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note
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3 (261.29): calcd. C, 36.74; H, 3.06; N, 26.79. Found: C, 36.65; H, 2.95; N, 26.68%. IR(KBr): 3421(w), 1662(m), 1631(s), 1600(m), 1570(s), 1525(m), 1467(m), 1421(s), 1392(s), 819(m), 802(m), 746(m), 725 (s), 677(m).
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30
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70349420307
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note
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2 = 0.1986 [I > 2σ(I)]. Data collections of 1 was performed with Mo Kα radiation (λ = 0.71073 Å) on a Rigaku SCXmini diffractometer by the ω scan technique at room temperature. The structures were solved by direct methods and refined with full-matrix least-squares technique using SHELXTL-97 software package [12]. All non-H atoms and H atoms were refined anisotropically. The aqua H atoms were located on Fourier map. All other H atoms were placed in geometrically idealized positions and constrained to ride on their parent atoms with Uiso(H) = 1.2 Ueq.
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31
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70349418983
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G.M. Sheldrick, SHELXS-97, Program for Crystal Structure Solution, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXS-97, Program for Crystal Structure Solution, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, University of Göttingen, Germany, 1997.
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