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23 (1361.61): calcd. C 28.20, H 3.97, N 20.56; found C 28.01, H 3.81, N 20.42. IR(KBr): 3435(w), 1665(m), 1625(s), 1601(m), 1574(s), 1529(m), 1475(m), 1427(s), 1395(s), 1360(m), 818(m), 802(m), 745(m), 726(s), 676(m).
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23 (1361.61): calcd. C 28.20, H 3.97, N 20.56; found C 28.01, H 3.81, N 20.42. IR(KBr): 3435(w), 1665(m), 1625(s), 1601(m), 1574(s), 1529(m), 1475(m), 1427(s), 1395(s), 1360(m), 818(m), 802(m), 745(m), 726(s), 676(m).
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32
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74149090335
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Crystal data for 1: M, 1361.61, Monoclinic, C2/c, a, 32.975(7) Å, b, 8.297(4) Å, c, 24.868(5) Å, β, 130.06(3)°, V, 5207(4) Å3, Z, 4, F(000, 2728, GOF, 1.070, R1, 0.0303, wR2, 0.0651 [I > 2σ(I, Data collection of 1 was performed with Mo Kα radiation (λ, 0.71073 Å) on a Rigaku SCXmini diffractometer by the ω scan technique at room temperature. The structure was solved by direct methods and refined with full-matrix least-squares technique using SHELXTL-97 software package [13, All non-H atoms were refined anisotropically. The aqua H atoms were located on Fourier map. All other H atoms were placed in geometrically idealized positions and constrained to ride on their parent atoms with UisoH, 1.2 Ueq
-
2 = 0.0651 [I > 2σ(I)]. Data collection of 1 was performed with Mo Kα radiation (λ = 0.71073 Å) on a Rigaku SCXmini diffractometer by the ω scan technique at room temperature. The structure was solved by direct methods and refined with full-matrix least-squares technique using SHELXTL-97 software package [13]. All non-H atoms were refined anisotropically. The aqua H atoms were located on Fourier map. All other H atoms were placed in geometrically idealized positions and constrained to ride on their parent atoms with Uiso(H) = 1.2 Ueq.
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