ Visco LC De Jonghe 1997 Thin-film solid oxide fuel cell with high performance at low-temperature Solid State Ionics 98 57 61 10.1016/S0167-2738(96)00525-5 (Pubitemid 127432458)
5. K Wiik CR Schmidt S Faaland S Shamsili MA Einarsrud T Grande 1999 Reactions between strontium-substituted lanthanum manganite and yttria-stabilized zirconia: I, powder samples J Am Ceram Soc 82 721 728 1:CAS:528:DyaK1MXitVOqtLg%3D
6. YL Liu S Primdahl M Mogensen 2003 Effects of impurities on microstructure in Ni/YSZ-YSZ half-cells for SOFC Solid State Ionics 161 1 10 10.1016/S0167-2738(03)00271-6 1:CAS:528:DC%2BD3sXmsVaqs7s%3D
7. BCH Steele A Heinzel 2001 Materials for fuel-cell technologies Nature 414 345 352 10.1038/35104620 1:CAS:528:DC%2BD3MXovFGitrs%3D 11713541 2001Natur.414..345S (Pubitemid 33097817)
8. 0.2 synthesized using various techniques Solid State Ionics 111 9 15 10.1016/S0167-2738(98)00172-6 1:CAS:528:DyaK1cXlt1aitLw%3D
9. 2-y/2 electrolytes for IT-SOFC operation at 500 °C Solid State Ionics 129 95 110 10.1016/S0167-2738(99)00319-7 1:CAS:528:DC%2BD3cXivVantbg%3D (Pubitemid 30582793)
10. MA Panhans RN Blumenthal 1993 A thermodynamic and electrical conductivity study of nonstoichiometric cerium dioxide Solid State Ionics 60 279 298 10.1016/0167-2738(93)90006-O 1:CAS:528:DyaK3sXktlyitrk%3D
11. D Terribile A Trovarelli J Llorca C de Leitenburg G Dolcetti 1998 The synthesis and characterization of mesoporous high-surface area ceria prepared using a hybrid organic/inorganic route J Catal 178 299 308 10.1006/jcat.1998. 2152 1:CAS:528:DyaK1cXls1Shur0%3D
12. X Yu F Li X Ye X Xin Z Xue 2000 Synthesis of cerium(IV) oxide ultrafine particles by solid-state reactions J Am Ceram Soc 83 964 966 10.1111/j.1151-2916.2000.tb01686.x 1:CAS:528:DC%2BD3cXis1Wrsrg%3D
13. T Tsuzki PG McCormik 2001 Synthesis of ultrafine ceria powders by mechanochemical processing J Am Ceram Soc 84 1453 1458
14. SB Boskovic BZ Matovic MD Vlajic VD Krstic 2007 Modified glycine nitrate procedure (MGNP) for the synthesis of SOFC nanopowders Ceram Int 33 89 93 10.1016/j.ceramint.2005.07.022 1:CAS:528:DC%2BD28XhtFKhtL3J (Pubitemid 44692012)
15. S Boskovic D Durovic Z Dohcevic-Mitrovic Z Popovic M Zinkevich F Aldinger 2005 Self propagating room temperature synthesis of nanopowders for SOFC J Power Sources 145 237 242 10.1016/j.jpowsour.2005.01.085 1:CAS:528: DC%2BD2MXot1Wlsb4%3D
16. MA Thundathil W Lai L Noailles BS Dunn SM Haile 2004 High surface-area ceria aerogel J Am Ceram Soc 87 1442 1445 1:CAS:528:DC%2BD2cXntVCisrw%3D
17. E Stewart MS Bhuiyan S Sathyamurthy M Paranthaman 2006 Studies of solution deposited cerium oxide thin films on textured Ni-alloy substrates for YBCO superconductor Mater Res Bull 41 1063 1068 10.1016/j.materresbull.2005.11. 015 1:CAS:528:DC%2BD28XkvFOjtLs%3D (Pubitemid 43766617)
18. C Xia Y Zhang M Liu 2003 LSM-GDC composite cathodes derived from a sol-gel process Electrochem Solid-State Lett 6 A290 A292 10.1149/1.1621830 1:CAS:528:DC%2BD3sXosF2ksr8%3D
19. C Guizard A Julbe O Robbe S Sarrade 2005 Synthesis and oxygen transport characteristics of dense and porous cerium/gadolinium oxide materials: interest in membranes reactors Catal Today 104 120 125 10.1016/j.cattod.2005.03.046 1:CAS:528:DC%2BD2MXltFGit7w%3D (Pubitemid 43160276)
20. X Xu Z Jiang X Fan C Xia 2006 LSM-SDC electrodes fabricated with an ion-impregnating process for SOFCs with doped ceria electrolytes Solid State Ionics 177 2113 2117 10.1016/j.ssi.2006.01.043 1:CAS:528:DC%2BD28XhtFSntrbO 19-25 (Pubitemid 44572420)
21. X Sha Z Lu X Huang J Miao Z Ding X Xin W Su 2007 Study on La and Y co-doped ceria-based electrolyte materials J Alloys Compd 428 59 64 10.1016/j.jallcom.2006.03.077 1:CAS:528:DC%2BD2sXmvFOm (Pubitemid 44969523)
22. S Pinol M Najib DM Bastidas A Calleja XG Capdevila M Segarra F Espiell JC Ruiz-Morales D Marrero-Lopez P Nunez 2004 Microstructure-conductivity relationship in Gd- and Sm-doped cerai-based electrolytes prepared by the acrylamide sol-gel-related method J Solid State Electrochem 8 650 654 10.1007/s10008-004-0506-0 1:CAS:528:DC%2BD2cXmtVGgtrk%3D
