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74549191005
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note
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-1): 961 (m), 882 (s), 820 (m), 776 (vs), 699 (s), 514 (w), 456 (m). TGA: thermal analysis (Figure S2 in the Supporting Information) shows the endothermic release of ∼14 water molecules below 110°C [caled (found): 4.34 (4.25)].
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36
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74549157792
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note
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2 = 0.081 (all data), GOF = 1.009.
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