Sensitive determination of midazolam and 1′-hydroxymidazolam in plasma by liquid-liquid extraction and column-switching liquid chromatography with ultraviolet absorbance detection and its application for measuring CYP3A activity

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 811, Issue 2, 2004, Pages 153-157

  Yasui Furukori, Norio ^a   Inoue, Yoshimasa ^b   Tateishi, Tomonori ^a  

^a HIROSAKI UNIVERSITY   (Japan)

^b Mitsubishi Pharma   (Japan)

Author keywords

1 Hydroxymidazolam; CYP3A4; HPLC; Midazolam

Indexed keywords

CHLOROFORM; FLOW RATE; MIDAZOLAM;

CHEMICAL OPERATIONS; ERROR ANALYSIS;

LIQUID CHROMATOGRAPHY;

ACETONITRILE; ALPHA HYDROXYMIDAZOLAM; BUFFER; CHLOROFORM; CYTOCHROME P450 3A; DRUG METABOLITE; HEXANE; MIDAZOLAM; PERCHLORIC ACID; PHOSPHATE;

ADULT; ANALYTICAL ERROR; ARTICLE; AUTOANALYSIS; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG ISOLATION; FEMALE; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HUMAN EXPERIMENT; INJECTION; LIGHT ABSORPTION; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; MALE; MEASUREMENT; NORMAL HUMAN; PH; PLASMA; PLASMA VOLUME; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SENSITIVITY ANALYSIS; SEPARATION TECHNIQUE; ULTRAVIOLET RADIATION; VALIDATION PROCESS;

ADULT; ARYL HYDROCARBON HYDROXYLASES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CYTOCHROME P-450 CYP3A; FEMALE; HUMANS; MALE; MIDAZOLAM; OXIDOREDUCTASES, N-DEMETHYLATING; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROPHOTOMETRY, ULTRAVIOLET;

EID: 7444226773     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2004.08.039     Document Type: Article

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