23. J Livage M Henry C Sanchez 1988 Sol-gel chemistry of transition metal oxides Prog Solid State Chem 18 259 341 10.1016/0079-6786(88)90005-2 1:CAS:528:DyaL1MXlsVWisbs%3D
24. J Livage C Sanchez 1992 Sol-gel chemistry J Non-Cryst Solids 145 11 19 10.1016/S0022-3093(05)80422-3 1:CAS:528:DyaK38XlslKnurY%3D 1992JNCS..145...11L
25. J-M Herrmann C Hoang-Van L Dibansa R Harivololona 1996 An in situ electrical conductivity study of a CeO2 aerogel supported palladium catalyst in correlation with the total oxidation of propane J Catal 159 361 367 10.1006/jcat.1996.0098 1:CAS:528:DyaK28XivFCgt7c%3D (Pubitemid 126373147)
26. C Hoang-Van R Harivololona B Pommier 1995 Preparation of single and binary inorganic oxide aerogels and their use as supports for automotive palladium catalysts Stud Surface Sci Catal 91 435 443 10.1016/S0167-2991(06) 81780-5 1:CAS:528:DyaK2MXnvF2lsbo%3D
27. T Adachi S Sakka 1988 The role of N,N-dimethylformanide, A DCCA, in the formation of silica gel monoliths by sol-gel method J Non-Cryst Solids 99 118 128 10.1016/0022-3093(88)90464-4 1:CAS:528:DyaL1cXhslahsbk%3D 1988JNCS...99..118A (Pubitemid 18577838)
28. Klug HP, Alexander LE (1954) X-ray diffraction procedures for polycrystalline and amorphous materials. Wiley, London
29. AR Stokes AJC Wilson 1944 The diffraction of X-rays by distorted crystal aggregates-I Proc Phys Soc London 56 174 181 10.1088/0959-5309/56/3/303 1:CAS:528:DyaH2MXhsFeh 1944PPS....56..174S
30. L Shaw J Villegas H Luo D Miracle 2003 Thermal stability of nanostructured Al93Fe3Ti2Cr2 alloys prepared via mechanical alloying Acta Mater 51 2647 2663 10.1016/S1359-6454(03)00075-2 1:CAS:528:DC%2BD3sXjt1egtLk%3D
31. AL Ortiz L Shaw 2004 X-ray diffraction analysis of a severely plastically deformed aluminum alloy Acta Mater 52 2185 2197 10.1016/j.actamat.2004.01.012 1:CAS:528:DC%2BD2cXjtFClsLo%3D
32. S Brunauer PH Emmett E Teller 1938 Adsorption of gases in multimolecular layers J Am Chem Soc 60 309 319 10.1021/ja01269a023 1:CAS:528: DyaA1cXivFaruw%3D%3D 1938JAChS..60..309B
33. EP Barrett LG Joyner PP Halenda 1951 The determination of pore volume and area distributions in porous substances. I. Computations from nitrogen isotherms J Am Chem Soc 73 373 380 10.1021/ja01145a126 1:CAS:528: DyaG3MXjsVygsg%3D%3D
34. P Chu DE Clark 1992 Infrared spectroscopy of silica sols-effects of water concentration, catalyst, and aging Spectrosc Lett 25 201 220 10.1080/00387019208020687 1992SpecL..25..201C
35. JL Rehspringer P Poix JC Bernier 1986 Synthesis of glass "precursor" BaO, TiO2, nH2O by gel processing J Non-Cryst Solids 82 286 292 10.1016/0022-3093(86)90143-2 1:CAS:528:DyaL28XksVOmu7o%3D 1986JNCS...82..286R
36. JB Chan J Jonas 1990 Effect of various amide additives on the tetramethoxysilane sol-gel process J Non-Cryst Solids 126 79 86 10.1016/0022-3093(90)91025-M 1:CAS:528:DyaK3MXkvVansg%3D%3D 1990JNCS..126...79C
37. AC Pierre GM Pajonk 2002 Chemistry of aerogels and their applications Chem Rev 102 4243 4265 10.1021/cr0101306 1:CAS:528:DC%2BD38XnvFCntLw%3D 12428989 (Pubitemid 35410371)
38. PF Simon R Ulrich HW Spiess U Wiesner 2001 Block copolymer-ceramic hybrid materials from organically modified ceramic precursors Chem Mater 13 3464 3486 10.1021/cm0110674 1:CAS:528:DC%2BD3MXnsV2nurs%3D (Pubitemid 32999285)
39. C Park J Yoon EL Thomas 2003 Enabling nanotechnology with self assembled block copolymer patterns Polymer 44 6725 6760 10.1016/j.polymer.2003.08.011 1:CAS:528:DC%2BD3sXns12nsL0%3D (Pubitemid 37210458)
40. P Yang D Zhao DI Margolese BF Chmelka GD Stucky 1999 Block copolymer templating syntheses of mesoporous metal oxides with large ordering lengths and semicrystalline framework Chem Mater 11 2813 2826 10.1021/cm990185c 1:CAS:528:DyaK1MXmtF2kur0%3D